Optimization of Separation Process of Eggshell and Shell Membrane

LIU Hengyang; GUO Xiaoxu; YIN Yuxin; SONG Shaoqi; LIU Meiyu; HE Hongju

doi:10.13386/j.issn1002-0306.2020090076

Volume 44 Issue 12

Jun. 2023

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Science and Technology of Food Industry > 2023 > 44(12): 193-200. > DOI: 10.13386/j.issn1002-0306.2020090076

LIU Hengyang, GUO Xiaoxu, YIN Yuxin, et al. Optimization of Separation Process of Eggshell and Shell Membrane[J]. Science and Technology of Food Industry, 2023, 44(12): 193−200. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020090076.

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Optimization of Separation Process of Eggshell and Shell Membrane

LIU Hengyang^{1, 2,},
GUO Xiaoxu¹,
YIN Yuxin¹,
SONG Shaoqi¹,
LIU Meiyu^{1, 2, ,},
HE Hongju^3, ,

1.
College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China
2.
Handan Key Laboratory of Natural Products and Functional Food Development, Handan 056038, China
3.
School of Food Science, Henan Institute of Science and Technology, Xinxiang 453003, China

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Received Date: September 07, 2022
Available Online: April 12, 2023

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Abstract

Abstract

The two must be separated first to exploit the eggshell and the eggshell membranes. In this paper, a combination of mechanical crushing, water flotation and dilute acid treatment was used for shell membrane separation, and the conditions of eggshell and subshell membrane separation were screened. The effects of hydrochloric acid volume, reaction time and hydrochloric acid concentration on the rate of eggshell membrane decalcification were investigated by single-factor tests. And the response surface method (RSM) was applied to optimize the process conditions for removing the residual eggshells from the eggshell membranes with dilute hydrochloric acid. The results showed that the shell-membrane separation effect was the best when the eggshells were crushed under the condition that the crusher runs for 5 s/time and crushes 3 times. The powder extraction rate was 58.72%, the membrane removal rate was 87.91%, and the comprehensive score was 72.91. The best conditions for removing the residual eggshell in the eggshell membrane with hydrochloric acid were 1 g crude eggshell membrane, 20 mL hydrochloric acid, 19 min reaction time, and 0.5 mol/L hydrochloric acid concentration, and the decalcification rate could reach 89.21%. This process would provide the technical support for the intensive processing of the eggshell.
- eggshell,
- shell membrane,
- separation,
- response surface optimization

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References (37)

References

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