Citation: | YE Jiaming, ZHONG Shihuan, YE Leihai, et al. Rapid Determination of Mebendazole and Its Metabolites in Cattle and Sheep Products by Captiva EMR-Lipid Technology Combined with UPLC-MS/MS[J]. Science and Technology of Food Industry, 2024, 45(3): 277−283. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2023030304. |
[1] |
SAHAR K H, GAMAl A E, FATMA Z, et al. Mebendazole from an anti-parasitic drug to a promising candidate for drug repurposing in colorectal cancer[J]. Life Sciences,2022(299):120−126.
|
[2] |
张洪玉, 赵明军, 彭翔, 等. 苯并咪唑类药物在鱼类上代谢规律及残留检测研究概况[J]. 中国渔业质量与标准,2012(2):94−100. [ZHANG H Y, ZHAO M J, PENG X, et al. Overview of metabolism and residue detection of benzimidazole drugs in fish[J]. Chinese Fishery Quality and Standards,2012(2):94−100.
|
[3] |
冯丽凤, 叶梦薇, 林浩学, 等. 超高效液相色谱-串联质谱法测定动物源性食品中9种苯并咪唑类药物残留[J]. 福建分析测试,2022(31):35−40. [FENG L F, YE M W, LIN H X, et al. Determination of 9 benzimidazole drug residues in animal derived foods by ultra high performance liquid chromatography tandem mass spectrometry[J]. Fujian Analysis and Testing,2022(31):35−40.
|
[4] |
于慧娟, 冯兵, 姜朝军, 等. 固相萃取-高效液相色谱法测定鱼/虾生物体中甲苯咪唑及代谢物的残留[J]. 分析试验室,2010,29(4):33−36. [YU H J, FENG B, JIANG C J, et al. Determination of residues of mebendazole and its metabolites in fish/shrimp organisms by solid phase extraction high performance liquid chromatography[J]. Chinese Journal of Analysis Laboratory,2010,29(4):33−36.
|
[5] |
姜朝军, 于慧娟, 蔡友琼, 等. 高效液相色谱法测定水产品中甲苯咪唑及其代谢物残留[J]. 食品与发酵工业,2009,35(12):130−133. [JINAG C J, YU H J, CAI Y Q, et al. Determination of mebendazole and its metabolites in fishery by HPLC-UV[J]. Food and Fermentation Industries,2009,35(12):130−133.
|
[6] |
温海滨, 林洁纯, 叶靖怡, 等. QuEChERS-超高效液相色谱-串联质谱法同时测定水产品中20种苯并咪唑类药物及其代谢物残留[J]. 食品安全质量检测学报,2021,12(18):7214−7221. [WEN H B, LIN J C, YE J Y, et al. Simultaneous determination of 20 benzimidazole drugs and their metabolite residues in aquatic products by QuEChERS ultra high performance liquid chromatography tandem mass spectrometry[J]. Journal of Food Safety & Quality,2021,12(18):7214−7221.
|
[7] |
刘永涛, 艾晓辉, 杨红. 同位素稀释高效液相色谱-串联质谱法测定水产品中甲苯咪唑及其代谢物的残留量[J]. 分析测试学报,2011,30(6):640−645. [LIU Y T, AI X H, YANG H. Simultaneous determination of mebendazole and its metabolites residues in fishery products by high performance liquid chromatography tandem mass spectrometry with isotope dilution[J]. Journal of Instrumental Analysis,2011,30(6):640−645.
|
[8] |
张培杨. 禽肉和禽蛋中左旋咪唑、甲苯咪唑及其两种代谢物残留HPLC-MS/MS检测方法的研究[D]. 扬州:扬州大学, 2021. [ZHANG P Y. Study on HPLC-MS/MS detection method for residues of levamisole, mebendazole, and their two metabolites in poultry meat and eggs[D]. Yangzhou:Yangzhou University, 2021.
ZHANG P Y. Study on HPLC-MS/MS detection method for residues of levamisole, mebendazole, and their two metabolites in poultry meat and eggs[D]. Yangzhou: Yangzhou University, 2021.
|
[9] |
陈思敏, 吴映璇, 蓝草, 等. 超高效液相色谱-串联质谱法测定乳制品中苯并咪唑类药物及其代谢物的残留量[J]. 理化检验(化学分册),2020,56(5):553−564. [CHEN S M, WU Y X, LAN C, et al. Determination of benzimidazole drugs and their metabolites in dairy products by ultra high performance liquid chromatography tandem mass spectrometry[J]. Physical Testing and Chemical Analysis(Part B:Chemical Analysis),2020,56(5):553−564.
|
[10] |
BEATRIZ A L, ELENA L, MYRA F F, et al. Development and validation of a methodology based on Captiva EMR-lipid clean-up and LC-MS/MS analysis for the simultaneous determination of mycotoxins in human plasma[J]. Talanta,2020(206):193−198.
|
[11] |
ANNA S, ANDRE W, RAGUI S, et al. A validated LC-MS/MS method for the quantitation of cefazolin in human adipose tissue:Application of EMR-Lipid sorbent as an efficient sample clean-up before mass spectrometric analyses[J]. Journal of Pharmaceutical and Biomedical Analysis,2022(213):114−151.
|
[12] |
YIN ZY, YUAN B, LYU W T, et al. Method development and validation for analysis of phenolic compounds in fatty complex matrices using enhanced matrix removal (EMR) lipid cleanup and UHPLC-QqQ-MS/MS[J]. Food Chemistry,2022,373:131096. doi: 10.1016/j.foodchem.2021.131096
|
[13] |
MIKAEL P, ELEA H, EDERINA N, et al. Analysis of veterinary drug- and pesticide residues in pig muscle by LC-QTOF-MS[J]. Food Control,2023(148):445−461.
|
[14] |
HONG W, HAOT, LIAN F A, et al. Screening and quantification of 146 veterinary drug residues in beef and chicken using QuEChERS combined with high performance liquid chromatography-quadrupole orbitrap mass spectrometry[J]. Food Chemistry,2023(405):234−241.
|
[15] |
陈思敏, 吴映璇, 邹游, 等. 高效液相色谱-串联质谱法测定乳和乳制品中19种苯并咪唑类药物及其代谢物残留量[J]. 食品安全质量检测学报,2019,10(24):8251−8260. [CHEN S M, WU Y X, ZOU Y, et al. Determination of 19 benzimidazole drugs and their metabolites residues in milk and dairy products by high performance liquid chromatography tandem mass spectrometry[J]. Journal of Food Safety & Quality,2019,10(24):8251−8260.
|
[16] |
李蓉, 杨璐齐, 罗阳丹, 等. QuEChERS/UPLC-Q-Orbitrap HRMS法测定水产及水产加工品中16种苯并咪唑类与13种硝基咪唑类药物残留[J]. 分析测试学报,2018,37(5):547−555. [LI R, YANG L Q, LUO Y D, et al. QuEChERS/UPLC-Q-Orbitrap HRMS method for the determination of 16 benzoimidazole and 13 nitroimidazole drug residues in aquatic products and processed products[J]. Journal of Instrumental Analysis,2018,37(5):547−555.
|
[17] |
陈瑞, 杨志伟, 朱凤妹, 等. 超高效液相色谱-串联质谱法测定牛奶和奶粉中五种苯并咪唑类药物[J]. 核农学报,2020,34(8):1776−1784. [CHEN R, YANG Z W, ZHU F M, et al. Determination of five benzimidazole drugs in milk and milk powder by ultra high performance liquid chromatography tandem mass spectrometry[J]. Journal of Nuclear Agricultural Sciences,2020,34(8):1776−1784.
|
[18] |
徐幸, 张燕, 舒平, 等. QuEChERS-同位素质谱内标法检测动物源性食品中 20 种头孢菌素的残留量[J]. 食品工业科技,2022,43(24):320−330. [XU X, ZHANG Y, SHU P, et al. Determination of 20 kinds of cephalosporins residues in animal derived food by QuEChERS-LC-MS/MS with isotope internal standards method[J]. Science and Technology of Food Industry,2022,43(24):320−330.
|
[19] |
LI H, WANG C, ZHU Q, et al. Reduction of matrix effects through a simplified QuEChERS method and using small injection volumes in a LC-MS/MS system for the determination of 28 pesticides in fruits and vegetables[J]. Analytical Methods,2016,8:5061−5069. doi: 10.1039/C6AY00080K
|
[20] |
HAN Y T, SONG L, LIU S W, et al. Simultaneous determination of 124 pesticide residues in Chinese liquor and liquor-making raw materials (sorghum and rice hull) by rapid multi-plug filtration cleanup and gas chromatography-tandem mass spectrometry[J]. Food Chemistry,2018,241(feb.15):258−267.
|
[21] |
密叶, 孙枫林, 丰暖, 等. Captiva EMR-Lipid过滤柱净化结合液相色谱串联质谱法测定海产品中9种羟基多溴联苯醚[J]. 中国卫生检验杂志,2022,32(5):517−520. [MI Y, SUN F L, FENG N, et al. Captiva EMR-Lipid filtration column purification combined with liquid chromatography tandem mass spectrometry for the determination of nine hydroxy polybrominated diphenyl ethers in seafood[J]. Chinese Journal of Health Laboratory,2022,32(5):517−520.
|
[22] |
王东鹏, 叶诚, 李小莎. Captiva EMR-Lipid固相萃取结合高效液相色谱-串联质谱法同时测定猪肉中氯霉素类药物残留量[J]. 食品安全质量检测学报,2021,12(19):7660−7666. [WANG D P, YE C, LI X S, et al. Simultaneous determination of chloramphenicol residues in pork using Captiva EMR-Lipid solid-phase extraction combined with high-performance liquid chromatography-tandem mass spectrometry[J]. Journal of Food Safety & Quality,2021,12(19):7660−7666.
|
[23] |
童兰艳, 肖昭竞, 李根容, 等. 超高效液相色谱-三重四极杆质谱法测定化妆品中 14 种美白活性成分[J]. 分析试验室,2022,41(1):96−102. [TONG L Y, XIAO Z J, LI G R, et al. Determination of 14 whitening active components in cosmetics by ultra-high performance liquid chromatography-triple quadrupole mass spectrometry[J]. Chinese Journal of Analysis Laboratory,2022,41(1):96−102.
|
[24] |
潘永波, 万娜, 王承业, 等. 快速滤过型净化结合液相色谱-质谱联用法测定海产品中19种磺胺类药物残留[J]. 食品工业科技,2023,44(7):320−328. [PAN Y B, WAN N, WANG C Y, et al. Determination of 19 sulfonamides residues in seafood by multi-plug filtration cleanup method combined with liquid chromatography-tandem mass spectrometry[J]. Science and Technology of Food Industry,2023,44(7):320−328.
|
[25] |
农业农村部, 国家卫生健康委, 市场监管总局. GB 31656.15-2022 食品安全国家标准 水产品中甲苯咪唑及其代谢物残留量的测定 液相色谱-串联质谱法[S]. 北京:中国标准出版社, 2022. [Ministry of Agriculture and Rural Affairs, National Health Commission, General Administration of Market Supervision. GB 31656.15-2022 National food safety standards Determination of mebendazole and its metabolites residues in aquatic products by liquid chromatography-tandem mass spectrometry method[S]. Beijing:Standards Press of China, 2022.
Ministry of Agriculture and Rural Affairs, National Health Commission, General Administration of Market Supervision. GB 31656.15-2022 National food safety standards Determination of mebendazole and its metabolites residues in aquatic products by liquid chromatography-tandem mass spectrometry method[S]. Beijing: Standards Press of China, 2022.
|
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