海藻酸钠-果胶复合溶液流变性质对核壳胶囊形成与质构的影响
Effect of Rheological Properties of Sodium Alginate-pectin Composite Solution on the Formation and Texture of Core-shell Capsules
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摘要: 基于海藻酸钠与果胶在钙离子体系中协同生成凝胶的原理,利用反向成球技术,通过在海藻酸钠-果胶复合溶液中加入含钙芯液,制备具有核壳结构的海藻酸钠果胶复合凝胶小球,即核壳胶囊。采用流变仪和质构分析仪分别研究海藻酸钠-果胶复合溶液和芯液的流变性质及其对核壳胶囊质构特性的影响。结果表明,随着果胶在复配体系中所占的比例上升,复合溶液的粘度逐渐下降,最佳的复配比例为海藻酸钠:果胶=7:3(w/w),复合溶液浓度为0.6%,其质构特性的最大力值为(430.1±24.4)g·cm-2,外壳的咀嚼性数值为(1054.9±23.4)g;流变分析显示,当芯液中黄原胶浓度0.4%、乳酸钙浓度1.5%时,所制备的核壳胶囊具有最优的球度(达标率100%)和良好的质构特性(最大力值为(376.3±18.2)g·cm-2,咀嚼性为(1104.0±43.3)g)。Abstract: Based on the synergistic gel formation mechanism between sodium alginate and pectin in presence of calcium ion,the sodium alginate-pectin hydrogel beads with shell-core structure,i.e. core-shell capsule,were prepared using reverse spherification technique,by adding the calcium-containing core solution into the sodium alginate-pectin complex solution. The rheological properties of both sodium alginate-pectin complex and the core solution were tested with the texture analyzer and rheometer and their effects on the texture properties of the core-shell capsules were studied. Results indicated that the viscosity of the complex solution gradually decreased gradually with the increase of the proportion of pectin in the complex system. The sodium alginate and pectin hydrogel beads prepared with sodium alginate-pectin ratio of 7:3 (w/w)and the concentration was 0.6%,showed the highest value of maximum force((430.1±24.4) g·cm-2)and chewability of the outer shell((1054.9±23.4) g).The optimized spherification(standard rate was 100%)and texture properties(the highest value of maximum force was(376.3±18.2) g·cm-2 the chewability was(1104.0±43.3) g)were obtained with xanthan gum concentration of 0.4% and the calcium lactate concentration of 1.5% in core liquid.