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中国精品科技期刊2020
何聪聪, 刘梦雅, 刘建彬, 刘笑生, 刘野, 宋焕禄. SPME和SAFE结合GC-O-MS分析鲜榨西瓜汁挥发性香气成分[J]. 食品工业科技, 2014, (02): 49-53. DOI: 10.13386/j.issn1002-0306.2014.02.022
引用本文: 何聪聪, 刘梦雅, 刘建彬, 刘笑生, 刘野, 宋焕禄. SPME和SAFE结合GC-O-MS分析鲜榨西瓜汁挥发性香气成分[J]. 食品工业科技, 2014, (02): 49-53. DOI: 10.13386/j.issn1002-0306.2014.02.022
HE Cong-cong, LIU Meng-ya, LIU Jian-bin, LIU Xiao-sheng, LIU Ye, SONG Huan-lu. Analysis of volatile aroma component of fresh watermelon juice by SPME and SAFE with GC-O-MS[J]. Science and Technology of Food Industry, 2014, (02): 49-53. DOI: 10.13386/j.issn1002-0306.2014.02.022
Citation: HE Cong-cong, LIU Meng-ya, LIU Jian-bin, LIU Xiao-sheng, LIU Ye, SONG Huan-lu. Analysis of volatile aroma component of fresh watermelon juice by SPME and SAFE with GC-O-MS[J]. Science and Technology of Food Industry, 2014, (02): 49-53. DOI: 10.13386/j.issn1002-0306.2014.02.022

SPME和SAFE结合GC-O-MS分析鲜榨西瓜汁挥发性香气成分

Analysis of volatile aroma component of fresh watermelon juice by SPME and SAFE with GC-O-MS

  • 摘要: 为比较不同萃取方式对西瓜汁风味的萃取效果,本研究采用固相微萃取(SPME)和溶剂辅助风味蒸发(SAFE)两种方法结合GC-O-MS对无籽西瓜中的挥发性香气成分进行分析。共鉴定出46种化合物,这些化合物主要包括醛类8种,烯醛类9种,醇类12种,酮类6种,呋喃2种,内酯1种,酯类2种。无籽西瓜中重要的挥发性香气成分有己醛(青草香)、6-甲基-5-庚烯-2-酮(柠檬味、苹果味)、反-6-壬烯醛(甜瓜味)、反-2-壬烯醛(甜瓜味、清香)、反,顺-2,6壬二烯醛(黄瓜味)、顺-3-壬烯-1-醇(清香、动物脂味)、反,顺-3,6-壬二烯-1-醇(黄瓜味)。SPME和SAFE对西瓜汁中关键香气成分均具有良好的萃取效果,但SPME萃取得到的化合物种类更多。 

     

    Abstract: In order to compare the different extraction methods on the flavor of seedless watermelon, the volatile aroma component of seedless watermelon were qualitatively and quantitatively analyzed by solid phase microextraction solvent assisted flavor evaporation with GC-O-MS. A total of 46 volatile aroma compounds were identified, mainly consisting of 8 aldehydes, 9 olefine aldehydes, 12 alcohols, 6 ketones, 2 furans, 1 lactone and 2 esters. The important volatile aroma component were hexanal (grass) , 6-methyl-5-Hepten-2-one (honeydew melon and fruity) , (E) -6-Nonenal (fruity) , (E) -2-Nonenal (melon and green) , (E, Z) -2, 6-Nonadienal (cumumber) , (Z) -3-Nonen-1-ol (green and fatty) , (E, Z) -3, 6-Nonadien-1-ol (cumumber) . SPME and SAFE both could extract odor-active compounds of watermelon juice adequately, while SPME could obtain more compounds.

     

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