Thermal desorption coupled to GC-MS for analyzing aroma components in fresh corn
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摘要: 采用热脱附-气相色谱/质谱联用技术(TD-GC/MS)首次分析了鲜食玉米的香气成分组成,并对普甜和紫糯两种鲜食玉米香气成分进行了比较。在最优实验参数:吸附温度30℃,吸附时间2h,冷阱温度-30℃下,普甜玉米和紫糯玉米共鉴定出香气成分38种,其中普甜玉米34种,紫糯玉米30种;普甜、紫糯玉米共有成分26种,相对含量之和分别为80.223%、90.783%;普甜玉米特有成分8种,相对含量之和为16.042%,紫糯玉米特有成分4种,相对含量之和为7.998%。该法分析鲜食玉米挥发性成分操作简单,浓缩富集效率高,重现性好,绿色环保,真实全面地反映了紫糯玉米和普甜玉米香气成分的构成。
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关键词:
- 鲜食玉米 /
- 香气 /
- 热脱附-气相色谱/质谱联用技术
Abstract: Thermal desorption (TD) combing with gas chromatographic and mass spectrum (GC/MS) was applied to analyze aroma components of fresh corns. It had optimized of thermal desorption parameters and compared aroma components of ordinary sweet corn and purple waxy corn. The results showed that thermal desorption's optimal parameters for analyzing aroma components of corn were 30℃ adsorption temperature, 2h adsorption time and-30℃ cold trap temperature. 38 kinds of aroma components in corn had been detected in two tested samples of ordinary sweet corn and purple waxy corn, 34 kinds of them were detected in ordinary sweet corn and 30 kinds in purple waxy corn. The relative contents of the common components in the two corns reached 80.223% and 90.783% respectively. Ordinary sweet corn had 8 species of endemic components and the relative content of 16.042%, purple waxy corn had 4 species of endemic components and the relative content of 7.998%. This method of analyzing fresh corn aroma components was simple, good repeatability, and the aroma components which measured the real aroma components of ordinary sweet corn and purple waxy corn.-
Keywords:
- fresh corn /
- aroma /
- TD-GC/MS
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[1] 宋江峰, 李大婧, 刘春泉, 等.甜糯玉米软罐头主要挥发性物质主成分分析和聚类分析[J].中国农业科学, 2010, 43 (10) :2122-2131. [2] 杨若明, 季玉田.玉米鲜食的功效和鲜食玉米的研究开发[J].北京农业科学, 1997, 15 (5) :40-42. [3] 张从宁, 王敏, 韩兴龙.夏玉米产量与穗粒结构的关系分析[J].种子, 1999 (4) :11-12. [4] 王利明, 宋同明, 陈绍江, 等.近等基因背景下有色与无色糯玉米的营养成分分析[J].作物杂志, 2002 (4) :17-20. [5] 郝玉兰, 潘金豹, 张秋芝, 等.糯玉米籽粒不同发育时期营养品质的变化[J].北京农学院学报, 2005, 20 (2) :14-18. [6] 蒋志宏, 汪国权, 徐以盛, 等.空气中总挥发性有机物热脱附-气相色谱联用测定方法的研究[J].环境与职业医学, 2006, 23 (3) :249-252. [7] 陈云霞, 游静, 陈淑莲, 等.用吹扫捕集-热脱附-气相色谱-质谱法分析生活污水中挥发性有机物[J].分析测试学报, 2000, 19 (1) :26-29. [8] 杜学伟, 王锴, 杜光尧, 等.热脱附/冷阱聚焦/气相色谱/质谱法卷烟香气分析[J].分析测试技术与仪器, 2007, 13 (1) :33-40. [9] 高群英, 高岩, 张汝民, 等.3种菊科植物香气成分的热脱附气质联用分析[J].浙江农林大学学报, 2011, 28 (2) :326-332. [10] 田怀香, 王璋.热脱附-气质联用分析金华火腿挥发性风味[J].食品与机械, 2007, 23 (3) :10-13. [11] 林翔云, 王滨, 王宝贝, 等.香料香精辞典[M].北京:化学工业出版社, 2006:401-402. [12] 康东方, 锦风, 王锡昌.顶空固相微萃取与GC-MS联用法分析米饭及其制品气味成分[J].中国粮油学报, 2007, 22 (5) :147-149. [13] Zhu H.Ester variability in apple varieties as determined by solid phase micro extraction and gas chromatography-mass spectrometry[J].Journal of Agricultural and Food Chemistry, 2004, 52:8086-8093.
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