SHI Yuqiang, WAN Huasong, MA Jun, et al. Effects of Microwave Treatment Time on the Quality of Soybean High-temperature Defatted Soybean Meal[J]. Science and Technology of Food Industry, 2022, 43(21): 52−59. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021120143.
Citation: SHI Yuqiang, WAN Huasong, MA Jun, et al. Effects of Microwave Treatment Time on the Quality of Soybean High-temperature Defatted Soybean Meal[J]. Science and Technology of Food Industry, 2022, 43(21): 52−59. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021120143.

Effects of Microwave Treatment Time on the Quality of Soybean High-temperature Defatted Soybean Meal

More Information
  • Received Date: December 13, 2021
  • Available Online: August 29, 2022
  • In order to improve the quality of high-temperature defatted soybean meal, which is the raw material for producing soybean protein powder, and improve the stability and reliability of process control. Under the condition of microwave power of 20 kW, wind speed of 2.5 m/s, and material thickness of 20 mm, the effects of microwave treatment for 4 to 6 min on the moisture content, temperature, total number of colonies, color after water-dissolving and the secondary structure of soybean protein in high-temperature defatted soybean meal were analyzed. It could be used to guide the production and application of high temperature defatted soybean meal for soybean protein powder production. The results showed that: When the microwave treatment time was between 4 and 6 min, the water content decreased at a rate of 1.51%/min; when the microwave treatment time was 5.45 min, the temperature could be controlled at 103 ℃, the killing rate of microorganisms reached 96.8%, and the total number of colonies reached 100 CFU/g; when the microwave treatment time was between 4.62 and 5.45 min, the red value of the aqueous solution were relatively stable, the brightness and yellow value changed slightly, and the color was good; when the microwave time was ≥5 min, the urease activity was negative, which met the requirements of food for infants and children; microwave treatment had a significant effect on the secondary structure of the protein. When the microwave time was between 4.29 and 5.45 min, the α-helix transformed to the β-turn and then disappeared, and the amount of the β-turn increased rapidly; when the microwave time was between 5.45 and 6 min, the β-turn was rapidly transformed to the α-helix; the β-sheet changed only in small amplitudes and was relatively stable during the entire microwave treatment process. Microwave treatment can effectively control the moisture, color, total number of colonies, urease activity of high-temperature defatted soybean meal, and improve the secondary structure of soybean protein, which is of positive significance for improving the quality of high-temperature defatted soybean meal and expanding the application field.
  • [1]
    刘新旗, 涂丛慧, 张连慧, 等. 大豆蛋白的营养保健功能研究现状[J]. 食品科学技术学报,2012,30(2):1−6. [LIU X Q, TU C H, ZHANG L H, et al. Research on nutrition and health benefits of soy protein[J]. Journal of Beijing Technology and Business University (Natural Science Edition),2012,30(2):1−6. doi: 10.3969/j.issn.1671-1513.2012.02.001
    [2]
    时玉强, 何东平, 刘军, 等. 谷氨酰胺转氨酶对大豆分离蛋白生产的影响[J]. 中国油脂,2018,43(4):25−27. [SHI Y Q, HE D G, LIU J, et al. Effect of glutamine transaminase on production of soybean protein isolate[J]. China Oils and Fats,2018,43(4):25−27. doi: 10.3969/j.issn.1003-7969.2018.04.006
    [3]
    时玉强, 马军, 崔玉涛. 不同pH及时间对大豆乳清蛋白溶液色值的影响[J]. 中国油脂,2020,45(9):50−53. [SHI Y Q, MA J, CUI Y T. Effect of different pH and time on color value of soybean whey protein solution[J]. China Oils and Fats,2020,45(9):50−53.
    [4]
    付婷婷, 覃小丽, 刘雄. 食品的微波加工研究新进展[J]. 中国粮油学报,2020,35(4):187−194. [FU T T, TAN X L, LIU X. New progress in microwave processing of food[J]. Journal of the Chinese Cereals and Oils Association,2020,35(4):187−194. doi: 10.3969/j.issn.1003-0174.2020.04.029
    [5]
    FU Y, FENG K L, WEI S Y, et al. Comparison of structural characteristics and bioactivities of polysaccharides from loquat leaves prepared by different drying techniques[J]. International Journal of Biological Macromolecules,2019:145.
    [6]
    MARSZAłEK K, MARTA M, SKAPSKA S, et al. Effect of continuous flow microwave and conventional heating on the bioactive compounds, colour, enzymes activity, microbial and sensory quality of strawberry purée[J]. Food & Bioprocess Technology,2015,8(9):1864−1876.
    [7]
    吕豪, 吕黄珍, 杨炳南, 等. 苦瓜微波-热风振动床干燥湿热特性与表观形态研究[J]. 农业机械学报,2020,51(4):373−381. [LÜ H, LÜ H Z, YANG B N, et al. Moisture and heat characteristics and apparent form of balsam pears in microwave-hot airflow vibrating bed drying[J]. Transactions of the Chinese Society for Agricultural Machinery,2020,51(4):373−381. doi: 10.6041/j.issn.1000-1298.2020.04.043
    [8]
    杜婕妤, 管娟, 汤海青, 等. 微波加热结合真空冷水浸泡对海参水发效果的影响[J]. 农业工程学报,2020,36(17):272−280. [DU J Y, GUAN J, TANG H Q, et al. Influnce of microwave heating combined with vacuum cold water immersion on sea cucumber (Stichopus japonicus) soaking effects[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE),2020,36(17):272−280. doi: 10.11975/j.issn.1002-6819.2020.17.032
    [9]
    ALIBAS I, ZIA M P, YILMAZ A, et al. Drying kinetics and quality characteristics of green apple peel (Mallus communis L. var. "Granny Smith") used in herbal tea production[J]. Journal of Food Processing and Preservation,2020,44(2):e14332.
    [10]
    龚楚婷, 张杭进, 岳进, 等. 新型果蔬漂烫技术研究进展[J]. 食品工业科技,2018,39(22):341−345, 352. [GONG C T, ZHANG H J, YUE J, et al. Research progress of new blanching technology for fruits and vegetables[J]. Science and Technology of Food Industry,2018,39(22):341−345, 352. doi: 10.13386/j.issn1002-0306.2018.22.059
    [11]
    张少颖, 王向东, 于有伟, 等. 微波预处理原料对苹果汁褐变的影响[J]. 农业工程学报,2010,26(5):347−351. [ZHANG S Y, WANG X D, YU Y W, et al. Effects of microwave treatment of raw apple on browning of apple juice[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE),2010,26(5):347−351.
    [12]
    张婷婷, 蒲云峰, 侯福荣, 等. 微波预处理对苹果汁褐变及品质的影响[J]. 中国食品学报,2020,20(5):166−173. [ZHANG T T, PU Y F, HOU F R, et al. Effect of microwave pretreatment on browning and quality of apple juice[J]. Journal of Chinese Institute of Food Science and Technology,2020,20(5):166−173. doi: 10.16429/j.1009-7848.2020.05.021
    [13]
    齐宝坤, 赵城彬, 李杨, 等. 热处理对大豆11S球蛋白溶解性和二级结构的影响[J]. 食品科学,2018,39(22):39−44. [QI B K, ZHAO C B, LI Y, et al. Effect of heat treatment on solubility and secondary structure of soybean 11S glycinin[J]. Food Science,2018,39(22):39−44. doi: 10.7506/spkx1002-6630-201822007
    [14]
    赵晋府. 食品技术原理[M]. 北京: 中国轻工业出版社, 2002: 244−248

    ZHAO J F. Principles of food technology[M]. Beijing: China Light Industry Press, 2002: 244−248.
    [15]
    WANG Z H, CHEN G. Theoretical study of fluidized-bed drying with microwave heating[J]. Industrial & Engineering Chemistry Research,2000,39(3):775−782.
    [16]
    VÁCLAV S, ANDREA N, KVĚTOSLAV N. Finite element analysis of mode stirrer impact on electric field uniformity in a microwave applicator[J]. Drying Technology,2012,30(13):1388−1396. doi: 10.1080/07373937.2012.664800
    [17]
    LI Z Y, WANG R F, KUDRA T. Uniformity issue in microwave drying[J]. Drying Technology,2011,29(6):652−660. doi: 10.1080/07373937.2010.521963
    [18]
    MURATA M. Browning and pigmentation in food through the Maillard reaction[J]. Glycoconjugate Journal,2021,38(3):283−292. doi: 10.1007/s10719-020-09943-x
    [19]
    KOUICHI N, HAYATO M, YOSHIFUMI Y, et al. Maillard reaction intermediates and related phytochemicals in black garlic determined by EPR and HPLC analyses[J]. Molecules,2020,25(19):4578. doi: 10.3390/molecules25194578
    [20]
    郑先哲, 朱广浩, 卢淑雯, 等. 通风改善发芽糙米微波连续干燥均匀性[J]. 农业工程学报,2017,33(13):280−286. [ZHENG X Z, ZHU G H, LU S W, et al. Ventilation improving drying uniformity of germinated brown rice under continuous microwave conditions[J]. Transactions of the Chinese Society of Agricultural Engineering (Transactions of the CSAE),2017,33(13):280−286. doi: 10.11975/j.issn.1002-6819.2017.13.037
    [21]
    ZENG S W, HUANG Q L, ZHAO S M. Effects of microwave irradiation dose and time on yeast ZSM-001 growth and cell membrane permeability[J]. Food Control,2014,46:360−367. doi: 10.1016/j.foodcont.2014.05.053
    [22]
    孙震, 徐世梅, 杭峰. 微波杀菌动力学及其影响因素的研究[J]. 食品科学,2007,28(11):126−130. [SUN Z, XUN S M, HANG F. Study on microwave irradiation kinetics of Staphylococcus aureus and Escherchia coli destruction and affecting factors[J]. Food Science,2007,28(11):126−130. doi: 10.3321/j.issn:1002-6630.2007.11.025
    [23]
    邱翔, 马黎. 不同热处理方法对全脂大豆脲酶活性的影响[J]. 西南民族大学学报(自然科学版),2011(1):93−97. [QIU X, MA L. Effect of different thermal heat treatment processing for full-fat soybean urease activity[J]. Journal of Southwest University for Nationalities (Natural Science Edition),2011(1):93−97.
    [24]
    刘威, 张小燕, 杨鸉, 等. 马铃薯片微波灭酶最佳工艺参数[J]. 农业机械学报,2013,44(8):213−218. [LIU W, ZHANG X Y, YANG Y, et al. Optimal technological parameters of microwave enzyme inactivation for potato slices[J]. Transactions of the Chinese Society for Agricultural Machinery,2013,44(8):213−218. doi: 10.6041/j.issn.1000-1298.2013.08.036
    [25]
    BARTH A. Infrared spectroscopy of proteins[J]. Biochimica et Biophysica Acta,2007,1767(9):1073−1101. doi: 10.1016/j.bbabio.2007.06.004
    [26]
    ZHAO X, CHEN F, XUE W, et al. FTIR spectra studies on the secondary structures of 7S and 11S globulins from soybean proteins using AOT reverse micellar extraction[J]. Food Hydrocolloids,2008,22(4):568−575. doi: 10.1016/j.foodhyd.2007.01.019
    [27]
    CARBONARO M, MASELLI P. Relationship between digestibility and secondary structure of raw and thermally treated legume proteins: A fourier transform infrared (FT-IR) spectroscopic study[J]. Amino Acids,2012,43:911−921. doi: 10.1007/s00726-011-1151-4
    [28]
    SCHMIDT V, GIACOMELLI C, SOLDI V. Thermal stability of films formed by soy protein isolate-sodium dodecyl sulfate[J]. Polymer Degradation & Stability,2005,87(1):25−31.
    [29]
    刘燕燕, 曾新安, 陈晓东. FTIR分析脉冲电场和热处理后的大豆分离蛋白结构变化[J]. 光谱学与光谱分析,2010,30(9):2340−2344. [LIU Y Y, ZENG X A, CHEN X D. Effects of pulsed electric fields and heat treatments on SPI structure analyzed by FTIR[J]. Spectroscopy and Spectral Analysis,2010,30(9):2340−2344. doi: 10.3964/j.issn.1000-0593(2010)09-2340-05
    [30]
    ELLEPOLA S W, CHOI S M, MA C Y. Conformational study of globulin from rice (Oryza sativa) seeds by Fourier-transform infrared spectroscopy[J]. International Journal of Biological Macromolecules,2005,37(1-2):12−20. doi: 10.1016/j.ijbiomac.2005.07.008
    [31]
    陶汝青, 夏宁, 滕建文. 热处理对大豆分离蛋白结构和凝胶性的影响[J]. 食品科学,2018,39(9):60−66. [TAO R Q, XIA N, TENG J W. Effect of heat treatment on the secondary structure and gel property of soybean protein isolate[J]. Food Science,2018,39(9):60−66. doi: 10.7506/spkx1002-6630-201809010
    [32]
    白明昧, 孙泽威, 龙国徽, 等. 热处理对全脂大豆蛋白质分子结构特征、溶解度和体外消化率的影响[J]. 西北农林科技大学学报(自然科学版),2016,44(11):31−38. [BAI M M, SUN Z L, LONG G H, et al. Effect of heat-treatment on molecular structure characteristics, solubility andin vitro digestibility of full-fat soybean protein[J]. Journal of Northwest A & F University (Natural Science Edition),2016,44(11):31−38. doi: 10.13207/j.cnki.jnwafu.2016.11.005
  • Cited by

    Periodical cited type(0)

    Other cited types(3)

Catalog

    Article Metrics

    Article views (239) PDF downloads (19) Cited by(3)

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return