HS-SPME-GC-MS Combined with Electronic Nose to Explore the Effects of Osmotic Dehydration Coupled with Drying Methods on the Volatile Compounds of Peach Chips

LONG Jie; WU Xinye; BI Jinfeng; YAO Minna; PANG Jie; LI Jiaxin

doi:10.13386/j.issn1002-0306.2021110341

Volume 43 Issue 18

Sep. 2022

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Science and Technology of Food Industry > 2022 > 43(18): 241-251. > DOI: 10.13386/j.issn1002-0306.2021110341

LONG Jie, WU Xinye, BI Jinfeng, et al. HS-SPME-GC-MS Combined with Electronic Nose to Explore the Effects of Osmotic Dehydration Coupled with Drying Methods on the Volatile Compounds of Peach Chips[J]. Science and Technology of Food Industry, 2022, 43(18): 241−251. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021110341.

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HS-SPME-GC-MS Combined with Electronic Nose to Explore the Effects of Osmotic Dehydration Coupled with Drying Methods on the Volatile Compounds of Peach Chips

1.
College of Food Science, Fujian Agriculture and Forestry University, Fuzhou 350002, China
2.
Institute of Food Science and Technology, Chinese Academy of Agricultural Sciences, Beijing 100193, China
3.
School of Food Science and Technology, Dalian Polytechnic University, Dalian 116034, China

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Received Date: November 28, 2021
Available Online: July 04, 2022

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Abstract

Abstract

In order to clarify the effects of different osmotic dehydration coupled with drying methods on the volatile substances of peach chips, head-space solid phase micro-extraction combined with gas chromatography mass spectrometry (HS-SPME-GC-MS) was used for the analysis of volatile components of peach chips prepared by sucrose osmotic dehydration combined with hot air drying (SH), isomalto-oligosaccharides osmotic dehydration combined with hot air drying (IH), sucrose osmotic dehydration combined with vacuum freeze drying (SF), isomalto-oligosaccharides osmotic dehydration combined with vacuum freeze drying (IF). The results showed that 61 volatile compounds were detected in the four drying methods, and the content of total volatile components in IF was the highest, which was 528.06 μg/g. Combined with the analysis of odor activity value (OAV), 13 (SH), 18 (IH), 20 (SF) and 22 (IF) key aroma components were selected respectively. Hexanal, trans-2-hexenal, nonanal, trans-2-nonenal, benzaldehyde, hexanol, trans-2-hexen-1-ol, 1-octen-3-oll, methyl benzoate and cis-3-hexenyl acetate were the key components in all drying methods. Principal component analysis of electronic nose could distinguish peach chips under different drying methods. The experiment showed that 30% isomalto-oligosaccharides osmotic dehydration combined with vacuum freeze-drying could obtain peach chips with good flavor. This study could provide a theoretical basis for the theoretical research and practical production of peach chips.

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[1]	毕金峰, 吕健, 刘璇, 等. 国内外桃加工科技与产业现状及展望[J]. 食品科学技术学报,2019,37(5):7−15. [BI J F, LÜ J, LIU X, et al. Research on techniques and industry situation and prospect for peach processing in domestic and aboard[J]. Journal of Food Science and Technology,2019,37(5):7−15. doi: 10.3969/j.issn.2095-6002.2019.05.002 BI J F, LÜ J, LIU X, et al. Research on techniques and industry situation and prospect for peach processing in domestic and aboard[J]. Journal of Food Science and Technology, 2019, 37(5): 7-15. doi: 10.3969/j.issn.2095-6002.2019.05.002
[2]	周国燕, 陈唯实, 叶秀东, 等. 猕猴桃热风干燥与冷冻干燥的实验研究[J]. 食品科学,2007(8):164−167. [ZHOU G Y, CHEN W S, YE X D, et al. Study on freeze-drying and hot-air drying kiwi-fruit slice[J]. Food Science,2007(8):164−167. doi: 10.3321/j.issn:1002-6630.2007.08.035 ZHOU G Y, CHEN W S, YE X D, et al. Study on freeze-drying and hot-air drying kiwi-fruit slice[J]. Food Science, 2007(8): 164-167. doi: 10.3321/j.issn:1002-6630.2007.08.035
[3]	汪廷彩, 苏平, 祝水兰. 真空冷冻干燥技术在食品加工中的应用及展望[J]. 粮油加工与食品机械,2002(12):31−34. [WANG T C, SU P, ZHU S L. Application and prospect of vacuum freeze drying technology in food processing[J]. Cereals and Oils Processing,2002(12):31−34. WANG T C, SU P, ZHU S L. Application and prospect of vacuum freeze drying technology in food processing[J]. Cereals and Oils Processing, 2002(12): 31-34.
[4]	张晓敏, 兰彦平, 周连第, 等. 果蔬渗透脱水技术研究进展[J]. 食品研究与开发,2012,33(9):204−207. [ZHANG X M, LAN Y P, ZHOU L D, et al. Research progress on osmotic dehydration in fruit and vegetables[J]. Food Research and Development,2012,33(9):204−207. ZHANG X M, LAN Y P, ZHOU L D, et al. Research progress on osmotic dehydration in fruit and vegetables[J]. Food Research and Development, 2012, 33(9): 204-207.
[5]	NAKNEAN P, MANEYAM R, KAM-ONSRI A. Effect of different osmotic agents on the physical, chemical and sensoryproperties of osmo-dried cantaloupe[J]. Chiang Mai Journal of Science,2012,40(3):427−439.
[6]	HU X, WANG R R, GUO J J, et al. Changes in the volatile components of candied kumquats in different processing methodologies with headspace-gas chromatography–ion mobility spectrometry[J]. Molecules,2019,24(17):3053. doi: 10.3390/molecules24173053
[7]	宋悦, 金鑫, 毕金峰, 等. 超声辅助渗透处理对热风干燥及真空冷冻干燥黄桃片品质的影响[J]. 食品科学,2020,41(15):177−185. [SONG Y, JIN X, BI J F, et al. Effect of ultrasonic-assisted osmotic dehydration on the quality characteristics of hot air dried and vacuum freeze dried yellow peach chips[J]. Food Science,2020,41(15):177−185. doi: 10.7506/spkx1002-6630-20190730-403 SONG Y, JIN X, BI J F, et al. Effect of ultrasonic-assisted osmotic dehydration on the quality characteristics of hot air dried and vacuum freeze dried yellow peach chips[J]. Food Science, 2020, 41(15): 177-185. doi: 10.7506/spkx1002-6630-20190730-403
[8]	SORNDECH W, NAKOM N, TONGTA S, et al. Isomalto-oligosaccharides: Recent insights in production technology and their use for food and medical applications[J]. LWT-Food Science and Technology,2018,95:135−142. doi: 10.1016/j.lwt.2018.04.098
[9]	YEN C H, TSENG Y H, KUO Y W, et al. Long-term supplementation of isomalto oligisaccharides improved colonic microflora profile, bowel function, and blood cholesterol levels in constipated elderly people: A placebolled, diet-controlled trial[J]. Nutrition,2011,27(4):445−450. doi: 10.1016/j.nut.2010.05.012
[10]	MELUCCI D, BENDINI A, TESINI F, et al. Rapid direct analysis to discriminate geographic origin of extra virgin olive oils by flash gas chromatography electronic nose and chemometrics[J]. Food Chemistry,2016,204:263−273. doi: 10.1016/j.foodchem.2016.02.131
[11]	PRAT L, ESPINOZA M I, AGOSIN E, et al. Identification of volatile compounds associated with the aroma of white strawberries (Fragaria chiloensis)[J]. Journal of the Science of Food and Agriculture,2014,94(4):752−759. doi: 10.1002/jsfa.6412
[12]	马尧, 郝慧慧, 张海红, 等. GC-MS结合电子鼻分析不同干燥方式对黄花菜粉挥发性物质的影响[J]. 食品科学, 2022, 43(6): 324-330. MA X, HAO H H, ZHANG H H, et al. The effects of different drying methods on volatile flavor components of daylily powder were analyzed by GC-MS combined with electronic nose[J]. Food Science, 2022, 43(6): 324-330.
[13]	SONG J X, CHEN Q Q, BI J F, et al. GC/MS coupled with MOS e-nose and flash GC e-nose for volatile characterization of Chinese jujubes as affected by different drying methods[J]. Food Chemistry,2020,331:127201. doi: 10.1016/j.foodchem.2020.127201
[14]	LÜ J, YI J, BI J, et al. Effect of sucrose concentration of osmotic dehydration pretreatment on drying characteristics and texture of peach chips dried by infrared drying coupled with explosion puffing drying[J]. Drying Technology,2017,35(15):1887−1896. doi: 10.1080/07373937.2017.1286670
[15]	UMER H, WANG D, WU G F, et al. Post-storage changes of volatile compounds in air- and sun-dried raisins with different packaging materials using HS-SPME with GC/MS[J]. Food Research International,2019,119:23−33. doi: 10.1016/j.foodres.2019.01.007
[16]	LIU Y, HE C C, SONG H L, et al. Comparison of fresh watermelon juice aroma characteristics of five varieties based on gas chromatography-olfactometry-mass spectrometry[J]. Food Research International,2018,107(MAY):119−129.
[17]	王鹏, 田洪磊, 詹萍, 等. 采用GC-MS技术分析新疆蟠桃鲜果及其果汁制品中的挥发性物质[J]. 食品与发酵工业,2016,42(11):199−205. [WANG P, TIAN H L, ZHAN P, et al. Analysis of volatile substances in Xinjiang flat peach fruits and its juice products by GC-MS[J]. Food and Fermentation Industries,2016,42(11):199−205. WANG P, TIAN H L, ZHAN P, et al. Analysis of volatile substances in Xinjiang flat peach fruits and its juice products by GC-MS[J]. Food and Fermentation Industries, 2016, 42(11): 199-205.
[18]	KARAFFA L S. The merck index: An encyclopedia of chemicals, drugs, and biologicals[M]. RSC Publishing, 2013.
[19]	AUBERT C, MILHET C. Distribution of the volatile compounds in the different parts of a white-fleshed peach (Prunus persica L. Batsch)[J]. Food Chemistry,2007,102(1):375−384. doi: 10.1016/j.foodchem.2006.05.030
[20]	REINECCIUS G. Flavor chemistry and technology[M]. CRC press, 2005.
[21]	李卓豪, 毕金峰, 易建勇, 等. 不同小分子糖渗透草莓的传质动力学及对真空冷冻干燥草莓品质的影响[J/OL]. 食品科学: 1−16[2022-08-16].http://kns.cnki.net/kcms/detail/11.2206.TS.20210911.1250.014.html LI Z H, BI J F, YI J Y, et al. Effects of osmotic dehydration with various small-molecule sugars on mass transfer kinetics of strawberries and qualities of its freezing-dried products[J/OL]. Food Science: 1−16[2022-08-16].http://kns.cnki.net/kcms/detail/11.2206.TS.20210911.1250.014.html
[22]	TIAN Y T, ZHAO Y T, HUANG J J, et al. Effects of different drying methods on the product quality and volatile compounds of whole shiitake mushrooms[J]. Food Chemistry, 2016, 197: 714−722.
[23]	SINESIO F, MONETA E, SPATARO P, et al. Determination of sensory quality of dehydrated vegetables with profiling[J]. Italian Journal of Food Science,1995,7(1):11−18.
[24]	张艳荣, 吕呈蔚, 刘通, 等. 不同干燥方式对姬松茸挥发性风味成分分析[J]. 食品科学,2016,37(10):116−121. [ZHANG Y R, LÜ C W, LIU T, et al. Effect of different drying methods on volatile flavor components in Agaricus blazei[J]. Food Science,2016,37(10):116−121. doi: 10.7506/spkx1002-6630-201610020 ZHANG Y R, LÜ C W, LIU T, et al. Effect of different drying methods on volatile flavor components in Agaricus blazei[J]. Food Science, 2016, 37(10): 116-121. doi: 10.7506/spkx1002-6630-201610020
[25]	范刚, 王可兴, 潘思轶. 水果中糖苷键合态香气物质的研究进展[J]. 中国农业科学,2010,43(24):5100−5111. [FAN G, WANG K X, PAN S Y. Advances in research of glycosidically bound aroma compounds in fruits[J]. Scientia Agricultura Sinica,2010,43(24):5100−5111. doi: 10.3864/j.issn.0578-1752.2010.24.014 FAN G, WANG K X, PAN S Y. Advances in research of glycosidically bound aroma compounds in fruits[J]. Scientia Agricultura Sinica, 2010, 43(24): 5100-5111. doi: 10.3864/j.issn.0578-1752.2010.24.014
[26]	FREEMAN G G, WHENHAM R J. The use of synthetic (±)-s-1-propyl-l-cysteine sulphoxide and of alliinase preparations in studies of flavour changes resulting from processing of onion (Allium cepa L.)[J]. Journal of the Science of Food and Agriculture,2010,26(9):1333−1346.
[27]	ZHANG B, SHEN J Y, WEI W W, et al. Expression of genes associated with aroma formation derived from the fatty acid pathway during peach fruit ripening[J]. Journal of Agricultural and Food Chemistry,2010,58:6157−6165. doi: 10.1021/jf100172e
[28]	FLINK J, KAREL M. Retention of organic volatiles in freeze-dried solutions of carbohydrates[J]. Journal of Agricultural and Food Chemistry,1970,18(2):295−297. doi: 10.1021/jf60168a014
[29]	蒋鹏飞, 王赵改, 史冠莹, 等. 不同干燥方式的苦瓜粉品质特性及香气成分比较[J]. 现代食品科技,2020,36(3):234−244. [JIANG P F, WANG Z G, SHI G Y, et al. Quality characteristics and aroma components of bitter gourd (Momordica charantia L.) powder dried by different methods[J]. Modern Food Science and Technology,2020,36(3):234−244. JIANG P F, WANG Z G, SHI G Y, et al. Quality characteristics and aroma components of bitter gourd (Momordica charantia L. ) powder dried by different methods [J]. Modern Food Science and Technology, 2020, 36(3): 234-244.
[30]	刘璇, 赖必辉, 毕金峰, 等. 不同干燥方式芒果脆片香气成分分析[J]. 食品科学,2013,34(22):179−184. [LIU X, LAI B H, BI J F, et al. Analysis of aroma components in mango chips by different drying methods[J]. Food Science,2013,34(22):179−184. LIU X, LAI B H, BI J F, et al. Analysis of aroma components in mango chips by different drying methods[J]. Food Science, 2013, 34(22): 179-184.
[31]	车夏宁, 林海龙, 赵永武, 等. 低聚异麦芽糖理化功能特性及生产方法研究进展[J]. 中国酿造,2014(7):4. [CHE X N, LIN H L, ZHAO Y W, et al. Research progress on physico chemical properties and physiological functions and production of isomalto-oligosaccharide[J]. China Brewing,2014(7):4. CHE X N, LIN H L, ZHAO Y W, et al. Research progress on physico chemical properties and physiological functions and production of isomalto-oligosaccharide[J]. China Brewing, 2014(7): 4.
[32]	CREWS C, CASTLE L. A review of the occurrence, formation and analysis of furan in heat-processed foods[J]. Trends in Food Science & Technology,2007,18(7):365−372.
[33]	杨杨, 王冰, 石彦国, 等. 酸浆豆腐后熟过程中风味物质的形成途径分析[J]. 食品科学, 2021, 42(20): 152-159. YANG Y, WANG B, WANG Y G, et al. Analysis of the formation of flavor substances in the process of ripening of fermented soybeans whey tofu[J/OL]. Food Science, 2021, 42(20): 152-159.
[34]	范霞, 崔心平. 基于HS-SPME/GC-MS和电子鼻技术研究江苏省不同肉质桃子七月份采后贮藏期的香气成分[J]. 食品科学, 2021, 42(20): 222−229 FAN X, CUI X P. Based on HS-SPME/GC-MS and electronic nose technology to study the aroma compounds of peach of different flesh types during the July postharvest storage in jiangsu province[J]. Food Science, 2021, 42(20): 222−229.
[35]	BELITZ H D, GROSCH W, SCHIEBERLE P. Food chemistry[M]. Springer Berlin Heidelberg, 2004.
[36]	席万鹏, 郁松林, 周志钦. 桃果实香气物质生物合成研究进展[J]. 园艺学报,2013,40(9):1679−1690. [XI W P, YU S L, ZHOU Z Q. Advances in aroma compounds biosynthesis of peach fruit[J]. Acta Horticulturae Sinica,2013,40(9):1679−1690. XI W P, YU S L, ZHOU Z Q. Advances in aroma compounds biosynthesis of peach fruit[J]. Acta Horticulturae Sinica, 2013, 40(9): 1679-1690.
[37]	WANG J, YUAN Z L, REN R C, et al. Comparison of volatiles of banana powder dehydrated by vacuum belt drying, freeze-drying and air-drying[J]. Food Chemistry,2007,104(4):1516−1521. doi: 10.1016/j.foodchem.2007.02.029
[38]	MUI W, DURANCE T D, SCAMAN C H. Flavor and texture of banana chips dried by combinations of hot air, vacuum, and microwave processing[J]. Journal of Agricultural and Food Chemistry,2002,50(7):1883−1889. doi: 10.1021/jf011218n
[39]	THIJSSEN H A C. Flavour retention in drying preconcentrated food liquids[J]. Journal of Applied Chemistry and Biotechnology,1971,21(12):372−377.
[40]	XU X D, XU R, JIA Q. Identification of dihydro-β-ionone as a key aroma compound in addition to C8 ketones and alcohols in Volvariella volvacea mushroom[J]. Food Chemistry, 2019, 293: 333-339.
[41]	VAN GEMERT L J. Compilations of odour threshold values in air, water and other media[M]. Oliemans Punter & Partners BV, 2003.
[42]	BALDWIN E A, BAI J, PLOTTO A, et al. Electronic noses and tongues: Applications for the food and pharmaceutical industries[J]. Sensors,2011,11(5):4744−4766. doi: 10.3390/s110504744

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