Study on the change of aroma compounds in hops with different drying methods
-
摘要: 采用固相微萃取-气相色谱-质谱联用法(SPME-GC-MS)测定了干燥方式对啤酒花挥发性成分的影响。新鲜啤酒花中鉴定出挥发性成分41种,其中醇类9种、醛类3种、酯类7种、酮类5种、烯烃类3种、有机酸类7种、其他成分7种,烯烃类占总相对含量的58.54%。与新鲜啤酒花比较,工厂热风干燥的酒花增加了2种成分,占总峰面积的0.57%;减少了11种,占总峰面积的3.69%;常温气流酒花增加了3种成分,占总峰面积的0.53%;减少了8种,占总峰面积的1.5%,挥发性成分种类和数量均与新鲜酒花相似,表明气流干燥能减少啤酒花挥发性成分损失。Abstract: Effects of drying methods on volatile components of hops were determined by solid phase microextraction-gas chromatography-mass spectrometry (SPME-GC-MS) .There were 41 kinds of volatile companents identified in fresh hops, including nine kinds of alcohols, three kinds of aldehydes, seven kinds of esters, five kinds of ketones, three kinds of alkenes, seven kinds of organic acid, seven kinds of other ingredients, and the olefins accounted for 58.54% of the total relative content.Compared with fresh hops, there was an increase of two kinds of components in hops of factory hot air drying, accounted for 0.57% of the total peak area, and a decrease of eleven kinds, accounted for 3.69% of the total peak area, there was an increase of two kinds of components in hops of ambient air drying, accounted for 0.53% of the total peak area, and a decrease of eight kinds, accounted for 1.5% of the total peak area, the volatile constituents species and quantity were similar to that of fresh hops, and air drying could reduce the loss of hops volatile components.
-
Keywords:
- hops /
- air drying /
- hot air drying /
- volatile components /
- gas chromatography
-
[1] EYRES G T, MARRIOTT P J, DUFOUR J.Comparison of odoractive compounds in the spicy fraction of hop (Humulus lupulus L.) essential oil from four different varieties[J].J Agric Food Chem, 2007, 55 (15) :6252-6261.
[2] 陈家华, 沈礼兵.高效液相色谱法测定酒花α-酸含量[J].色谱, 1999, 17 (2) :184-186. [3] PATZAK J, NESVADBA V, K, ROFTA K, et al.Assessment of the genetic diversity of wild hops (Humulus lupulus L.) in Europe using chemical and molecular analyses[J].Biochem Syst Ecol, 2010, 38 (2) :136-145.
[4] Moir M.Hops-A Millennium Review[J].Journal of the American Society of Brewing Chemists, 2000, 56:131-146.
[5] 杨小兰, 田艳花, 师成滨, 等.啤酒花中黄腐酚的生理活性作用的研究进展[J].食品科学, 2007, 7:526-530. [6] 薛华丽, 蒲陆梅.啤酒花固相微萃-气质联用成分分析[J].中国酿造, 2011 (2) :170-172. [7] 朱恩俊.新型酒花制品在啤酒工业的应用[J].中国酿造, 2006 (10) :53-56. [8] 倪倩, 佟玲, 李文博, 等.气相色谱-质谱法测定普洱茶挥发油的化学成分[J].安徽农业科学, 2011, 39 (12) :7072-7073. [9] 陈飞龙, 刘莉.丁香普通粉及超微粉中挥发油的化学成分研究[J].时珍国医国药, 2010, 12 (12) :3056-3057. [10] 胡晓倩, 朱洋洋, 陈乐, 等.新鲜黄山贡菊叶中挥发油的提取[J].食品与发酵工业, 2011 (3) :210-214. [11] 刘国声, 周银珍, 刘胜利.啤酒花的香气成分[J].食品科学, 1987 (4) :25-27. [12] 刘玉梅.新疆野生啤酒花的分析评价[J].中国酿造, 2010 (3) :49-52. [13] 李峰, 刘玉梅.马格努门啤酒花挥发性成分的气相色谱-质谱联用分析[J].食品科学, 2012, 33 (22) :259-263.
计量
- 文章访问数: 120
- HTML全文浏览量: 9
- PDF下载量: 181