Supercritical fluid extraction of total flavonoids from Zanthoxylum bungeagum maxim pericarp[J]. Science and Technology of Food Industry, 2013, (05): 188-191. DOI: 10.13386/j.issn1002-0306.2013.05.035
Citation: Supercritical fluid extraction of total flavonoids from Zanthoxylum bungeagum maxim pericarp[J]. Science and Technology of Food Industry, 2013, (05): 188-191. DOI: 10.13386/j.issn1002-0306.2013.05.035

Supercritical fluid extraction of total flavonoids from Zanthoxylum bungeagum maxim pericarp

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  • Received Date: September 09, 2012
  • The total flavonoids from Zanthoxylum bungeagum maxim pericarp was extracted by supercritical fluid extraction (SFE) , and the total flavonoid content in the extract was investigated by the sodium nitrite-aluminum nitrate method with Rutin as a standard product. The effects of pressure, temperature, dosage of chemical preparation and time on extract abilities of flavone were investigated. The optimum technology parameter was investigated by the orthogonal design:the factors influencing the yield were as follows:temperature>pressure>time>dosage of chemical preparation, as a result, the best craft conditions were extraction temperature 50℃, extraction pressure 35MPa, extraction time 150min, dosage of chemical preparation 4mL/g, and the extraction rate was 19.574%.
  • [1]
    崔俊, 李孟楼.花椒开发利用研究进展[J].林业科技开发, 2008, 22 (2) :9-14.
    [2]
    乌兰格日乐, 白海泉, 翁慧.黄酮的抗氧化活性研究进展[J].内蒙古民族大学学报:自然科学版, 2008, 23 (3) :277-280.
    [3]
    陈维枢. 超临界萃取的原理和应用[M]. 北京:化学工业出版社, 1998.
    [4]
    Stahl E, Quirin KW, Gerard D. Dense gases for ext reaction and refining[M].Heidelberg:Springer-Verlag Press, 1988.
    [5]
    付玉杰, 祖元刚, 赵春建, 等.超临界二氧化碳萃取甘草黄酮的工艺[J].应用化学, 2003, 12 (20) :1217-1219.
    [6]
    孙婷.超临界CO2法萃取银杏叶黄酮及其含量测定的研究[J].中国食品学报, 2005, 5 (3) :126-129.
    [7]
    孙凯, 崔鹏.鱼腥草挥发油超临界CO2萃取分离工艺的研究[J].安徽化工, 2012, 38 (2) :34-36.
    [8]
    李秋红, 罗莉萍, 叶文峰.超临界CO2 萃取杜仲叶总黄酮的研究[J].食品科学, 2006, 12 (27) :553-555.
    [9]
    郭新梅.正交实验设计应用要点及其DPS实施[J].农业基础科学, 2012 (3) :40-44.
    [10]
    吴亮亮, 石雪萍, 张卫明.花椒总黄酮测定方法研究[J].食品工业科技, 2010, 31 (10) :372-374.
    [11]
    宋江峰.超临界CO2萃取黄酮类化合物影响因素研究进展[J].粮食与油脂, 2008 (10) :12-14.
    [12]
    余清, 郑小严, 黄红霞, 等.超临界CO2萃取乌饭树叶总黄酮的工艺[J].福建农林大学学报:自然科学版, 2009, 38 (1) :98-102.
    [13]
    李卫民, 金箔, 冯毅凡.中药现代化与超临界流体萃取技术[M].北京:中国医药科技出版社, 2002.
    [14]
    武正才, 梁晓原, 缪菊莲, 等.超临界C02萃取灯盏花中总黄酮成分的工艺研究[J].云南中医学院学报, 2004, 27 (2) :34-36.
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