响应面法优化白骨壤多糖的辅助水提工艺

尹枭雄; 方旭波; 余辉; 孙海燕; 王阳光

doi:10.13386/j.issn1002-0306.2014.03.024

响应面法优化白骨壤多糖的辅助水提工艺

1. 浙江海洋学院食品与医药学院
2. 浙江省水产品加工技术研究联合重点实验室

基金项目:

浙江省自然科学基金(LY12C20006)；

详细信息

作者简介:
尹枭雄 (1989-) , 男, 硕士, 研究方向:天然产物的提取与应用。;

中图分类号: TQ461
计量
- 文章访问数: 147
- HTML全文浏览量: 27
- PDF下载量: 196
出版历程
- 收稿日期: 2013-07-10

Optimization of ultrasound-assisted extraction of polysaccharides from Avicennia marina by response surface analysis

School of Food Science and Pharmacy, ZheJiang Ocean University
Joint Key Laboratory of Zhejiang Province for the Research of Fishery Processing Technology

摘要

摘要: 对白骨壤多糖的超声提取工艺进行优化。在单因素实验的基础上,设计选取提取温度,超声时间,料液比,提取次数四个因素作为实验因素,以多糖得率为指标,利用响应面分析法,模拟得到回归方程的预估模型,最终确定白骨壤多糖的最优化提取条件为提取温度100℃,超声时间46min,料液比为1∶49,浸提次数1次,在此条件下实际得率为4.76%。
- 超声 /
- 白骨壤 /
- 多糖 /
- 响应面分析法
Abstract: In order to optimize ultrasonic extraction of polysaccharides in Avicennia marina, a mathematical regression model ( water /material ratio, extraction temperature ultrasonic time and extraction times as the factors, the yield of polysaccharides as index) for predicting extraction yield of polysaccharides was established by fitting Box-Benhnken central composite design experimental results.The optimal protocol for polysaccharides extraction from Avicennia marina was based on one time extraction for 46min at 100℃ with a ratio of water to dry material of 49∶1, the optimum extracting rate for the Avicennia marina was 4.76%.
- ultrasonic wave /
- Avicennia marina /
- polysaccharide /
- response surface methodology

HTML全文

参考文献(13)

[1]	郭子超, 杜佳泽, 郑明峰, 等.海洋与陆地的边缘生态[M].汕头:《侨中教研》, 2004.
[2]	赵亚, 郭跃伟.真红树林植物化学成分及生物活性研究概况[J].中国天然药物, 2004, 5 (2) :135-140.
[3]	Minocha P K, Tiwari K P.A triterpenoidal saponin from Acanthus ilicifolius[J].Phytochemistry, 1981, 20 (1) :135-137.
[4]	Erickson K L, Beutler J A, Cardellina J H, et al.A novel phorbol ester from Excoecaria agallocha[J].Journal of Natural Products, 1995, 58 (5) :769-972.
[5]	Anjaneyulu A S, Rao V L.Five diterpenoids (agal-lochins A-E) from the mangrove plant Excoecaria agallocha Linn[J].Phytochemistry, 2000, 55 (8) :891-901.
[6]	Box G E P, Hunter W G.Statistics for experiments:an introduction to design, data analysis and model building[M].New Nork:Wiley, 1990.
[7]	张忠堤.秋葵用湿润暴露疗法治疗烧 (烫) 伤73例报告[J].现代医药卫生, 1995, 11 (增刊1) :75-76.
[8]	任丹丹, 陈谷, 黄秋葵, 等.多糖的提取、分离及其体外结合胆酸盐能力的分析[J].食品科学, 2010, 31 (13) :110-113.
[9]	王鸿, 邓泽元, 刘蓉, 等.响应曲面法优化山蕗菜根多糖的提取工艺[J].食品科学, 2010, 30 (2) :46-50.
[10]	慕运动.响应面方法及其在食品工业中的应用[J].郑州工程学院学报, 2001, 22 (3) :91-94.
[11]	李金钟, 马海乐, 吴沿友, 等.超声波提取山药多糖的研究[J].粮油食品科技, 2005, 13 (5) :14-16.
[12]	谢建华, 谢明勇, 聂少平, 等.青钱柳多糖提取工艺的研究[J].食品科学, 2007, 28 (10) :188-191.
[13]	章银良, 李红旗, 高峻, 等.螺旋藻多糖提取新工艺的研究[J].食品与发酵工业, 1998, 25 (2) , P 15-18.

施引文献

资源附件(0)

计量

文章访问数: 147
HTML全文浏览量: 27
PDF下载量: 196
被引次数: 0

响应面法优化白骨壤多糖的辅助水提工艺

作者简介: 尹枭雄 (1989-) , 男, 硕士, 研究方向:天然产物的提取与应用。;

计量

出版历程

Optimization of ultrasound-assisted extraction of polysaccharides from Avicennia marina by response surface analysis

计量

出版历程

目录

作者简介:
尹枭雄 (1989-) , 男, 硕士, 研究方向:天然产物的提取与应用。;