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中国精品科技期刊2020
梁绍成, 肖小丽, 奉夏平, 黄秀丽, 陈嘉聪, 吕淑霞. 超声萃取-ICP-OES法快速测定食品中硼砂[J]. 食品工业科技, 2014, (03): 292-295. DOI: 10.13386/j.issn1002-0306.2014.03.020
引用本文: 梁绍成, 肖小丽, 奉夏平, 黄秀丽, 陈嘉聪, 吕淑霞. 超声萃取-ICP-OES法快速测定食品中硼砂[J]. 食品工业科技, 2014, (03): 292-295. DOI: 10.13386/j.issn1002-0306.2014.03.020
LIANG Shao-cheng, XIAO Xiao-li, FENG Xia-ping, HUANG Xiu-li, CHEN Jia-cong, LV Shu-xia. Rapid determination of borax in food by ICP-OES method with water ultrasonic extraction[J]. Science and Technology of Food Industry, 2014, (03): 292-295. DOI: 10.13386/j.issn1002-0306.2014.03.020
Citation: LIANG Shao-cheng, XIAO Xiao-li, FENG Xia-ping, HUANG Xiu-li, CHEN Jia-cong, LV Shu-xia. Rapid determination of borax in food by ICP-OES method with water ultrasonic extraction[J]. Science and Technology of Food Industry, 2014, (03): 292-295. DOI: 10.13386/j.issn1002-0306.2014.03.020

超声萃取-ICP-OES法快速测定食品中硼砂

Rapid determination of borax in food by ICP-OES method with water ultrasonic extraction

  • 摘要: 建立超声萃取-电感耦合等离子体发射光谱(ICP-OES)法快速测定食品中硼砂含量的方法。食品样品经水超声萃取后,直接采用ICP-OES法测定其中硼元素含量,再换算成硼砂的含量。该法在0.0550mg/L范围内线性良好,相关系数为0.9999,检出限为0.95mg/kg(以硼砂计),低中高三个不同浓度加标回收率为99.1%102.4%,相对标准偏差为0.55%0.80%。该方法操作简单,分析快速、灵敏、准确,适用于食品中硼砂含量的测定。 

     

    Abstract: Rapid determination method of borax content in food by inductively coupled plasma atomic emission spectrometry ( ICP- OES) with water ultrasonic extraction was established. Food sample was extracted by water ultrasonic, and the boron element content in food was directly determined by ICP- OES method, conversion into borax content again.The calibration curve was linear in the range of 0.0550mg /L, the correlation coefficient was 0. 9999 and the detection limit was 0.95mg /kg ( the borax) , the spiked recoveries ranged from 99.1% to 102.4% of three different levels, the relative standard deviation was 0.55% 0.80%.It indicated that the method was simple, sensitive, accurate and short of analytical cycle, which could meet the demand for the determination of borax content in food.

     

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