响应面法优化超声-微波协同辅助提取橄榄多酚工艺研究

项昭保; 刘星宇

doi:10.13386/j.issn1002-0306.2016.01.032

响应面法优化超声-微波协同辅助提取橄榄多酚工艺研究

项昭保^1,2,
刘星宇³

1. 催化与功能有机分子重庆市重点实验室
2. 重庆工商大学环境与资源学院
3. 重庆邮电大学生物信息学院

基金项目:

重庆市基础与前沿研究计划一般项目(CSTC2014jcyj A10099)；重庆工商大学科研启动项目(2015-56-07)；重庆工商大学科研基金项目(2015)；重庆邮电大学大学生科研训练项目(A2014-49)；

详细信息

作者简介:
项昭保(1977-),男,博士,教授,主要从事天然产物成分研究工作,E-mail:xiangzb@126.com。;

中图分类号: TQ28
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- 文章访问数: 225
- HTML全文浏览量: 47
- PDF下载量: 423
出版历程
- 收稿日期: 2015-01-22

Optimization of ultrasonic- microwave synergistic extraction of polyphenol from Canarium album by response surface methodology

XIANG Zhao- bao^1,2,
LIU Xing-yu³

Chongqing Key Laboratory of Catalysis & Functional Organic Molecules
College of Environmental and Resources,Chongqing Technology and Business University
College of Bio- Information,Chongqing University of Posts and Telecommunications

摘要

摘要: 目的:优化超声-微波协同提取橄榄多酚的工艺条件,为工业化生产中提取橄榄多酚提供参考。方法:在单因素实验的基础上,采用响应面法优化超声-微波协同提取橄榄多酚的提取工艺。结果:橄榄多酚最佳提取工艺为:微波功率为550 W,微波提取时间为4.4 min,超声功率为330 W,乙醇浓度为62%,此条件下的橄榄多酚实际得率为6.33%,接近于模型预测值6.35%。结论:该工艺简便、快速、得率高,为工业化应用提供了精确有效的参考标准,为广泛开发利用橄榄资源提供了良好的参考价值。
- 橄榄 /
- 多酚 /
- 超声 /
- 微波 /
- 提取 /
- 响应面法
Abstract: Objective: The technology for ultrasonic- microwave synergistic extracting polyphenols from Canarium album was optimized,which can provide certain references for actual production. Methods: On the basis of single factor experiments,the optimum conditions for the extraction of polyphenol was obtained by response surface methodology.Results: The optimum conditions of extracting polyphenol from Canarium album were as follows:microwave power 550 W,microwave extraction time 4.4 min,ultrasonic power 330 W,ethanol concentration 62%.Under these conditions,the polyphenol yield was 6.33%,which was close to the model predictive value of 6.35%.Conclusion: the optimum process was simple and rapid,which had good yield.Furthermore,this study offered not only an accurate and effective reference standard for industrial applications,but also a good reference value for widely exploitation and utilization of Canarium album resource.
- Canarium album /
- polyphenols /
- ultrasonic /
- microwave /
- extraction /
- response surface methodology

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参考文献(15)

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