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中国精品科技期刊2020

响应曲面分析法优化香菇多糖铁(Ⅲ)配合工艺研究

任广明, 郭兴, 陈志新

任广明, 郭兴, 陈志新. 响应曲面分析法优化香菇多糖铁(Ⅲ)配合工艺研究[J]. 食品工业科技, 2014, (04): 251-255. DOI: 10.13386/j.issn1002-0306.2014.04.072
引用本文: 任广明, 郭兴, 陈志新. 响应曲面分析法优化香菇多糖铁(Ⅲ)配合工艺研究[J]. 食品工业科技, 2014, (04): 251-255. DOI: 10.13386/j.issn1002-0306.2014.04.072
REN Guang-ming, GUO Xing, CHEN Zhi-xin. Optimization of synthesis of lentinan-Iron (Ⅲ) complex by response surface methodology[J]. Science and Technology of Food Industry, 2014, (04): 251-255. DOI: 10.13386/j.issn1002-0306.2014.04.072
Citation: REN Guang-ming, GUO Xing, CHEN Zhi-xin. Optimization of synthesis of lentinan-Iron (Ⅲ) complex by response surface methodology[J]. Science and Technology of Food Industry, 2014, (04): 251-255. DOI: 10.13386/j.issn1002-0306.2014.04.072

响应曲面分析法优化香菇多糖铁(Ⅲ)配合工艺研究

基金项目: 

黑龙江省森林工业总局项目(sgzjY2011020);

详细信息
    作者简介:

    任广明 (1984-) , 女, 博士研究生, 研究方面:微生物学。;

  • 中图分类号: TS201.1

Optimization of synthesis of lentinan-Iron (Ⅲ) complex by response surface methodology

  • 摘要: 在单因素基础上,以铁结合率为评价指标,采用Box-Behnken Design设计原理,分析香菇多糖与柠檬酸三钠质量比、pH和温度对香菇多糖铁(Ⅲ)结合率的影响,建立相应的预测模型。最佳优化工艺为香菇多糖与柠檬酸三钠质量比为1.8,pH为8.0,温度为68.7℃,铁结合率为11.69%。验证结果表明,响应曲面法所优化出的配合工艺合理、有效、具有可行性。 
    Abstract: Based on the single factor tests, the effects of mass ratio between lentinan and catalyst sodium citrate, pH reaction temperature on iron combination rate of lentinan- Fe ( Ⅲ) were designed using Box-Behnken to assess the combination rate of iron (Ⅲ) . A prediction model was established. The optimal synthesis conditions were mass ratio between lentinan and catalyst sodium citrate of 1.8, pH8.0, reaction temperature of 68.70℃, iron combination rate of lentinan-Fe (Ⅲ) was 11.69%. It was generally accepted that the response surface method was scientific and optimum for the synthesis of lentinan-Iron (Ⅲ) complex.
  • [1] 丁虹.贫血和铁缺乏对易患人群的影响及控制措施[J].中国食物与营养, 2005 (5) :14-16.
    [2]

    Oates P S, Morgan E H.Defective iron uptake by the duodenum of Belgarade rats diets of different ion content[J].Am J Physiol, 1996, 65:272-275.

    [3] 王广慧, 戴明, 魏雅冬.香菇多糖的提取工艺研究[J].食品科技, 2013, 38 (1) :192-194.
    [4]

    Coem L H, Bowen L H, Speer J A.The Recharacterization of a Polysaccharide Iron Complex (Niferex) [J].J Inorg Biochem, 1995, 58:269-278.

    [5]

    Kudasheva D S, Lai J, Ulman A, et al.Structure of carbohydrate-bound polynuclear iron oxyhydroxide nanoparticles in parenteral formulations[J].J Inorg Biochem, 2004, 98 (11) :1757-1769.

    [6] 杨娟, 吴谋成, 张声华, 等.香菇蛋白多糖抗疲劳作用研究[J].营养学报, 2001, 23 (4) :350-353.
    [7] 庞春龙, 印遇龙, 阮征, 等.β-呋喃果糖苷酶法合成低聚乳果糖工艺优化[J].食品科学, 2011, 32 (4) :102-106.
    [8]

    Mohana S, Shrivastava S, Divecha J, et al.Response surface methodology for optimization of medium for decolorization of textile dye Direct Black 22 by a novel bacterial consortium[J].Bioresource Technology, 2008, 99 (3) :562-569.

    [9]

    Gangadharan D, Sivaramakrishnan S, Nampoothiri K M, et al.Response surface methodology for the optimization of alphaamylase production by Bacillus amyloliquefaciens[J].Bioresource Technology, 2008, 99 (11) :4597-4602.

    [10]

    Hameed B H, Tan I A W, Ahmad A L.Optimization of basic dye removal by oil palm fibre-based activated carbon using response surface methodology[J].J Hazard Mat, 2008, 158 (2/3) :324-332.

    [11]

    Thana P, Machmudah S, Goto M, et al.Response surface methodology to supercritical carbon dioxide extraction of astaxanthin from Haematococcus pluvialis[J].Bioresource Technology, 2008, 99 (8) :3110-3115.

    [12]

    Annadurai G, Ling L, Lee J F.Statistical optimization of medium components and growth conditions by response surface methodology to enhance phenol degradation by Pseudomonas putida[J].J Hazard Mat, 2008, 151 (1) :171-178.

    [13]

    Trupkin S, Levin L, Forchiassin F, et al.Optimization of a culture medium for ligninolytic enzyme production and synthetic dye decolorization using response surface methodology[J].Ind Microbiol Biotechnol, 2003, 30 (12) :682-690.

    [14] 卢日峰, 王欣, 郭丽, 等.两种方法纯化香菇多糖的对比研究[J].中国实验诊断学, 2008, 12 (4) :488-490.
    [15] 缪建, 杨文革, 周彬, 等.香菇多糖提取分离的研究[J].生物加工过程, 2007, 5 (3) :74-78.
    [16] 陈毓荃.生物化学实验方法和技术[M].北京:科学出版社, 2002:171-174.
    [17] 王元凤, 金征宇, 魏新林.茶多糖金属络合物的制备及清除自由基活性研究[J].天然产物研究与开发, 2009, 21:382-387.
    [18] 赵燕, 杨兴斌, 李晓晔, 等.当归多糖铁配合物的制备及其药用性能的初步研究[J].微量元素与健康研究, 2005, 22 (6) :20-22.
    [19] 李明静, 杨静, 王宁, 等.怀山药多糖铁 (Ⅲ) 的组成及性能表征[J].中国中药杂志, 2008, 33 (16) :2002-2004.
    [20]

    Shi DC, Zhang YS.Study on complex-ation between glucan and FOOH micronucleus surface[J].ABBS, 1989, 21:201-208.

    [21]

    Cheng HF, Li XF, Dongye GZ, et al.Synthesis, Property and structure of iron (Ⅲ) -exocarpiumCitri grandispolysaccharide complex[J].Chin J Pharm, 2000, 31 (9) :394-395.

    [22]

    Spiro T G, Pape L, Saltman P.The hydrolytic polymerization of ferric citrate[J].J Am Chem Soc, 1967, 89:5555-5559.

    [23] 石德成.人参多糖铁的制备及一般特性[J].东北师大学报, 1988 (3) :109-114.
    [24] 马莹, 何静, 马荣骏.三价铁离子在酸性水溶液中的行为[J].湖南有色金属, 2005, 21 (l) :36-39.
    [25] 毛跟年, 汤木红, 凌未霄, 等.甘露低聚糖铁配合物的制备工艺研究[J].食品科技, 2008, 33 (6) :134-137.
    [26] 陈作伟, 张勤, 王诗华, 等.正交实验研究当归多糖铁合成工艺[J].西南国防医药, 2003, 13 (4) :374-376.
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出版历程
  • 收稿日期:  2013-05-12

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