XU Dan, CHEN Yunyun, SHEN Hongli, et al. Changes of Flavor Profile of Squid Tentacles during the Baking Process was Analyzed by Gas Chromatography-Ion Mobility Spectroscopy and Electronic Tongue[J]. Science and Technology of Food Industry, 2025, 46(11): 1−8. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2024060422.
Citation: XU Dan, CHEN Yunyun, SHEN Hongli, et al. Changes of Flavor Profile of Squid Tentacles during the Baking Process was Analyzed by Gas Chromatography-Ion Mobility Spectroscopy and Electronic Tongue[J]. Science and Technology of Food Industry, 2025, 46(11): 1−8. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2024060422.

Changes of Flavor Profile of Squid Tentacles during the Baking Process was Analyzed by Gas Chromatography-Ion Mobility Spectroscopy and Electronic Tongue

More Information
  • Received Date: June 27, 2024
  • Available Online: March 27, 2025
  • Gas chromatography-ion mobility spectroscopy and electronic tongue technology were used to analyze the differences and changes of flavor substances in the baking of squid tentacles, in order to study the changes of flavor profile in the baking of squid tentacles. The results showed that with the extension of baking time, the composition of free amino acids in squid tentacles changed little, which mainly affected the content of free amino acids, and then affected the quality and flavor of squid tentacles. There were obvious differences in the taste of squid tentacles during the baking process. The sour taste remained basically unchanged, and the umami, saltiness and umami richness showed an enhanced trend, without obvious bitterness and astringency. In the samples with five different baking times, 29 flavor compounds were detected, including 14 aldehydes, 3 ketones, 5 alcohols, 3 esters, 2 acids, and 2 olefins. Among them, aldehydes played a dominant role in the overall flavor of squid tentacles and showed an increasing trend with the extension of baking time, which was consistent with the trend of esters. However, the content of acid substances showed an opposite trend, and the content of ketone and alcohol substances first decreased and then increased. Less olefin content contributed less to the flavor. The flavor substances of the squid tentacles have changed significantly during the roasting process, which could help to understand the changes of the flavor contour during the roasting process, and provided a scientific basis for optimizing the squid whiskers roasting process and improved the product quality.
  • [1]
    王兴伟. 基于炒制猪肉风味质构形成机制的微波加工及调控方法[D]. 无锡:江南大学, 2023. [WANG X W. Microwave processing and control methods based on the flavor and texture formation mechanism of stir-fried pork[D]. Wuxi:Jiangnan University, 2023.]

    WANG X W. Microwave processing and control methods based on the flavor and texture formation mechanism of stir-fried pork[D]. Wuxi: Jiangnan University, 2023.
    [2]
    张春江, 张良, 黄峰, 等. 中式肉类菜肴加工中营养品质变化研究进展[J]. 生物产业技术,2017(4):76−81. [ZHANG C J, ZHANG L, HUANG F, et al. Progress of nutrition changes of Chinese meat cuisines during processing[J]. Biotechnology & Business,2017(4):76−81.]

    ZHANG C J, ZHANG L, HUANG F, et al. Progress of nutrition changes of Chinese meat cuisines during processing[J]. Biotechnology & Business, 2017(4): 76−81.
    [3]
    BAI S, LUO Y R, SHEN R M, et al. Formation of flavor volatile compounds at different processing stages of household stir-frying mutton sao zi in the northwest of China[J]. LWT-Food Science & Technology,2021,139(1):110735.
    [4]
    柏霜, 尤丽琴, 罗瑞明, 等. 中式烤制滩羊肉香气活性物质分析[J]. 中国食品学报,2023,23(5):311−321. [BAI S, YOU L Q, LUO R M, et al. Analysis of aroma active compounds in chinese stir-fried tan mutton[J]. Journal of Chinese Institute of Food Science and Technology,2023,23(5):311−321.]

    BAI S, YOU L Q, LUO R M, et al. Analysis of aroma active compounds in chinese stir-fried tan mutton[J]. Journal of Chinese Institute of Food Science and Technology, 2023, 23(5): 311−321.
    [5]
    胡磊, 谢庆超, 潘迎捷, 等. 蒸制和煮制对中华绒螯蟹中胆固醇和脂肪酸含量的影响[J]. 上海海洋大学学报,2023,32(3):649−659. [HU L, XIE Q C, PAN Y J, et al. Effect of steaming and boiling on the cholesterol and fatty acid content in Chinese mitten crab (Eriocheir sinensis)[J]. Journal of Shanghai Ocean University,2023,32(3):649−659.] doi: 10.12024/jsou.20220303744

    HU L, XIE Q C, PAN Y J, et al. Effect of steaming and boiling on the cholesterol and fatty acid content in Chinese mitten crab (Eriocheir sinensis)[J]. Journal of Shanghai Ocean University, 2023, 32(3): 649−659. doi: 10.12024/jsou.20220303744
    [6]
    CHEN Y, LI P, LIAO L Y, et al. Characteristic fingerprints and volatile flavor compound variations in Liuyang Douchi during fermentation via HS-GC-IMS and HS-SPME-GC-MS[J]. Food Chemistry,2021,361:130055. doi: 10.1016/j.foodchem.2021.130055
    [7]
    姜鹏飞, 柳杨, 张浩, 等. 气相色谱-离子迁移谱在水产领域的应用[J]. 中国食品学报,2023,23(6):431−440. [JIANG P F, LIU Y, ZHANG H, et al. Application of gas chromatography-lon mobility spectrometry in aquaculture[J]. Journal of Chinese Institute of Food Science and Technology,2023,23(6):431−440.]

    JIANG P F, LIU Y, ZHANG H, et al. Application of gas chromatography-lon mobility spectrometry in aquaculture[J]. Journal of Chinese Institute of Food Science and Technology, 2023, 23(6): 431−440.
    [8]
    许丹, 朱剑, 陈瑜, 等. 智能感官分析技术结合传统感官评价对细点圆趾蟹蟹肉制品品质特性研究[J]. 浙江大学学报(理学版),2022,49(3):336−343. [XU D, ZHU J, CHEN Y, et al. Study on quality characteristics of crab meat products of Ovalipes punctatus by intelligent sensory analysis combined with traditional sensory evaluation[J]. Journal of Zhejiang University (Science Edition),2022,49(3):336−343.]

    XU D, ZHU J, CHEN Y, et al. Study on quality characteristics of crab meat products of Ovalipes punctatus by intelligent sensory analysis combined with traditional sensory evaluation[J]. Journal of Zhejiang University (Science Edition), 2022, 49(3): 336−343.
    [9]
    董萍. 智能感官技术在中餐烹饪中的应用[J]. 肉类工业,2022(3):39−43. [DONG P. Application of intelligent sensory technology in Chinese cuisine[J]. Meat Industry,2022(3):39−43.] doi: 10.3969/j.issn.1008-5467.2022.03.007

    DONG P. Application of intelligent sensory technology in Chinese cuisine[J]. Meat Industry, 2022(3): 39−43. doi: 10.3969/j.issn.1008-5467.2022.03.007
    [10]
    姜燕, 郭海南, 于润美, 等. 智能感官技术在大米及米酒感官品质分析中的应用[J]. 食品研究与开发,2018,39(18):32−37. [JIANG Y, GUO H N, YU R M, et al. Application of intelligent sensory instruments in sensory quality analysis of rice and rice wine[J]. Food Research and Development,2018,39(18):32−37.] doi: 10.3969/j.issn.1005-6521.2018.18.006

    JIANG Y, GUO H N, YU R M, et al. Application of intelligent sensory instruments in sensory quality analysis of rice and rice wine[J]. Food Research and Development, 2018, 39(18): 32−37. doi: 10.3969/j.issn.1005-6521.2018.18.006
    [11]
    范思华. 沙蟹汁中氨基酸和小分子肽对其鲜味影响的研究[D]. 南宁:广西大学, 2019:12-25. [FAN S H. Effects of amino acids and oligopeptides on the umami of soldier crab sauce[D]. Nanning:Guangxi University, 2019:12-25.]

    FAN S H. Effects of amino acids and oligopeptides on the umami of soldier crab sauce[D]. Nanning: Guangxi University, 2019: 12-25.
    [12]
    陈丽兰, 陈祖明, 袁灿. 气相色谱-离子迁移谱结合化学计量法分析不同烤制时间对郫县豆瓣酱挥发性化合物的影响[J]. 食品科学,2023,44(14):283−290. [CHEN L L, CHEN Z M, YUAN C. Effect of cooking time on volatile compounds of pixian bean paste determined by gas chromatography-lon mobility spectrometry combined with chemometrics[J]. Food Science,2023,44(14):283−290.] doi: 10.7506/spkx1002-6630-20221103-025

    CHEN L L, CHEN Z M, YUAN C. Effect of cooking time on volatile compounds of pixian bean paste determined by gas chromatography-lon mobility spectrometry combined with chemometrics[J]. Food Science, 2023, 44(14): 283−290. doi: 10.7506/spkx1002-6630-20221103-025
    [13]
    徐永霞, 白旭婷, 冯媛, 等. 基于GC-IMS和化学计量学分析海鲈鱼肉蒸制过程中风味物质的变化[J]. 食品科学,2021,42(22):270−275. [XU Y X, BAI X T, FENG Y, et al. Changes of flavor compounds in sea bass during steaming process as analyzed by gas chromatographylon mobility spectroscopy and chemometrics[J]. Food Science,2021,42(22):270−275.]

    XU Y X, BAI X T, FENG Y, et al. Changes of flavor compounds in sea bass during steaming process as analyzed by gas chromatographylon mobility spectroscopy and chemometrics[J]. Food Science, 2021, 42(22): 270−275.
    [14]
    刘胜男, 刘云锋, 曹荣, 等. 加工方式对玉筋鱼干风味的影响[J]. 食品科学,2021,42(20):167−172. [LIU S N, LIU Y F, CAO R, et al. Effects of processing methods on the flavor of dried ammodvtes personatus[J]. Food Science,2021,42(20):167−172.]

    LIU S N, LIU Y F, CAO R, et al. Effects of processing methods on the flavor of dried ammodvtes personatus[J]. Food Science, 2021, 42(20): 167−172.
    [15]
    陈瑜, 马剑锋, 许丹, 等. 基于两步水解法制备三疣梭子蟹调味品的酶解工艺优化研究[J]. 浙江大学学报(农业与生命科学版),2022,48(3):321−335. [CHEN Y, MA J F, XU D, et al. Optimization of enzymolysis technology for preparing Portunus trituberculatus seasoning based on a two-step hydrolysis method[J]. Journal of Zhejiang University (Agriculture and Life Sciences),2022,48(3):321−335.]

    CHEN Y, MA J F, XU D, et al. Optimization of enzymolysis technology for preparing Portunus trituberculatus seasoning based on a two-step hydrolysis method[J]. Journal of Zhejiang University (Agriculture and Life Sciences), 2022, 48(3): 321−335.
    [16]
    许丹, 朱剑, 严忠雍, 等. 加工方式对金枪鱼鱼糜制品氨基酸组成和营养价值影响研究[J]. 中国调味品,2020,45(11):74−80. [XU D, ZHU J, YAN Z Y, et al. Amino acid composition and nutritional value of tuna surimi products prepared by different processing methods[J]. China Condiment,2020,45(11):74−80.]

    XU D, ZHU J, YAN Z Y, et al. Amino acid composition and nutritional value of tuna surimi products prepared by different processing methods[J]. China Condiment, 2020, 45(11): 74−80.
    [17]
    刘梦, 张顺亮, 臧明伍, 等. 基于非靶向代谢组学分析牛肉干法成熟过程代谢产物的变化[J]. 食品科学,2023,44(10):249−256. [LIU M, ZHANG S L , ZANG M W, et al. Non-targeted metabolomics analysis of metabolite changes in beef during dry aging[J]. Food Science,2023,44(10):249−256.]

    LIU M, ZHANG S L , ZANG M W, et al. Non-targeted metabolomics analysis of metabolite changes in beef during dry aging[J]. Food Science, 2023, 44(10): 249−256.
    [18]
    杨昭, 梁瑞进, 姚玉静, 等. 烤制温度对酱油游离氨基酸变化规律的影响[J]. 中国调味品,2020,45(5):142−146. [YANG Z, LIANG R J, YAO Y J, et al. Effect of frying temperature on the change rule of free amino acids in soy sauce[J]. China Condiment,2020,45(5):142−146.]

    YANG Z, LIANG R J, YAO Y J, et al. Effect of frying temperature on the change rule of free amino acids in soy sauce[J]. China Condiment, 2020, 45(5): 142−146.
    [19]
    RYU S, PARK M R, MABURUTSE B E, et al. Diversity and characteristics of meat microbiological community on dry aged beef[J]. Journal of Microbiology & Biotechnology,2018,28(1):105−108.
    [20]
    帕尔哈提·柔孜, 则拉莱·司玛依, 刘源, 等. 3种甘草种子蛋白游离氨基酸组成及呈味特性的对比分析[J]. 食品研究与开发 2023, 44(8):53-60, 218. [PAERHATI·R M, ZE LA LAI·S M Y, LIU Y, et al. Comparative analysis of free amino acid composition in proteins of seeds of three glycyrrhiza species and the flavor characteristics[J]. Research and Development, 2023, 44(8):53-60, 218.]

    PAERHATI·R M, ZE LA LAI·S M Y, LIU Y, et al. Comparative analysis of free amino acid composition in proteins of seeds of three glycyrrhiza species and the flavor characteristics[J]. Research and Development, 2023, 44(8): 53-60, 218.
    [21]
    JIN Y Z, XU M H, JIN Y S, et al. Simultaneous detection and analysis of free amino acids and glutathione in different shrimp[J]. Foods,2022,11:2599.
    [22]
    沙小梅, 蒋文丽, 李鑫, 等. 不同烹饪方式小龙虾的风味特征分析[J]. 食品与发酵工业,2023,49(13):288−296. [SHA X M, JIANG W L, LI, X, et al. Analysis of flavor characteristics of Procambarus clarkia in different cooking methods[J]. Food and Fermentation Industries,2023,49(13):288−296.]

    SHA X M, JIANG W L, LI, X, et al. Analysis of flavor characteristics of Procambarus clarkia in different cooking methods[J]. Food and Fermentation Industries, 2023, 49(13): 288−296.
    [23]
    YU Z L, JIANG H R, GUO R C, et al. Taste, umami-enhance effect and amino acid sequence of peptides separated from silkworm pupa hydrolysate[J]. Food Research International,2018,108:144−150. doi: 10.1016/j.foodres.2018.02.047
    [24]
    WANG H L, ZHANG J J, ZHU Y Z, et al. Volatile components present in different parts of grass carp[J]. Journal of Food Biochemistry,2018,42:e12668. doi: 10.1111/jfbc.12668
    [25]
    冯敏, 汪敏, 常国斌, 等. 电子鼻检测辐照肉鸭产品的挥发性风味物质[J]. 核农学报,2019,30(6):1116−1121. [FENG M, WANG M, CHANG G B, et al. The detection of volatile flavor substances of irradiated duck products by electronic nose[J]. Nuclear Agricultural Sciences,2019,30(6):1116−1121.]

    FENG M, WANG M, CHANG G B, et al. The detection of volatile flavor substances of irradiated duck products by electronic nose[J]. Nuclear Agricultural Sciences, 2019, 30(6): 1116−1121.
    [26]
    王玲, 吴盈萍, 李海英, 等. 28日龄塔里木鸽与白卡奴鸽体重和体尺的聚类与主成分分析[J]. 饲料研究,2023,46(16):55−60. [WANG L, WU Y P, LI H Y, et al. Clustering and principal component analysis of weight and body size for 28-day-old Tarim pigeon and white Carnean pigeon[J]. Feed Research,2023,46(16):55−60.]

    WANG L, WU Y P, LI H Y, et al. Clustering and principal component analysis of weight and body size for 28-day-old Tarim pigeon and white Carnean pigeon[J]. Feed Research, 2023, 46(16): 55−60.
    [27]
    LI X F, ZHU J C, LI C, et al. Evolution of volatile compounds and spoilage bacteria in smoked bacon during refrigeration using an e-nose and gc-ms combined with partial least squares regression[J]. Molecules,2018,23:3286. doi: 10.3390/molecules23123286
    [28]
    胡燕燕. 羊肉电烤制工艺研究及其特征风味物质解析[D]. 石河子:石河子大学, 2023:45-47. [HU Y Y. Research on electric roasting process of mutton and its research analysis of characteristic flavor substances [D]. Shihezi:Shihezi University, 2023:45-47.]

    HU Y Y. Research on electric roasting process of mutton and its research analysis of characteristic flavor substances [D]. Shihezi: Shihezi University, 2023: 45-47.
    [29]
    LIU H, HUI T, FANG F, et al. The formation of key aroma compounds in roasted mutton during the traditional charcoal process[J]. Meat Science,2022,184:108689.
    [30]
    马勇, 魏从娇, 王雍雍, 等. 发酵香肠中3-甲基丁醛产生途径的研究进展[J]. 食品与发酵工业,2023,49(9):324−333. [MA Y, WEI C J, WANG Y Y, et al. Research progress on the production pathway of 3-methylbutanal in fermented sausage[J]. Food and Fermentation Industries,2023,49(9):324−333.]

    MA Y, WEI C J, WANG Y Y, et al. Research progress on the production pathway of 3-methylbutanal in fermented sausage[J]. Food and Fermentation Industries, 2023, 49(9): 324−333.
    [31]
    SMIT B A, ENGELS W J M, SMIT G. Branched chain aldehydes:Production and breakdown pathways and relevance for flavour in foods[J]. Applied Microbiology and Biotechnology,2009,81(6):987−999. doi: 10.1007/s00253-008-1758-x
    [32]
    陈丽兰, 陈祖明, 袁灿. 郫县豆瓣烤制后挥发性风味物质的分析[J]. 中国调味品,2020,45(4):177−180. [CHEN L L, CHEN Z M, YUAN C. Analysis of volatile flavor components of fried pixian soybean paste[J]. China Condiment,2020,45(4):177−180.]

    CHEN L L, CHEN Z M, YUAN C. Analysis of volatile flavor components of fried pixian soybean paste[J]. China Condiment, 2020, 45(4): 177−180.
    [33]
    余远江, 庞一扬, 袁桃静, 等. 基于电子鼻、HS-GC-IMS和HS-SPME-GC-MS分析五种水产原料的风味特征[J]. 食品工业科技,2021,42(19):106−117. [YU Y J, PANG Y Y, YUAN T J, et al. Analysis of flavor characteristics of five aquatic raw materials based on electronic nose, HS-GC-IMS and HS-SPME-GC-MS[J]. Science and Technology of Food Industry,2021,42(19):106−117.]

    YU Y J, PANG Y Y, YUAN T J, et al. Analysis of flavor characteristics of five aquatic raw materials based on electronic nose, HS-GC-IMS and HS-SPME-GC-MS[J]. Science and Technology of Food Industry, 2021, 42(19): 106−117.
    [34]
    刘薇, 陈敏, 徐雅倩, 等. 烤制时间对中式烤五花肉挥发性风味物质的影响[J]. 中国调味品,2021,46(10):54−58. [LIU W, CHEN M, XU Y Q, et al. Effect of roasting time on the volatile flavor compounds of Chinese roasted pork belly[J]. China Condiment,2021,46(10):54−58.]

    LIU W, CHEN M, XU Y Q, et al. Effect of roasting time on the volatile flavor compounds of Chinese roasted pork belly[J]. China Condiment, 2021, 46(10): 54−58.
    [35]
    陈臣, 田同辉, 刘政, 等. 基于感官评价、GC-IMS和GC-MS的中式酸凝奶酪挥发性风味比较[J]. 食品科学,2023,44(16):228−236. [CHEN C, TIAN T H, LIU Z, et al. Comparative study on volatile flavor of chinese acid-curd cheese using sensory evaluation, gaschromatography-lon mobility spectrometry and gas chromatography-mass spectrometry[J]. Food Science,2023,44(16):228−236.]

    CHEN C, TIAN T H, LIU Z, et al. Comparative study on volatile flavor of chinese acid-curd cheese using sensory evaluation, gaschromatography-lon mobility spectrometry and gas chromatography-mass spectrometry[J]. Food Science, 2023, 44(16): 228−236.
    [36]
    谭馨怡, 卢云浩, 任尧, 等. 不同陈酿时间下郫县豆瓣挥发性风味化合物及标志性风味成分解析[J]. 中国调味品,2021,46(10):43−46. [TAN X Y, LU Y H, REN Y, et al. Analysis of volatile flavor compounds and characteristic flavor components of Pixian bean paste at various aging time[J]. China Condiment,2021,46(10):43−46.] doi: 10.3969/j.issn.1000-9973.2021.10.008

    TAN X Y, LU Y H, REN Y, et al. Analysis of volatile flavor compounds and characteristic flavor components of Pixian bean paste at various aging time[J]. China Condiment, 2021, 46(10): 43−46. doi: 10.3969/j.issn.1000-9973.2021.10.008
    [37]
    金文刚, 刘俊霞, 赵萍, 等. 基于顶空气相色谐-离子迁移谐分析洋县不同色泽糙米蒸煮后挥发性风味物质差异[J]. 食品科学,2022,43(18):258−264. [JIN W G, LIU J X, ZHAO P, et al. Analysis of the differences in volatile flavorsubstances in Yangxian brown rice of diferent colors ater cooking based on headspace gas chromatography-ionmobility spectrometry[J]. Food Science,2022,43(18):258−264.]

    JIN W G, LIU J X, ZHAO P, et al. Analysis of the differences in volatile flavorsubstances in Yangxian brown rice of diferent colors ater cooking based on headspace gas chromatography-ionmobility spectrometry[J]. Food Science, 2022, 43(18): 258−264.

Catalog

    Article Metrics

    Article views (12) PDF downloads (3) Cited by()

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return