Processing Comparative of Solvent Extraction and Ultrasonic-assisted Extraction for Polyphenols from <i>Lycium ruthenicum</i> Murr.

WU Yun; ZENG Wenqi; WANG Lipeng; YANG Nana; HU Haobin

doi:10.13386/j.issn1002-0306.2020040125

Volume 42 Issue 4

Feb. 2021

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Science and Technology of Food Industry > 2021 > 42(4): 108-114. > DOI: 10.13386/j.issn1002-0306.2020040125

WU Yun, ZENG Wenqi, WANG Lipeng, YANG Nana, HU Haobin. Processing Comparative of Solvent Extraction and Ultrasonic-assisted Extraction for Polyphenols from Lycium ruthenicum Murr.[J]. Science and Technology of Food Industry, 2021, 42(4): 108-114. DOI: 10.13386/j.issn1002-0306.2020040125

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Processing Comparative of Solvent Extraction and Ultrasonic-assisted Extraction for Polyphenols from Lycium ruthenicum Murr.

College of Chemistry and Chemical Engineering, Longdong University, Qingyang 745000, China

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Received Date: April 13, 2020
Available Online: March 01, 2021

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Abstract

Abstract

The suitable extraction technology of polyphenols from Lycium ruthenicum Murr. was investigated. Single factor experiments and Box-Behnken(BB)experimental design method were adopted to optimize the extraction technology parameters,and the solvent extraction and ultrasonic assisted extraction were compared in this paper. The results showed that the optimum extraction parameters of solvent extraction were:Ethanol volume fraction 70%,liquid to solid ratio 50:1 mL/g,extraction temperature 58 ℃,extraction time 37 min,and the yield of Lycium ruthenicum Murr. polyphenols was 35.9021 mg/g with the RSD to the predicted value was 0.95%. The optimum extraction parameters of ultrasonic assisted extraction were:Ethanol volume fraction 60%,liquid to solid ratio 50:1 mL/g,extraction temperature 36 ℃,extraction time 31 min and ultrasonic power 240 W,and the yield of Lycium ruthenicum Murr. polyphenols was 39.6845 mg/g with the RSD to the predicted value was 0.29%. It was found that the solvent extraction method had more ethanol dosage with 1.16 times than ultrasonic assisted extraction,the extraction temperature 22 ℃ higher and extended the extraction time 16.22% than the latter. Therefore,the ultrasonic-assisted extraction process had advantages of simple process,time-saving,low energy consumption and high efficiency,which would provide foundation for further study of Lycium ruthenicum Murr. polyphenols.
- Lycium ruthenicum Murr.,
- polyphenols,
- solvent extraction,
- ultrasonic-assisted extraction,
- response surface,
- process comparison

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[1]	林丽,晋玲,郭玉环. 不同产区黑果枸杞的鉴定[J]. 时珍国医国药,2018,29(11):2670-2673.
[2]	Wang H Q,Li J N,Tao W W,et al. Lycium ruthenicum studies:Molecular biology,phytochemistry and pharmacology[J]. Food Chemistry,2018,240:759-766.
[3]	郝媛媛,颉耀文,张文培,等. 荒漠黑果枸杞研究进展[J]. 草业科学,2016,33(9):1835-1845.
[4]	Liu Z G,Dang J,Wang Q L,et al. Optimization of polysaccharides from Lycium ruthenicum fruit using RSM and its antioxidant activity[J]. International Journal of Biological Macromolecules,2013,61:127-134.
[5]	孙晓红,王潼,吕康文,等. 野生黑枸杞与普通红枸杞营养成分和相关活性物质的分析与评价[J]. 营养学报,2016,38(5):509-511.
[6]	双全,张海霞,卢宇,等. 野生黑果枸杞化学成分及抗氧化活性研究[J]. 食品工业科技,2017,38(4):94-100.
[7]	张霞,张芳,高晓娟,等. 不同干燥方法对黑果枸杞中活性成分含量及其抗氧化活性的影响[J]. 中国中药杂志,2017,42(20):3926-3931.
[8]	尹民强,吴金龙,王天琦.等. 黑果枸杞抗氧化能力评价及比较研究[J]. 中国果菜,2019,39(11):52-56.
[9]	Luo Y,Fang J L,Yuan K,et al. Ameliorative effect of purified anthocyanin from Lycium ruthenicum on atherosclerosis in rats through synergistic modulation of the gut microbiota and NF-κB/SREBP-2 pathways[J]. Journal of Functional Foods,2019,59:223-233.
[10]	Peng Y J,Yan Y M,Wan P,et al. Gut microbiota modulation and anti-inflammatory properties of anthocyanins from the fruits of Lycium ruthenicum Murray in dextran sodium sulfate-induced colitis in mice[J]. Free Radical Biology and Medicine,2019,136:96-108.
[11]	Ni W H,Gao T T,Wang H L,et al. Anti-fatigue activity of polysaccharides from the fruits of four Tibetan Plateau indigenous medicinal plants[J]. Journal of Ethnopharmacology,2013,150(2):529-535.
[12]	曹茸茸. 黑果枸杞抗运动疲劳作用研究[D]. 兰州:甘肃中医药大学,2018:8-15.
[13]	Tian B M,Zhao J H,An W,et al. Lycium ruthenicum diet alters the gut microbiota and partially enhances gut barrier function in male C57BL/6 mice[J]. Journal of Functional Foods,2019,52:516-528.
[14]	林丽,李进,李永洁,等. 黑果枸杞花色巧对氧化低密度脂蛋白损伤血管内皮细胞的保护作用[J]. 中国药学杂志,2013,48(8):606-611.
[15]	Zhang G,Chen S S,Zhou W,et al. Anthocyanin composition of fruit extracts from Lycium ruthenicum and their protective effect for gouty arthritis[J]. Industrial Crops and Products,2019,129:414-423.
[16]	李钦俊,谭亮,杲秀珍,等. 柴达木野生黑果枸杞营养成分分析与比较[J]. 食品工业科技,2019,40(18):273-281 ,288.
[17]	郑覃,李建颖,杨璐,等. 超声辅助提取黑果枸杞花色苷的工艺优化[J]. 食品工业科技,2019,38(14):227-231.
[18]	姚思敏蔷,单虹宇,于雅静,等. 响应曲面法优化超声波辅助提取黑果枸杞中花青素工艺[J]. 食品工业科技,2017,38(16):210-215 ,219.
[19]	Li Y,Zou X,Shen T,et al. Determination of geographical origin and anthocyanin content of black goji berry(Lycium ruthenicum Murr.)using near infrared spectroscopy and chemometrics[J]Food Analytical Methods,2017,10:1034-1044.
[20]	Hu N,Zheng J,Li W C,et al. Isolation,stability,and antioxidant activity of anthocyanins from Lycium ruthenicum Murray and Nitraria tangutorum Bobr of Qinghai-Tibetan Plateau[J]. Separation Science and Technology,2014,49(18):2897-2906.
[21]	张佳,赫军,张蕾,等. 黑果枸杞果实化学成分研究[J]. 中国药学杂志,2016,51(24):2150-2154.
[22]	夏园园,莫仁楠,曲炜,等. 黑果枸杞化学成分研究进展[J]. 药学进展,2015,39(5):351-356.
[23]	周宁,戴旖旎,白旭光,等.姜黄素对肝癌细胞凋亡及TNF-α、IL-1β、IL-6炎性因子影响的机制研究[J]. 癌症进展,2017,15(11):1282-1285.
[24]	李巍巍,李俊发,郭安臣,等.植物多酚神经保护作用的研究进展[J]. 中国卒中杂志,2015,10(2):141-146.
[25]	Ainsworth E A,Gillespie K M. Estimation of total phenolic content and other oxidation substrates in plant tissues using Folin-Ciocalteu reagent[J]. Nature Protocols,2007,2(4):875-877.

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