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中国精品科技期刊2020
孙雪,张蕊,范方宇,等. 复凝聚法制备西番莲果皮花色苷微胶囊及其性质分析[J]. 食品工业科技,2021,42(17):187−193. doi: 10.13386/j.issn1002-0306.2020120144.
引用本文: 孙雪,张蕊,范方宇,等. 复凝聚法制备西番莲果皮花色苷微胶囊及其性质分析[J]. 食品工业科技,2021,42(17):187−193. doi: 10.13386/j.issn1002-0306.2020120144.
SUN Xue, ZHANG Rui, FAN Fangyu, et al. Preparation and Properties of Anthocyanin Microcapsules from Passiflora edulis Rind by Complex Coacervation[J]. Science and Technology of Food Industry, 2021, 42(17): 187−193. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020120144.
Citation: SUN Xue, ZHANG Rui, FAN Fangyu, et al. Preparation and Properties of Anthocyanin Microcapsules from Passiflora edulis Rind by Complex Coacervation[J]. Science and Technology of Food Industry, 2021, 42(17): 187−193. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020120144.

复凝聚法制备西番莲果皮花色苷微胶囊及其性质分析

Preparation and Properties of Anthocyanin Microcapsules from Passiflora edulis Rind by Complex Coacervation

  • 摘要: 为提高花色苷稳定性,以西番莲果皮花色苷为芯材,明胶、阿拉伯胶为壁材,采用复凝聚法制备花色苷微胶囊。研究以包埋率为指标,采用响应面法优化西番莲果皮花色苷微胶囊最佳制备条件,进而以粒径、水分含量、形态及热稳定性研究了西番莲果皮花色苷微胶囊性质。结果表明:芯壁比1:4.7,壁材质量比(明胶: 阿拉伯胶质量比)6:7,壁材浓度1.5%,pH3.30,反应温度40 ℃,反应时间30 min,谷氨酰胺转氨酶25 U/g明胶,此时模型可靠性高,西番莲果皮花色苷包埋率最高为96.83%。最佳操作条件下所得微胶囊的粒径为12.15 μm,其水分含量为2.69%,微胶囊呈表面光滑的球形结构,熔融温度为82.51 ℃。此研究为西番莲果皮花色苷的应用提供了参考。

     

    Abstract: In order to improve the stability of anthocyanin, microcapsules of Passiflora edulis rind anthocyanin were prepared by complex coacervation using gelatin and gum Arabic as wall materials. In this study, the embedding efficiency of anthocyanin microcapsules was optimized by the Box-Behnken design. Meanwhile, properties of anthocyanin microcapsules were studied by droplet size, moisture content, morphology and thermal stability. The results showed that the optimum conditions of anthocyanin microcapsules were the core/wall ratio 1:4.7, gelatin/gum Arabi ratio 6:7, the wall material concentration 1.5%, pH value 3.30, reaction temperature 40 ℃, reaction time 30 min and transglutaminase dosage 25 U/g gelatin. Under these conditions, the model was reliable and the embedding efficiency of microcapsules was 96.83%. The particle size, moisture content, and the melting temperature of anthocyanin microcapsules were 12.15 μm, 2.69%, and 82.51 ℃, respectively. Microcapsules presented spherical structures with smooth surfaces. The research provides some references for the application of Passiflora edulis rind anthocyanin.

     

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