Determination of 19 Carbamate Pesticide and Metabolites Residues in Eggs by QuEChERS-UPLC-MS/MS

TAN Jianlin; PENG Zhenhua; ZHAO Xiulin; MA Xuetao; ZHANG Xueyuan; LIU Xiaolin; HU Zengbin; FENG Lei

doi:10.13386/j.issn1002-0306.2021030261

Volume 43 Issue 1

Dec. 2021

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Science and Technology of Food Industry > 2022 > 43(1): 320-325. > DOI: 10.13386/j.issn1002-0306.2021030261

TAN Jianlin, PENG Zhenhua, ZHAO Xiulin, et al. Determination of 19 Carbamate Pesticide and Metabolites Residues in Eggs by QuEChERS-UPLC-MS/MS[J]. Science and Technology of Food Industry, 2022, 43(1): 320−325. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021030261.

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Determination of 19 Carbamate Pesticide and Metabolites Residues in Eggs by QuEChERS-UPLC-MS/MS

Yunnan Institute of Product Quality Supervision & Inspection, Nationnal Agricultural and Sideline Products Quity Supervision and Inspection Center, Kunming 650223, China

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Received Date: March 21, 2021
Available Online: October 27, 2021

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Abstract

Abstract

The residues of 19 carbamate pesticides and their metabolites in eggs were determined by QuEChERS-UPLC-MS/MS. Egg samples were extracted by acetonitrile, purified by dispersion solid phase extraction, and determined by UPLC-MS/MS. The linearity of 19 carbamate pesticides and their metabolites in the range of 0.2~50 ng/mL was good (R²>0.999), and the detection limit of the method was 1.0~10 μg/kg. The recoveries were 69.3%~107.6 % and RSD was lower than 9.21% at 10, 20 and 50 μg/kg. The method is simple, rapid, efficient and accurate with high recovery, and can meet the needs of detection and confirmation of 19 carbamate pesticides and their metabolites residues in eggs.
- UPLC-MS/MS,
- dispersive solid phase extraction,
- eggs,
- carbamate pesticide,
- metabolites

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References

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