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中国精品科技期刊2020
雷春妮, 王波, 解迎双, 周小平, 张敏, 孙苗苗, 陈瑞霞. 吹扫捕集-气相色谱/质谱联用分析玫瑰花水香气成分[J]. 食品工业科技, 2020, 41(2): 201-206. DOI: 10.13386/j.issn1002-0306.2020.02.032
引用本文: 雷春妮, 王波, 解迎双, 周小平, 张敏, 孙苗苗, 陈瑞霞. 吹扫捕集-气相色谱/质谱联用分析玫瑰花水香气成分[J]. 食品工业科技, 2020, 41(2): 201-206. DOI: 10.13386/j.issn1002-0306.2020.02.032
LEI Chun-ni, WANG Bo, XIE Ying-shuang, ZHOU Xiao-ping, ZHANG Min, SUN Miao-miao, CHEN Rui-xia. Analysis of Rose Water Aroma Components by Purge and Trap-Gas Chromatography/Mass Spectrometry[J]. Science and Technology of Food Industry, 2020, 41(2): 201-206. DOI: 10.13386/j.issn1002-0306.2020.02.032
Citation: LEI Chun-ni, WANG Bo, XIE Ying-shuang, ZHOU Xiao-ping, ZHANG Min, SUN Miao-miao, CHEN Rui-xia. Analysis of Rose Water Aroma Components by Purge and Trap-Gas Chromatography/Mass Spectrometry[J]. Science and Technology of Food Industry, 2020, 41(2): 201-206. DOI: 10.13386/j.issn1002-0306.2020.02.032

吹扫捕集-气相色谱/质谱联用分析玫瑰花水香气成分

Analysis of Rose Water Aroma Components by Purge and Trap-Gas Chromatography/Mass Spectrometry

  • 摘要: 采用吹扫捕集-气相色谱/质谱联用技术首次分析了玫瑰花水的香气组成成分,并对苦水和大马士革两种玫瑰花水香气成分进行比较。结果表明,吹扫捕集最优实验参数为:样品量7.0 mL;吹扫温度40℃;吹扫时间13 min,此时苦水和大马士革玫瑰花水共鉴定出香气成分71种,其中苦水玫瑰花水69种,大马士革玫瑰花水61种;苦水、大马士革共有成分59种,苦水玫瑰花水特有成分10种(相对含量之和为4.15%),大马士革玫瑰花水特有成分2种,相对含量之和为0.54%。吹扫捕集法分析玫瑰花水香气成分操作简单,浓缩富集效率高,重现性好,绿色环保,真实全面地反映了玫瑰花水香气成分的构成,为玫瑰花水香气特征研究提供技术支撑,为其开发利用和产品质量控制提供理论依据。

     

    Abstract: The aroma composition of rose water was first analyzed by the combination of blowing capture-gas chromatography/mass spectrometry technique,and the aroma components of rose water in bitter water and damascus were compared. Results showed that,the optimum experimental parameters of purging and trapping were:Sample volume 7.0 mL,purging temperature 40℃,purging time 13 min. A total of 71 aroma components were identified in kushu water and damascus rose water,of which 69 kinds of kushui rose water,61 kinds of damascus rose water.There were 59 kinds of consensus ingredients of kushui water and damascus,10 kinds of special ingredients of kushui rose water with the relative contents was 4.15%,and the unique ingredients of damascus rose water were 0.54%. The method of purging and trapping analysis of rose water aroma components was simple in operation,high in enrichment,good in reproducibility,and friendly to environment,which reflected the composition of rose water aroma components and would provide the technology for the study of rose water aroma characteristics and theoretical basis for its development and utilization and product quality control.

     

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