Preparation of Kiwifruit Biomass Carbon Dots by Microwave Method and Application of Fe<sup>3+</sup> Detection in Honeysuckle

ZHAO Hongbin; LENG Tiancui; LIU Xiaomeng; JIANG Yanping; LI Chunrong; MENG Tiehong; HU Xianyun

doi:10.13386/j.issn1002-0306.2021040147

Volume 43 Issue 3

Jan. 2022

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Science and Technology of Food Industry > 2022 > 43(3): 246-253. > DOI: 10.13386/j.issn1002-0306.2021040147

ZHAO Hongbin, LENG Tiancui, LIU Xiaomeng, et al. Preparation of Kiwifruit Biomass Carbon Dots by Microwave Method and Application of Fe³⁺ Detection in Honeysuckle[J]. Science and Technology of Food Industry, 2022, 43(3): 246−253. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021040147.

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Preparation of Kiwifruit Biomass Carbon Dots by Microwave Method and Application of Fe³⁺ Detection in Honeysuckle

1.
Department of Pharmacy, Qiannan Medical College for Nationalities, Duyun 558000, China
2.
Pharmacy of the Third Hospital Affiliated to Guizhou Medical University, Duyun 558000, China
3.
The Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China

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Received Date: April 14, 2021
Available Online: November 28, 2021

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Abstract

Abstract

In order to establish a rapid detection method for Fe³⁺, the kiwifruit biomass carbon dots (CDs) were prepared by microwave method with kiwifruit juice as carbon source and ethylenediamine as surface modifier. The CDs were rich in -OH, -NH and C-O groups, had an average particle size about 2.5 nm, which were soluble in water and stable. The CDs emitted blue fluorescence under 365 nm ultraviolet light. A new and rapid detection method for Fe³⁺ was established with the CDs based on the fluorescence quenching effect of Fe³⁺. When the addition amount of Fe³⁺ from 0.2 to 10 μmol/L, the fluorescent intensity (F/F₀) of CDs decreased linearly with the increase of Fe³⁺(R²=0.9934), and the limit of detection (S/N=3) was 0.12 μmol/L. This detection method was applied to the determination of Fe³⁺ content and the recovery was 98.82%～103.20% , RSD was between 1.67% and 2.05%. The operation of this detection method was simple, rapid and strong selective.
- kiwifruit,
- biomass,
- carbon dots,
- preparation method,
- honeysuckle,
- ferric ions,
- detection

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