Research on the Identification of Matheran Wine Region in the East Foot of Helan Mountain

KAI Jianrong; MA Haiyan; ZHANG Wei; CHEN Xiang; WANG Caiyan; ZHANG Jing; LI Caihong; GE Qian

doi:10.13386/j.issn1002-0306.2023100186

Volume 45 Issue 19

Sep. 2024

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Science and Technology of Food Industry > 2024 > 45(19): 278-285. > DOI: 10.13386/j.issn1002-0306.2023100186

KAI Jianrong, MA Haiyan, ZHANG Wei, et al. Research on the Identification of Matheran Wine Region in the East Foot of Helan Mountain[J]. Science and Technology of Food Industry, 2024, 45(19): 278−285. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2023100186.

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Research on the Identification of Matheran Wine Region in the East Foot of Helan Mountain

1.
Institute of Quality Standard and Testing Technology for Agro-Products of Ningxia, Yinchuan 750002, China
2.
Ningxia Polytechnic, Yinchuan 750021, China
3.
Institute of Agricultural Resources and Environment, Ningxia Academy of Agricultural and Forestry Sciences,Yinchuan 750002, China

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Received Date: October 22, 2023
Available Online: August 19, 2024

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Abstract

Abstract

Objective: To explore the feasibility of using stable carbon and oxygen isotopes and mineral elements in small-scale regional wine production identification, the fractionation characteristics of stable isotopes of carbon and oxygen in wine of Matheran single wine from different sub-producing areas at the eastern foot of Helan Mountain in Ningxia were studied. Methods: Forty-five samples of Massellan single wine from 5 sub-producing areas of Hongsipu, Qingtongxia, Yongning, Helan, and Zhenbeipu were selected to analyze the mineral element contents and the values of δ¹³C and δ¹⁸O. The fisher linear discriminant analysis method was used to establish a wine region discriminant model based on stable isotopes and mineral elements. Result: Carbon and oxygen stable isotopes exhibited significant fractionation during wine fermentation, with a total δ¹³C>ethanol δ¹³C>glycerol δ¹³C, and the three showed a certain degree of homology. The order of the δ¹⁸O size was grape juice δ¹⁸O>wine δ¹⁸O>water δ¹⁸O. As、B、K、Li、Mn、Ni、Pb、Rb、Sb、Sr、Ti and Cs showed significant differences between some production areas (P<0.05). There was no significant difference in the distribution of δ¹³C, δ¹⁸O, Ba, Ca and other 13 mineral elements among different regions (P>0.05). The accuracy rate of origin discrimination based on stable carbon and oxygen isotopes was only 40%, while the accuracy rates based on mineral elements and carbon and oxygen stable isotopes combined with mineral elements were both 95.6%. Conclusion: Mineral elements can distinguish wine samples from different sub-producing areas effectively. Stable carbon and oxygen isotopes cannot be used to identify the producing areas of wine from different small-scale regions.
- wine at the eastern of Helan Mountain,
- sub-producing area,
- stable isotope,
- mineral elements,
- origin identification

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References

[1]	王舒伟, 马雪蕾, 马银凤, 等. ‘马瑟兰’葡萄在我国的栽培表现及研究进展[J]. 中外葡萄与葡萄酒,2019(3):66−70. [WANG S W, MA X L, MA Y F, et al. Cultivation performance and research progress on 'Marselan' grapevine in China[J]. Sino-Overseas Grapevine & Wine,2019(3):66−70.] WANG S W, MA X L, MA Y F, et al. Cultivation performance and research progress on 'Marselan' grapevine in China[J]. Sino-Overseas Grapevine & Wine, 2019（3）: 66−70.
[2]	白世践, 户金鸽, 蔡军社, 等. 极端干旱区酿酒葡萄品种‘马瑟兰’的光合和酿酒特性分析[J]. 新疆农业科学,2021,58(3):511−521. [BAI S J, HU J G, CAI J S, et al. Study on photosynthetic and vinification characteristics of wine grape varity 'Marseland' in extremely arid regions[J]. Xinjiang Agricultural Sciences,2021,58(3):511−521.] BAI S J, HU J G, CAI J S, et al. Study on photosynthetic and vinification characteristics of wine grape varity 'Marseland' in extremely arid regions[J]. Xinjiang Agricultural Sciences, 2021, 58（3）: 511−521.
[3]	张晓煜, 韩颖娟, 张磊, 等. 基于GIS的宁夏酿酒葡萄种植区划[J]. 农业工程学报,2007,23(10):275−278. [ZHANG X Y, HAN Y J, ZHANG L, et al. Planting regionalization of wine grape in Ningxia using GIS[J]. Transactions of the Chinese Society of Agricultural Engineering,2007,23(10):275−278.] doi: 10.3321/j.issn:1002-6819.2007.10.050 ZHANG X Y, HAN Y J, ZHANG L, et al. Planting regionalization of wine grape in Ningxia using GIS[J]. Transactions of the Chinese Society of Agricultural Engineering, 2007, 23（10）: 275−278. doi: 10.3321/j.issn:1002-6819.2007.10.050
[4]	BLOTEVOGEL S, SCHRECK E, LAPLANCHE C, et al. Soil chemistry and meteorological conditions influence the elemental profiles of West European wines[J]. Food Chemistry,2019,298:125033. doi: 10.1016/j.foodchem.2019.125033
[5]	RICARDO-RODRIGUES S, LARANJO M, COELLO R, et al. Terroir influence on quality of 'Crimson' table grapes[J]. Scientia Horticulturae,2019,245:244−249. doi: 10.1016/j.scienta.2018.10.035
[6]	ALONSO G P, PARGA-DANS E, ARRIBAS B P, et al. Elemental composition, rare earths and minority elements in organic and conventional wines from volcanic areas:The canary islands (Spain)[J]. PLoS One,2021,16(11):e0258739. doi: 10.1371/journal.pone.0258739
[7]	SOARES F, ANZANELLO M J, FOGLIATTO F S, et al. Element selection and concentration analysis for classifying South America wine samples according to the country of origin[J]. Computers and Electronics in Agriculture,2018,150:33−40. doi: 10.1016/j.compag.2018.03.027
[8]	ORELLANA S, JOHANSEN A M, GAZIS C. Geographic classification of U. S. Washington State wines using elemental and water isotope composition[J]. Food Chemistry,2019,1:100007.
[9]	刘霞, 李彩霞, 焦扬. 河西走廊张掖地区土壤、葡萄及葡萄酒矿质元素特征分析[J]. 中国酿造,2019,38(1):179−182. [LIU X, LI C X, JIAO Y. Characteristics analysis of mineral elements in soil, grapes and wine from Zhangye region of Hexi Corridor[J]. China Brewing,2019,38(1):179−182.] doi: 10.11882/j.issn.0254-5071.2019.01.036 LIU X, LI C X, JIAO Y. Characteristics analysis of mineral elements in soil, grapes and wine from Zhangye region of Hexi Corridor[J]. China Brewing, 2019, 38（1）: 179−182. doi: 10.11882/j.issn.0254-5071.2019.01.036
[10]	李彩虹, 开建荣, 闫玥, 等. 基于矿质元素的我国不同产地葡萄酒的判别分析[J]. 食品与发酵工业,2022,48(20):265−272. [LI C H, KAI J R, YAN Y, et al. Discriminant analysis of wines from different regions of China based on mineral elements[J]. Food and Fermentation Industries,2022,48(20):265−272.] LI C H, KAI J R, YAN Y, et al. Discriminant analysis of wines from different regions of China based on mineral elements[J]. Food and Fermentation Industries, 2022, 48（20）: 265−272.
[11]	YABUSHITA M, SHIBAYAMA N, NAKAJIMA K, et al. Selective glucose to fructose isomerization in ethanol catalyzed by hydrotalcites[J]. ACS Catalysis,2019,9(3):2101−2109. doi: 10.1021/acscatal.8b05145
[12]	CAMIN F, BONER M, BONTEMPO L, et al. Stable isotope techniques for verifying the declaregeographical origin of food in legal cases[J]. Trends in Food Science and Technology,2017,61(7):176−187.
[13]	LIU X, LIU Z, QIAN Q, et al. Isotope chemometrics determines farming methods and geographical origin of vegetables from Yangtze River Delta Region, China[J]. Food Chemistry,2021,342:128379. doi: 10.1016/j.foodchem.2020.128379
[14]	CRAWFORD J, HOLLINS S E, MEREDITH K T, et al. Precipitation stable isotope variability and subcloud evaporation processes in asemi-arid region[J]. Hydrological Processes,2017,31(1):20−34. doi: 10.1002/hyp.10885
[15]	CIAISi P, JOUZEL J. Deuterium and oxygen 18 in precipitation:Isotopic model, including mixed cloud processes[J]. Journal of Geophysical Research Atmospheres,1994,99(D8):16793−16803. doi: 10.1029/94JD00412
[16]	CHUNG I M, KIM J K, AN Y J, et al. Compound-specific δ¹³C and δ¹⁵N analyses of fatty acids and amino acids for discrimination of organic, pesticide-free, and conventional rice (Oryza sativa L.)[J]. Food Chemistry,2019,283:305−314. doi: 10.1016/j.foodchem.2018.12.129
[17]	YUAN Y Y, ZHANG W X, ZHANG Y Z, et al. Differentiating organically farmed rice from conventional and green rice harvested from an experimental field trial using stable isotopes and multi-element chemometrics[J]. Journal of Agricultural and Food Chemistry,2018,66(11):2607−2615. doi: 10.1021/acs.jafc.7b05422
[18]	LYU C G, YANG J, WANG T L, et al. A field trialsbased authentication study of conventionally and organically grown Chinese yams using light stable isotopes and multi-elemental analysis combined with machine learning algorithms[J]. Food Chemistry,2021,343:128506. doi: 10.1016/j.foodchem.2020.128506
[19]	吴浩, 谢丽琪, 靳保辉, 等. 气相色谱-燃烧-同位素比率质谱法测定葡萄酒中5种挥发性组分的碳同位素比值及其在产地溯源中的应用[J]. 分析化学,2015,43(3):344−349. [WU H, XIE L Q, JIN B H, et al. Gas chromatography-combustion-isotope ratio mass spectrometry for determination of five volatile components in wine and its application in geographical origin traceability[J]. Chinese Journal of Analytical Chemistry,2015,43(3):344−349.] doi: 10.11895/j.issn.0253-3820.140761 WU H, XIE L Q, JIN B H, et al. Gas chromatography-combustion-isotope ratio mass spectrometry for determination of five volatile components in wine and its application in geographical origin traceability[J]. Chinese Journal of Analytical Chemistry, 2015, 43（3）: 344−349. doi: 10.11895/j.issn.0253-3820.140761
[20]	江伟, 吴幼茹, 薛洁. C、H、O同位素分析在葡萄酒产区鉴别中的应用[J]. 食品科学,2016,37(6):166−171. [JIANG W, WU Y R, XUE J. Application of C, H and O isotopes for identifying the geographical origin of wines[J]. Food Science,2016,37(6):166−171.] doi: 10.7506/spkx1002-6630-201606030 JIANG W, WU Y R, XUE J. Application of C, H and O isotopes for identifying the geographical origin of wines[J]. Food Science, 2016, 37（6）: 166−171. doi: 10.7506/spkx1002-6630-201606030
[21]	开建荣, 石欣, 李彩虹, 等. 基于矿物元素技术的中宁不同产区枸杞的判别分析[J]. 食品与发酵工业,2022,48(9):253−260. [KAI J R, SHI X, LI C H, et al. Discriminant analysis of Lycium barbarum from different areas in Zhongning based on mineral element technique[J]. Food and Fermentation Industries,2022,48(9):253−260.] KAI J R, SHI X, LI C H, et al. Discriminant analysis of Lycium barbarum from different areas in Zhongning based on mineral element technique[J]. Food and Fermentation Industries, 2022, 48（9）: 253−260.
[22]	SPANGENBERG J E, ZUFFEREY V. Carbon isotope compositions of whole wine, wine solid residue, and wine ethanol, determined by EA-IRMS and GC-C-IRMS, can record the vine water status a comparative reappraisal[J]. Analytical and Bioanalytical Chemistry,2019,411(10):2031−2043. doi: 10.1007/s00216-019-01625-4
[23]	张遴, 蔡砚, 乐爱山, 等. 稳定同位素比质谱法鉴别蔗糖和甜菜糖[J]. 食品科学,2010,31(2):124−126. [ZHANG L, CAI Y, LE A S, et al. Element analysis stable isotope ratio mass spectrometric differentiation of cane sugar and beet sugar[J]. Food Science,2010,31(2):124−126.] ZHANG L, CAI Y, LE A S, et al. Element analysis stable isotope ratio mass spectrometric differentiation of cane sugar and beet sugar[J]. Food Science, 2010, 31（2）: 124−126.
[24]	中华人民共和国工业和信息化部. 起泡葡萄酒中二氧化碳的稳定碳同位素比值(¹³C/¹²C)测定方法稳定同位素比值质谱法 QB/T 4852-2015[S]. 北京:中国标准出版社, 2015. [Ministry of Industry and Information Technology of the People's Republic of China. Determination of thecarbon isotope ratio (¹³C/¹²C) of CO₂ in sparkling wines-Method using isotope mass spectrometry QB/T 4852-2015[S]. Beijing:China Standards Press, 2015.] Ministry of Industry and Information Technology of the People's Republic of China. Determination of thecarbon isotope ratio （¹³C/¹²C） of CO₂ in sparkling wines-Method using isotope mass spectrometry QB/T 4852-2015[S]. Beijing: China Standards Press, 2015.
[25]	中华人民共和国海关总署. 出口葡萄酒中丙三醇碳稳定同位素比值的测定液相色谱-稳定同位素比值质谱法 SN/T 4675.31-2019[S]. 北京:中国标准出版社, 2019. [General Administration of Customs of the People's Republic of China. Determination of carbon stable isotpope ratio of glycerol in wine for expore-LC-IRMS method SN/T 4675.31-2019[S]. Beijing:China Standards Press, 2019.] General Administration of Customs of the People's Republic of China. Determination of carbon stable isotpope ratio of glycerol in wine for expore-LC-IRMS method SN/T 4675.31-2019[S]. Beijing: China Standards Press, 2019.
[26]	中华人民共和国工业和信息化部. 葡萄酒中水的稳定氧同位素比值(¹⁸O/¹⁶O)测定方法同位素平衡交换法 QB/T 4853-2015[S]. 北京:中国标准出版社, 2015. [Ministry of Industry and Information Technology of the People's Republic of China. Determination of the oxygen ratio (¹⁸O/¹⁶O) of water in wines-Method using isotope equilibrium exchange reaction QB/T 4853-2015[S]. Beijing:China Standards Press, 2015.] Ministry of Industry and Information Technology of the People's Republic of China. Determination of the oxygen ratio （¹⁸O/¹⁶O） of water in wines-Method using isotope equilibrium exchange reaction QB/T 4853-2015[S]. Beijing: China Standards Press, 2015.
[27]	开建荣, 王彩艳, 王晓静, 等. 微波消解-ICP-MS法测定枸杞中49种无机元素含量[J]. 宁夏农林科技,2020,61(2):55−59. [KAI J R, WANG C Y, WANG X J, et al. Determination of 49 inorganic elements in Lycium barbarum by microwave digestion-ICP-MS[J]. Journal of Ningxia Agriculture and Forestry Science and Technology,2020,61(2):55−59.] doi: 10.3969/j.issn.1002-204x.2020.02.017 KAI J R, WANG C Y, WANG X J, et al. Determination of 49 inorganic elements in Lycium barbarum by microwave digestion-ICP-MS[J]. Journal of Ningxia Agriculture and Forestry Science and Technology, 2020, 61（2）: 55−59. doi: 10.3969/j.issn.1002-204x.2020.02.017
[28]	SMITH A M, STITT M. Coordination of carbon supply and plant growth[J]. Plant Cell and Environment,2010,30(9):1126−1149.
[29]	中华人民共和国国家质量监督检验检疫总局, 中国国家标准化管理委员会. 葡萄酒:GB/T 15037-2006[S]. 北京:中国标准出版社, 2006. [General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of China. Wine:GB/T 15037-2006[S]. Beijing:China Standards Press, 2006.] General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of China. Wine: GB/T 15037-2006[S]. Beijing: China Standards Press, 2006.
[30]	MONSALLIER-BITEA C, JAMIN E, LEES M, et al. Study of the influence of alcoholic fermentation and distillation on the oxygen-18/oxygen-16 isotope ratio of ethanol[J]. Journal of Agricultural and Food Chemistry,2006,54(2):279−284. doi: 10.1021/jf0516686
[31]	申雪. 葡萄酒中稳定同位素特征变化与影响因素及产地溯源研究[D]. 乌鲁木齐:新疆农业大学, 2021. [SHEN X. Study on the characteristic changes and influencing factor of stable isotope in wine and the traceability of producing area[D]. Urumqi:Xinjiang Agricultural University, 2021.] SHEN X. Study on the characteristic changes and influencing factor of stable isotope in wine and the traceability of producing area[D]. Urumqi: Xinjiang Agricultural University, 2021.
[32]	WU H, TIAN L, CHEN B, et al. Verification of imported red wine origin into China using multi isotope and elemental analyses[J]. Food Chemistry,2019,301:125137. doi: 10.1016/j.foodchem.2019.125137
[33]	MAGDAS D A, CUNA S, CRISTEA G, et al. Stable isotopesdetermination in some Romanian wines[J]. Isotopes in Environmental and Health Studies,2012,48(2):345−353. doi: 10.1080/10256016.2012.661731

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