Citation: | HAO Junguang, KE Feng, LIANG Zhenrong, et al. Determination of 18 Organic Acids in Rice Flavored Liquor Fermentation Broth by High Pressure Liquid Chromatography[J]. Science and Technology of Food Industry, 2021, 42(19): 283−290. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020120143. |
[1] |
荆春海, 郭兆阳. 白酒中有机酸测定方法综述[J]. 山东轻工业学院学报,2011,25(3):30−33. [JING Chunhai, GUO Zhaoyang. Determination methods of organic acids in Chinese liquor[J]. Journal of Shandong Polytechnic University,2011,25(3):30−33.
|
[2] |
刘凡, 周新虎, 陈翔, 等. 洋河浓香型白酒发酵过程酒醅微生物群落结构解析及其与有机酸合成的相关性[J]. 微生物学报,2018,58(12):2087−2099. [LIU Fan, ZHOU Xinhu, CHEN Xiang, et al. Microbial community of fermented grains and its correlation with organic acids biosynthesis during Yanghe strong-aroma liquor manufacturing process[J]. Acta Microbiologica Sinica,2018,58(12):2087−2099.
|
[3] |
曹云刚, 马丽, 杜小威, 等. 汾酒酒醅发酵过程中有机酸的变化规律[J]. 食品科学,2011,32(7):229−232. [CAO Yungang, MA Li, DU Xiaowei, et al. Variation of organic acids in fermented grains during fermentation of Fen liquor[J]. Food Science,2011,32(7):229−232.
|
[4] |
张方, 张宿义, 苏占元, 等. 有机酸对浓香型白酒品质及其酿造过程影响的研究进展[J]. 酿酒科技,2016(1):94−97, 102. [ZHANG Fang, ZHANG Suyi, SU Zhanyuan, et al. Research progress in the effects of organic acids on the quality of Nongxiang Baijiu and its production process[J]. Liquor-making Science & Technology,2016(1):94−97, 102.
|
[5] |
孟望霓, 田志强. 酱香型白酒风味物质贮藏周期变化规律分析[J]. 酿酒科技,2015(7):21−27. [MENG Wangni, TIAN Zhiqiang. The change rules of the flavoring compounds of Jiangxiang Baijiu (liquor) during the storage period[J]. Liquor-making Science & Technology,2015(7):21−27.
|
[6] |
汪诗欣, 开朗, 杨静怡, 等. 浓香型白酒中短链脂肪酸及其乙酯对人体的影响[J]. 食品与发酵工业,2020,46(16):257−263. [WANG Shixin, KAI Lang, YANG Jingyi, et al. Research progress on health effects of short-chain fatty acids and its ethyl esters in strong aroma-type Baijiu[J]. Food and Fermentation Industries,2020,46(16):257−263.
|
[7] |
谢佳. 杂醇、酸、酯组成及氨基酸对白酒醉度的调节作用[D]. 广州: 华南理工大学, 2018.
XIE Jia. Effect of composition of fusel alcohols, acids, esters and amino acids on intoxicating degree of liqour[D]. Guangzhou: South China University of Technology, 2018.
|
[8] |
胡志平, 梁振荣, 柯锋. 米香型白酒酒曲的研究与应用[J]. 轻工科技,2015(2):9−11. [HU Zhiping, LIANG Zhenrong, KE Feng, et al. Study and application of rice flavor liquor koji[J]. Light Industry Science and Technology,2015(2):9−11.
|
[9] |
李明球, 彭松林. 低度小曲米香型白酒生产过程中几个问题的探讨[J]. 酿酒,2018,45(1):50−52. [LI Mingqiu, PENG Songlin. Discussion on several problems in the production of low alcohol-xiaoqu-rice flavor liquor[J]. Liquor Making,2018,45(1):50−52. doi: 10.3969/j.issn.1002-8110.2018.01.018
|
[10] |
胡志平, 柯锋, 叶静萱. 纯手工酒曲与机械酒曲的米香型白酒品质对比分析[J]. 酿酒科技,2019(3):90−93. [HU Zhiping, KE Feng, YE Jingxuan, et al. Comparative analysis of the quality of Mixiang Baijiu produced by handmade Jiuqu, mechanical Jiuqu[J]. Liquor-making Science & Technology,2019(3):90−93.
|
[11] |
唐取来, 刘彩霞, 肖冬光. 新型液态发酵生产米香型白酒的研究(Ⅲ)-纯种培养酿酒酵母与传统小曲协同糖化发酵的研究[J]. 酿酒科技,2016(5):35−37, 47. [TANG Qulai, LIU Caixia, XIAO Dongguang, et al. Production of Mixiang Baijiu by new-type liquid fermentation (III): cooperative sacchariferous fermentation of pure-bred cultured yeast and traditional Xiaoqu[J]. Liquor-making Science & Technology,2016(5):35−37, 47.
|
[12] |
邱修柄. 米香型白酒上头成分的形成机理及控制措施研究[D]. 广州: 仲恺农业工程学院, 2014.
QIU Xiubing. Research on formation mechanism and controlling measurement of dizzying ingredient in rice-wine[D]. Guangzhou: Zhongkai University of Agriculture and Engineering, 2014.
|
[13] |
温承坤, 陈孝, 王奕芳, 等. 米酒功能性成分研究进展[J]. 中国酿造,2019,38(12):5−8. [WEN Chengkun, CHEN Xiao, WANG Yifang, et al. Research progress on functional components of rice wine[J]. China Brewing,2019,38(12):5−8. doi: 10.11882/j.issn.0254-5071.2019.12.002
|
[14] |
范文来, 龚舒蓓, 徐岩. 白酒有机酸谱[J]. 酿酒,2019,46(1):37−42. [FAN Wenlai, GONG Shubei, XU Yan. Organic acid spectrum of Baijiu[J]. Liquor Making,2019,46(1):37−42. doi: 10.3969/j.issn.1002-8110.2019.01.013
|
[15] |
胡国栋, 程劲松, 朱叶. 白酒中游离有机酸的定量测定[J]. 色谱,1994,12(4):265−267. [HU Guodong, CHENG Jingsong, ZHU Ye, et al. Quantitative determination of freer organic acids in Chinese liquor[J]. Chinese Journal of Chromatography,1994,12(4):265−267.
|
[16] |
Ma Y H, LI M P, Zhang S W. Simultaneous determination of organic acids in Chinese liquor by GC-MS method[J]. Asian Journal of Chemistry,2014,26(14):4707−4710.
|
[17] |
杨会, 范文来, 徐岩. 基于BSTFA衍生化法白酒不挥发有机酸研究[J]. 食品与发酵工业,2017,43(5):192−197. [YANG Hui, FAN Wenlai, XU Yan. Characterization of non-volatile organic acids in Baijiu (Chinese liquors) based on BSTFA derivatization coupled with GC-MS[J]. Food and Fermentation Industries,2017,43(5):192−197.
|
[18] |
唐坤甜, 赵彩云, 韩兴林, 等. 白酒味觉成分有机酸含量分析及其对酿造工艺的影响[J]. 食品与发酵工业,2016,42(7):202−208. [TANG Kuntian, ZHAO Caiyun, HAN Xinglin, et al. Determination of organic acids in liquors using ion chromatography[J]. Food and Fermentation Industries,2016,42(7):202−208.
|
[19] |
Geng X M, Zhang S F, Wang Q, et al. Determination of organic acids in the presence of inorganic anions by ion chromatography with suppressed conductivity detection[J]. Journal of Chromatography A,2008,1192:187−190. doi: 10.1016/j.chroma.2008.03.073
|
[20] |
宋卫得, 李兆杰, 杨立明, 等. 离子色谱法快速测定白酒中多种有机酸和阴离子[J]. 中国酿造,2017,36(11):153−157. [SONG Weide, LI Zhaojie, YANG Liming, et al. Rapid determination of various organic acids and anions in Baijiu by ion chromatography[J]. China Brewing,2017,36(11):153−157.
|
[21] |
廖勤俭, 王小琴, 周韩玲, 等. 高效液相色谱-四级杆飞行时间质谱法鉴别白酒中羧酸[J]. 酿酒科技,2019(12):77−81. [LIAO Qinjian, WANG Xiaoqin, ZHOU Hanling, et al. Identification of carboxylic acid compounds in Baijiu by LC-QTOF[J]. Liquor Making,2019(12):77−81.
|
[22] |
Coelho E M, Padilha C V S, Miskinis G A, et al. Simultaneous analysis of sugars and organic acids in wine and grape juices by HPLC: Method validation and characterization of products from northeast[J]. Brazil Journal of Food Composition and Analysis, 2018, 66: 160−167.
|
[23] |
Ivanova-Petropulos V, Petruševa D, Mitrev S. Rapid and simple method for determination of target organic acids in wine using HPLC-DAD analysis[J]. Food Analytical Methods,2020(13):1078−1087.
|
[24] |
杨成聪, 沈馨, 马雪伟, 等. 高效液相色谱法测定米酒中有机酸的含量[J]. 食品研究与开发,2018,39(10):116−123. [YANG Chengcong, SHEN Xin, MA Xuewei, et al. Determination of organic acids in rice wine by high performance liquid chromatography[J]. Food Research And Development,2018,39(10):116−123. doi: 10.3969/j.issn.1005-6521.2018.10.021
|
[25] |
陈和地, 任怡琳, 耿燕, 等. 基于超高效液相色谱法快速测定短链脂肪酸方法的建立[J]. 生物加工过程,2019,17(4):365−371. [CHEN Hedi, REN Yilin, GENG Yan, et al. Determination of organic acid in rice wine by high performance liquid chromatography[J]. Chinese Journal of Bioprocess Engineering,2019,17(4):365−371. doi: 10.3969/j.issn.1672-3678.2019.04.006
|
[26] |
李咏如, 李徐, 陶胜男, 等. 反相高效液相色谱法测定Rancimat测量池水中的短链脂肪酸[J]. 中国油脂,2017,42(9):126−128. [LI Yongru, LI Xu, TAO Shengnan, et al. Analysis of short chain fatty acids by ultra-performance liquid chromatography[J]. China Oils and Fats,2017,42(9):126−128. doi: 10.3969/j.issn.1003-7969.2017.09.024
|
[27] |
张寒琦. 仪器分析[M]. 第二版. 北京: 高等教育出版社, 2013: 312.
Zhang Hanqi. Instrumentation analysis[M]. Second Edition. Beijing: Higher Education Press, 2013: 312.
|
[28] |
郝俊光, 陈婉玲, 杨丽, 等. 红茶菌发酵罗城毛葡萄13种有机酸的同时检测[J]. 食品工业科技,2020,41(22):260−266. [HAO J G, CHEN W L, YANG L. Simultaneous determination of 13 organic acids during the fermentation of luocheng Vitis quinnquangularis Rehd. by Kombucha consortium[J]. Science and Technology of Food Industry,2020,41(22):260−266.
|
[29] |
李建芳, 周枫, 王爽, 等. 野生猕猴桃酒苹果酸-乳酸发酵优良乳酸菌的筛选与耐受性研究[J]. 中国酿造,2019,38(8):56−59. [LI Jianfang, ZHOU Feng, WANG Shuang, et al. Screening and tolerance of superior lactic acid bacteria for wild kiwifruit wine malolactic fermentation[J]. China Brewing,2019,38(8):56−59. doi: 10.11882/j.issn.0254-5071.2019.08.012
|
[30] |
李玮黎. 西凤酒酒醅中乙酸菌的分离鉴定及其生理生化特性研究[D]. 咸阳: 西北农林科技大学, 2014.
LI Weili. The isolation and identification and physiological and biochemical characteristics of acetic acid bacteria in fermented grains of Feng-flavor liquor[D]. Xianyang: Northwest Agriculture & Forestry University, 2014.
|