柴达木盆地唐古特白刺果油的响应曲面优化超声-微波协同提取工艺研究

多本加; 刘瑞林; 许海燕; 张继方

doi:10.13386/j.issn1002-0306.2014.24.047

柴达木盆地唐古特白刺果油的响应曲面优化超声-微波协同提取工艺研究

1. 青海师范大学民族师范学院
2. 药用资源与天然药物化学教育部重点实验室,陕西师范大学化学化工学院
3. 陕西国际商贸学院

基金项目:

中央高校基本科研业务经费(GK201304003)；陕西师范大学大学生创新创业训练计划(201410718010)；

详细信息

作者简介:
多本加 (1975-) , 男, 硕士研究生, 副教授, 主要从事化学计量学方面的研究。;

刘瑞林 (1987-) , 男, 博士, 主要从事功能性碳基纳米材料及脂肪酸组学等领域的应用方面的研究。;

中图分类号: TQ464
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出版历程
- 收稿日期: 2014-04-08

Study on ultrasonic-microwave synergistic extraction optimized with response surface methodology of Qaidam Basin Nitraria tangutorum Bobr. oil

Department of Chemistry, Minorities Teuchers College, Qinghai Normal University
Key Laboratory of Medicinal Resource and Natural Pharmaceutical Chemistry of Ministry of Education, School of Chemistry and Chemical Engineering, Shaanxi Normal University
Shaanxi Institute of International Trade & Commerce

摘要

摘要: 研究超声-微波协同提取柴达木盆地唐古特白刺果油的工艺。以提取率为指标,通过单因素实验分别考察了提取剂种类、微波功率、超声功率、液料比和提取时间对白刺果油提取率的影响。利用Design-Expert软件设计正交实验,并用响应曲面优化法优化唐古特白刺果油的提取工艺,确定的最佳提取工艺参数为:微波功率490W,超声功率290W,液料比20∶1m L/g,提取时间8min。在此最佳条件下,唐古特白刺果油的一次提取率为5.71%±0.18%（n=3）,与理论计算值5.91%基本接近,说明回归模型能较好地预测唐古特白刺果油的提取率。实验结果表明,超声-微波协同提取唐古特白刺果油具有提取率高、速度快、操作简便等优点,另外为唐古特白刺果的进一步开发提供了参考依据。
- 超声-微波协同提取 /
- 唐古特白刺果油 /
- 响应曲面法
Abstract: To study the ultrasonic-microwave synergistic extraction technology of Qaidam Basin Nitraria tangutorum Bobr. oil. The type of extractant, microwave power, ultrasonic power, solvent to solid sample ratio and extraction time were investigated by using single factor experiment method with extraction yield of Nitraria tangutorum Bobr. oil as evaluation index. On the basis of single factor experiment, the factors showed significant effects were selected in the further orthogonal experiments designed by Design-Expert software. The best combination of extraction parameters was obtained with response surface methodology as follows:microwave power 490 W, ultrasonic power 290 W, solvent to sample ratio 20 ∶ 1m L / g and extraction time 8min. Under these best conditions, the extraction yield of Nitraria tangutorum Bobr. oil was 5.71% ±0.18% (n =3) . The results from experimental value are quite consistent with the theoretical expectation value 5.91%, thus regression model could well predict extraction yield of Nitraria tangutorum Bobr. oil. Results of the trial indicated that the ultrasonic-microwave synergistic extraction of Nitraria tangutorum Bobr. oil had many advantages such as high yield, high speed, simple operation and so on. Additionally, the results provided the scientific reference for further study of Nitraria tangutorum Bobr.
- ultrasonic-microwave synergistic extraction /
- Nitraria tangutorum Bobr.oil /
- response surface methodology

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参考文献(12)

[1]	杨仁明, 索有瑞, 王洪伦.唐古特白刺果实化学成分和功效作用研究进展[J].天然产物研究与开发, 2012, 24:985-989.
[2]	刘瑞林, 詹汉英, 陈钿, 等.响应曲面优化超声辅助提取山茱萸籽油工艺及其成分分析[J].食品科学, 2012, 33 (12) :1-7.
[3]	刘瑞林, 詹汉英, 张志琪.山茱萸籽总黄酮的响应曲面法优化微波辅助提取工艺的研究[J].食品工业科技, 2012, 33 (7) :228-231.
[4]	Liu R-L, Zhang J, Mou Z-L, et al.Microwave-assisted onestep extraction-derivatization for rapid analysis of fatty acids profile in herbal medicine by gas chromatography-mass spectrometry[J].Analyst, 2012, 137 (21) , 5135-5143.
[5]	刘瑞林, 王德金, 袁静, 等.超声-微波协同提取山茱英籽油工艺优化研究[J].中国食品添加剂, 2012 (5) :83-91.
[6]	詹汉英, 刘瑞林, 王德金, 等.微波-超声波协同一步提取衍生化-气相色谱-质谱联用快速分析中药材猫爪草中的脂肪酸[J].色谱, 2013, 31 (3) :240-248.
[7]	Liu R-L, Song S-H, Wu M, et al.Rapid analysis of fatty acid profiles in raw nuts and seeds by microwave-ultrasonic synergistic in situ extraction-derivatisation and gas chromatography-mass spectrometry[J].Food Chemistry, 2013, 141:4269-4277.
[8]	Han Z-P, Liu R-L, Cui H-Y, et al.Microwave-assisted extraction and LC/MS analysis of phenolic antioxidants in sweet apricot (Prunus armeniaca L.) kernel skins[J].Journal of Liquid Chromatography&Related Technologies, 2013, 36:2182-2195.
[9]	Zhou X-Y, Liu R-L, Ma X, et al.Polyethylene glycol as a novel solvent for extraction of crude polysaccharides from pericarpium granati[J].Carbohydrate Polymers, 2014, 101:886-889.
[10]	朱芸, 刘金荣, 赵文斌, 等.正交实验法优选白刺果油提取工艺[J].食品科技, 2005 (1) :21-22.
[11]	Liu R-L, Liu Y, Zhou X-Y, et al.Biomass-derived highly porous functional carbon fabricated by using a free-standing template for efficient removal of methylene blue[J].Bioresource Technology, 2014, 154:138-147.
[12]	Liu R-L, Ji W-J, He T, et al.Fabrication of nitrogen-doped hierarchically porous carbons through a hybrid dual-template route for CO2capture and haemoperfusion[J].Carbon, 2014, 76:84-95.