金樱子黄酮两种提取工艺优化及比较

高品一; 金梅; 杨頔; 蒋福宇; 张文超; 张振学; 刘学贵

doi:10.13386/j.issn1002-0306.2014.01.035

金樱子黄酮两种提取工艺优化及比较

1. 沈阳化工大学制药与生物工程学院
2. 沈阳化工大学化学工程学院

基金项目:

辽宁省博士启动基金(20121072)资助项目；辽宁省教育厅基金(L201106)资助项目；

详细信息

作者简介:
高品一 (1982-) , 男, 博士, 讲师, 研究方向:天然产物活性成分研究。;

中图分类号: TQ914
计量
- 文章访问数: 139
- HTML全文浏览量: 13
- PDF下载量: 748
出版历程
- 收稿日期: 2013-06-25

Optimization of extraction technology of flavonoids from Rose Laevigata Michx.and their comparison

College of Pharmaceutical and Biological Engineering, Shenyang University of Chemical Technology
College of Chemical Engineering, Shenyang University of Chemical Technology

摘要

摘要: 以金樱子果实为研究对象,用黄酮得率作为衡量提取工艺的指标。通过单因素实验、正交实验优化传统加热提法和微波助提法提取金樱子果实中黄酮的提取工艺,并比较其工艺条件。验证实验表明,传统加热提法最佳工艺测得金樱子果实黄酮得率为7.84%,相对标准偏差(RSD)为0.89%;微波助提法最佳工艺测得金樱子果实黄酮得率为9.06%,相对标准偏差(RSD)为1.01%。运用微波技术提取金樱子果实中黄酮含量减少了提取时间,提高了效率。因此,恰当的提取条件可使金樱子果实中黄酮的得率更高。
- 金樱子 /
- 黄酮得率 /
- 微波提取 /
- 含量测定
Abstract: Taking fruit of Rose Laevigata Michx. as material, the yield of falconoid indicators as the evaluation standard, and its flavonoid extraction process with traditional extraction and microwave- assisted extraction were optimized by single factor and orthogonal experiment. Validation experiments showed that the flavonoid yield of traditional methods was 7.84% with the RSD 0.89%, and that yield of microwave-assisted methods was 9.06% with the RSD 1.01%.Microwave technique to extract flavonoids from the fruit of Rose Laevigata Michx.not only reduced extraction time but also improved experimental efficiency.Therefore, the flavonoid extraction could be improved by the appropriate conditions.
- Rose Laevigata Michx. /
- falconoid yield /
- microwave-assisted /
- content determination

HTML全文

参考文献(17)

[1]	姚晏群.海晏县农业产业化发展现状调查分析[J].青海农牧业, 2008 (2) :24.
[2]	Pin-Yi Gao, Ling-Zhi Li, Ying Peng, et al.Triterpenes from fruits of Rosa laevigata[J].Biochemical Systematics and Ecology, 2010, 38:457-459.
[3]	Na Zeng, Yang Shen, Ling-Zhi Li, et al.Anti-inflammatory Triterpenes from the Leaves of Rosa Laevigata[J].Journal of Natural Products, 2011, 74 (4) :732-738.
[4]	周志军.地市级农科院种子产业创新思路探讨[J].吉林蔬菜, 2008 (5) :17-18.
[5]	禹桂芳, 丁建江, 何宁, 等.宁夏泾源县特色林木种苗产业发展现状及对策[J].陕西农业科学, 2008 (8) :48.
[6]	Aoki T, Akashi T, Ayabe S.Flavonoids of Leguminous Plants:Structure, Biological Activity, and Biosynthesis[J].Journal of Plant Research, 2000, 113:475-488.
[7]	程秋月, 郭菁, 张成义.黄酮类化合物药理作用的研究[J].北华大学学报:自然科学版, 2011, 12 (2) :180-183.
[8]	Liu Yuetao, Lu Binan, Xu Lina, et al.The antioxidant activity and hypolipidemic activity of the total flavonoids from the fruit of Rose leavigata Michx[J].Natural science, 2010, 2 (3) :175-183.
[9]	Liu Yuetao, Lu Binan, Peng Jinyong.Hepatoprotective activity of the total flavonoids from Rosa laevigata Michx fruit in mice treated by paracetamol[J].Food Chemistry, 2011, 125 (2) :719-725.
[10]	卢俊, 陈福北, 温彩莲.超声波辅助提取金樱子中黄酮类化合物工艺研究[J].农业机械, 2011:145-148.
[11]	薛梅, 王自军, 闫豫君, 等.金樱子中总黄酮和多糖的微波提取与含量测定[J].食品工业科技, 2005, 26 (10) :134-135, 137.
[12]	中国药典委员会.中华人民共和国药典[M].北京:化学工业出版社, 2005:218.
[13]	Yan-Ling Wang, Guang-Sheng Xi, Yong-Chun Zheng, et al.Microwave-assisted extraction of flavonoids from Chinese herb Radix puerariae (Ge Gen) [J].Journal of Medicinal Plants Research, 2010, 4 (4) :304-308.
[14]	彭程程, 王青山, 赵国祥, 等.黄酮类化合物的研究进展[J].农产品加工:学刊, 2010, 208 (5) :39-43.
[15]	张春红, 许宁, 刘长江, 等.微波辅助法提取野生软枣猕猴桃茎黄酮的工艺优化[J].食品工业科技, 2011, 32 (12) :335-337.
[16]	王青豪, 方芳, 张熊禄.微波辅助提取绞股蓝黄酮工艺研究[J].食品科学, 2010, 31 (22) :150-151.
[17]	蒋雪蕾, 刘军海, 李安源.超声辅助正交实验优化提取桔皮总黄酮的工艺研究[J].广东化学, 2013, 40 (5) :53-54.

施引文献

资源附件(0)

计量

文章访问数: 139
HTML全文浏览量: 13
PDF下载量: 748
被引次数: 0

金樱子黄酮两种提取工艺优化及比较

作者简介: 高品一 (1982-) , 男, 博士, 讲师, 研究方向:天然产物活性成分研究。;

计量

出版历程

Optimization of extraction technology of flavonoids from Rose Laevigata Michx.and their comparison

计量

出版历程

目录

作者简介:
高品一 (1982-) , 男, 博士, 讲师, 研究方向:天然产物活性成分研究。;