Determination of residues of NVP in PVPP by high performance liquid chromatography
-
摘要: 建立了液相色谱法测定不溶性聚乙烯聚吡咯烷酮(PVPP)中N-乙烯基吡咯烷酮(NVP)残留量的检测方法。样品采用水提取,紫外检测器分析,检测波长为235nm,流动相为乙腈∶水(10∶90,V/V)。结果表明:NVP在0.0251.0μg/m L的浓度范围内具有良好的线性,线性相关系数为0.9999,方法的定量限为1.0mg/kg,回收率为96.0%103.0%,相对标准偏差为1.06%2.64%,该方法操作简便,分离效果好,回收率和精密度均能达到分析要求。Abstract: Reverse high performance liquid chromatography method was developed for the determination of NVP in PVPP. The Sample were extracted by water and analyzed by using UV detector at 235 nm. The liquid phase was acetonitrile/water(10∶90). The experimental results showed that the linear range of NVP was 0.025~1.0μg/m L,Correlative coefficient was 0.9999. The limit of quantitation was 1.0mg/kg,the average recoveries were 96.0%~103.0%,the coefficient of variation were 1.06%~2.64%. This method showed simple,good separation effect and high recoveries and precision met the demand of analysis.
-
Keywords:
- PVPP /
- NVP /
- high performance liquid chromatography
-
期刊类型引用(2)
1. 牛俊桀,史波林,钟葵,李洪亮,温烃,汪厚银,安志丛,高海燕,赵镭. 中心点剖面法:一种快速感官分析方法及其在食品中的应用研究进展. 食品科学. 2024(23): 23311-23320 . 百度学术
2. 常晓敏,赵慧敏,张悦,刘佳妮,李玄烨,李晓龙,初柏君,王翔宇,朱保庆. 桌布法结合极化投影地图法剖析葵花籽油香味特征. 食品安全质量检测学报. 2023(13): 184-192 . 百度学术
其他类型引用(1)
计量
- 文章访问数:
- HTML全文浏览量:
- PDF下载量:
- 被引次数: 3