Simultaneous Determination of 21 Bisphenol and Bisphenol Derivatives in Baijiu Contact Plastic Materials by UPLC-Q-Orbitrap High Resolution Mass Spectrometry

Song LIU; Zhenyu ZHAO; Wenwen ZENG; Ye NIE; Heyu WANG

doi:10.13386/j.issn1002-0306.2020060229

Volume 42 Issue 9

Apr. 2021

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Science and Technology of Food Industry > 2021 > 42(9): 263-269. > DOI: 10.13386/j.issn1002-0306.2020060229

LIU Song, ZHAO Zhenyu, ZENG Wenwen, et al. Simultaneous Determination of 21 Bisphenol and Bisphenol Derivatives in Baijiu Contact Plastic Materials by UPLC-Q-Orbitrap High Resolution Mass Spectrometry[J]. Science and Technology of Food Industry, 2021, 42(9): 263−269. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020060229.

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Simultaneous Determination of 21 Bisphenol and Bisphenol Derivatives in Baijiu Contact Plastic Materials by UPLC-Q-Orbitrap High Resolution Mass Spectrometry

Kweichow Moutai Co., Ltd., Renhuai 564501, China

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Received Date: June 17, 2020
Available Online: March 15, 2021

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Abstract

Abstract

A method was developed for the simultaneous determination of 21 bisphenol and bisphenol derivatives in Baijiu contact plastic materials by ultra high performance liquid chromatography- high resolution mass spectrometry. The simulation solution was diluted 10 times with methanol. The compounds were separated on a C₁₈ chromatographic column with the gradient elution of water (contain 5 mmol/L ammonium) and methanol as mobile phase. The result showed that the limits of quantification were in the range of 2.5～500.0 µg/L, and the correlation coefficients (R²) of 21 target compounds were higher than 0.9965. The average spiked recoveries were in the range of 82.3%～106.4%, and the relative standard deviations (RSD) were in the range of 0.7%～5.2%. This method was simple, rapid, sensitive, accurate, and could be used for the monitoring of 21 bisphenol and bisphenol diglycidyl ethers in Baijiu and Baijiu contact plastic materials
- bisphenol and bisphenol derivatives,
- baijiu,
- baijiu contact plastic materials,
- UPLC-Q-Orbitrap HRMS

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[1]	邱月, 李根容, 龙梅, 等. 超高效合相色谱法同时检测塑料食品接触材料中11种双酚类化合物[J]. 分析化学研究报告,2020,48(2):255−261.
[2]	曹晨, 李文斌, 宋青, 等. 采用固相萃取/高效液相色谱法测定保健食品中12种双酚类化合物的迁移量[J]. 首都公共卫生,2017,11(6):25−29.
[3]	胡向蔚, 张文德, 刘炎桥. 食品罐内涂料中双酚A环氧衍生物的迁移及其检测[J]. 食品科学,2006,27(4):264−266. doi: 10.3321/j.issn:1002-6630.2006.04.066
[4]	端正花, 朱琳, 王平, 等. 双酚A对斑马鱼不同发育阶段的毒性及机理[J]. 环境化学,2007,26(4):491−494. doi: 10.3321/j.issn:0254-6108.2007.04.018
[5]	曹国洲, 陈少鸿, 肖道清, 等. 食品罐内壁涂料中双酚–二缩水甘油醚的快速检测和迁移规律[J]. 分析化学,2014,42(3):403−408.
[6]	刘智敏, 许志刚, 何素琼, 等. 环境雌激素双酚A的样品前处理技术与分析检测研究进展[J]. 云南师范大学学报: 自然科学版,2012,32(6):58−66.
[7]	Bang D Y, Kyung M, Kim M J, et al. Human risk assessment of endocrine-disrupting chemicals derived from plastic food containers[J]. Comprehensive Reviews in Food Science & Food Safety,2012,11(5):453−470.
[8]	Commission regulation (EC) No. 1895/2005 on the restriction of use of certain epoxy derivatives in materials and articles intended to come intocontact with food[S]. 2005.
[9]	中华人民共和国国家卫生和计划生育委员会. GB 9685-2016文后参考文献著录规则[S]. 北京: 中华人民共和国国家卫生和计划生育委员会. 2016.
[10]	李亚宁, 周启星. 四溴双酚-A的代谢转化与生态毒理效应研究进展[J]. 生态学杂志,2008,27(2):263−268.
[11]	Ji K, Hong S, Kho Y, et al. Effects of bisphenol S exposure on endocrine functions and reproduction of zebra fish[J]. Environmental Science & Technology,2013,47(15):8793−8000.
[12]	韩疏影, 宋易霖, 康安, 等. 在线富集与高效液相色谱-荧光检测法联用同时检测儿童水杯中9种双酚类物质[J]. 色谱,2019,37(11):1185−1192.
[13]	冯文燕, 仝亚男, 王淞, 等. 高效液相色谱法测定热敏纸中的双酚S含量[J]. 造纸科学与技术,2018(2):76−78.
[14]	杨金泉, 贺小敏, 施敏芳, 等. 固相萃取-超高效液相色谱-串联质谱法测定饮用水中双酚A和双酚S[J]. 食品科学,2019,40(20):332−337. doi: 10.7506/spkx1002-6630-20180827-295
[15]	龚文杰, 陈晓红, 王群利. 液相色谱-串联质谱法快速测定环境水中四溴双酚A[J]. 中国卫生检验杂志,2019(5):513−516.
[16]	李志刚. 液相色谱串联质谱测定纺织品中的四溴双酚A[J]. 分析测试报,2017,36(10):1260−1264.
[17]	唐熙, 陈高群, 梁鸣, 等. 气相色谱法测定塑料奶瓶中迁移出的双酚A[J]. 福建分析测试,2010,19(4):13−17. doi: 10.3969/j.issn.1009-8143.2010.04.004
[18]	李英, 王楼明, 张琛, 等. 固相微萃取-气相色谱-质谱法测定水中双酚A[J]. 质谱学报,2005,26(1):18−18. doi: 10.3969/j.issn.1004-2997.2005.01.005
[19]	许龙, 章英, 朱立鑫, 等. 双酚A单克隆抗体的制备及酶联免疫分析方法的建立[J]. 食品科学,2015,36(20):202−206. doi: 10.7506/spkx1002-6630-201520039
[20]	肖全伟, 黎源倩, 邹晓莉. 非水毛细管电泳-化学发光法测定食品包装材料中酚类环境激素[J]. 分析化学,2009(11):60−65.
[21]	顾翔源, 张瑞, 姜峰, 等. 银纳米粒子比色传感器法测定食品及水样中双酚A[J]. 安徽农业科学,2018,46(34):185−189.
[22]	张雨佳, 凌云, 张元, 等. 食品及环境样品中双酚类物质的前处理及检测方法研究进展[J]. 色谱,2019,37(12):1268−1274.
[23]	Dang A, Sieng M, Pesek J J, et al. Determination of bisphenol a in receipts and carbon paper by HPLC-UV[J]. Journal of Liquid Chromatography & Related Technologies,2015,38(4):438−442.
[24]	Selvaraj K K, Shanmugam G, Sampath S, et al. GC-MS determination of bisphenol A and alkylphenol ethoxylates in river water from India and their ecotoxicological risk assessment[J]. Ecotoxicology & Environmental Safety,2014,99(1):13−20.
[25]	刘超. 液质联用技术测定邻苯二甲酸酯类及酚类环境激素的研究[D]. 南昌: 南昌大学, 2007: 39.
[26]	张海婧, 林少彬. 固相萃取-高效液相色谱-串联质谱测定水中8种双酚-二环氧甘油醚[J]. 色谱,2014,7(32):730−734.
[27]	张朝晖, 罗生亮, 吴少林, 等. 鱼肉类罐头中双酚-二环氧甘油醚的固相萃取/HPLC-MS/MS法检测[J]. 分析测试学报,2009,28(6):714−719. doi: 10.3969/j.issn.1004-4957.2009.06.017
[28]	凌云, 雍伟, 何佩霞, 等. 超高效液相色谱-三重四级杆串联质谱法同时测定饮料中11中磷酸酯类增塑剂含量[J]. 中国食品卫生杂志,2019,6(31):528−532.
[29]	孟明辉, 贺泽英, 徐亚平, 等. QuEChERS方法结合高效液相色谱-串联质谱法同时测定土壤中20种抗生素[J]. 农业环境科学学报,2017,36(8):1672−1679. doi: 10.11654/jaes.2017-0249

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3.	马裕清，段万里，彭蕾，耿丙杰，唐凌瑄，王浩能，高方圆. 食品包装材料中双酚A检测方法的研究进展. 上海预防医学. 2023(06): 604-612 .
4.	孙震，郭铮蕾，刘莉，万晓楠，韩深，张朝晖，杨宇. 双酚A国内外管控法规和检测方法研究进展. 中国口岸科学技术. 2022(02): 38-44 .
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7.	黄煜，李杰. 高效液相色谱法测定工业双酚A中的微量杂质. 化学试剂. 2022(08): 1213-1217 .
8.	张慧，曹慧，姜侃，肖功年，王瑾，周学军，厉小燕. 高效液相色谱-三重四极杆串联质谱法研究塑料接触材料中酚类化合物向奶油中的迁移. 食品科学. 2022(18): 339-345 .
9.	王庆亮. 白酒品质分析及质量安全控制研究进展. 酿酒科技. 2021(08): 97-101 .