ZHOU Shuangli, RUAN Zheng, WEI Jianming, et al. Research on Flow Characteristics of Purified Frocto-oligosaccharide (P-FOS) Powder Based on the Particle Size[J]. Science and Technology of Food Industry, 2023, 44(20): 53−60. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022120018.
Citation: ZHOU Shuangli, RUAN Zheng, WEI Jianming, et al. Research on Flow Characteristics of Purified Frocto-oligosaccharide (P-FOS) Powder Based on the Particle Size[J]. Science and Technology of Food Industry, 2023, 44(20): 53−60. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022120018.

Research on Flow Characteristics of Purified Frocto-oligosaccharide (P-FOS) Powder Based on the Particle Size

More Information
  • Received Date: December 14, 2022
  • Available Online: August 10, 2023
  • The fluidity of powder has an important impact on the key production processes such as mixing, conveying and packaging. To solve the fluidity problem in the production of purified frocto-oligosaccharide (P-FOS) powder, the influence of different particle sizes and their proportions on the fluidity of P-FOS powder was investigated. The flow characteristic of P-FOS was analyzed by using the powder rheometer. Research on the mixing experiment based on the different particle sizes (180~250, 150~180, 120~150, and <120 μm). Then, the regression model was carried out using particle size as an independent variable and the powder flow index ff as an dependent variable. The results showed that there was no significant difference in the content of frocto-oligosaccharide with different particle sizes (P>0.05), but the fluidity of P-FOS dry powder with the reduction of particle size. P-FOS dry powders with different particle sizes exhibit fluidity across different regions. The flow indices of samples with particle sizes in the range of 180~250, 150~180 and 120~150 μm were 12.5, 7.7, and 6.6, respectively. Their flow features were in the zone of easy flow area. Meanwhile, the flow indices of samples with particle sizes of 109~120 and 96~109 μm were 2.9 and 3.3, respectively. Their flow characteristics were in the bonding region. The mixing ratio of particles of different particle sizes had a significant influence on fluidity. The relationship between the particle size and the flow index was consistent with the square regression model, and the R2 (adjusted) could reach to 99.43%. If the particle size distribution was known, the fluidity of the P-FOS powder could be predicted and regulated by this model, thus guaranteeing the continuity and stability of the transport and packing of the dry powder.
  • [1]
    贺苹苹. 大蒜低聚糖的制备及其益生活性的研究[D]. 泰安: 山东农业大学, 2019

    HE P P. Preparation of garlic oligosaccharides and study on their probiotic activity[D]. Taian: Shandong Agricultural University, 2019.
    [2]
    陈又铭, 李宁, 袁卫涛, 等. 低聚果糖的功能性质及其在食品中的应用[J]. 中国食品添加剂,2022(1):11−15. [CHEN Y M, LI N, YUAN W T, et al. The function properties of fructo-oligosaccharides and its application in food[J]. China Food Additives,2022(1):11−15. doi: 10.19804/j.issn1006-2513.2022.01.002

    CHEN Y M, LI N, YUAN W T, et al. The function properties of fructo-oligosaccharides and its application in food[J]. China Food Additives, 2022(1): 11-15. doi: 10.19804/j.issn1006-2513.2022.01.002
    [3]
    SUDHA M L, SOUMYA C, SARAVANAN M, et al. Influence of short chain fructo-oligosaccharide (SC-FOS) on the dough rheological, microstructural properties and, bread quality during storage[J]. Food Science and Technology,2022,1(158):1−8.
    [4]
    贺芳霞. 一种有助于提高免疫力的全营养特殊医学用途配方食品的研制[D]. 武汉: 华中农业大学, 2022

    HE F X. Development of a whole nutritional medical formula food for special medical purpose that helps to improve immunity[D]. Wuhan: Huazhong Agricultural University, 2022
    [5]
    张金, 王美华, 杨永龙, 等. 低聚果糖和低聚半乳糖的研究进展及在乳制品中的应用[J]. 中国食品添加剂,2020(10):129−134. [ZHANG J, WANG M H, YANG Y L, et al. Research progress and application in dairy products of fructo-oligosaccharide and galacto-oligosaccharide[J]. China Food Additives,2020(10):129−134.

    [ZHANG J, WANG M H, YANG Y L, et al. Research progress and application in dairy products of fructo-oligosaccharide and galacto-oligosaccharide[J]. China Food Additives, 2020(10): 129-134. ]
    [6]
    翟浩杰. 饲料中添加甘露寡糖对刺参生长性能、肠道及免疫功能的影响[D]. 大连: 大连海洋大学, 2022

    ZHAI H J. Effects of dietary mannan oligosaccharides on growth performance, intestinal and immune functions of sea cucumber[D]. Dalian: Dalian Ocean University, 2022.
    [7]
    SINGH R S, SINGH T. Hetero-modification of halloysite nanoclay to immobilize endoinulinase for the preparation of fructooligosaccharides[J]. Food Research International,2022,9(159):21−29.
    [8]
    周代营, 张欣, 聂阳, 等. 真空带式干燥与喷雾干燥的灵芝皇粉体性质对比[J]. 医药导报,2020,39(8):1125−1128. [ZHOU D Y, ZHANG X, NIE Y, et al. Quality comparison of Ganoderma lucidum powder by vacuum belt drying and spray drying[J]. Herald of Medicine,2020,39(8):1125−1128.

    ZHOU D Y, ZHANG X, NIE Y, et al. Quality comparison of Ganoderma lucidum powder by vacuum belt drying and spray drying[J]. Herald of Medicine, 2020, 39(8): 1125-1128.
    [9]
    何海兵, 常凯强, 王怀豫, 等. 威灵仙配方颗粒真空带式干燥工艺优选[J]. 今日药学,2020,30(9):612−615. [HE H B, CHANG K Q, WANG H Y, et al. Study of vacuum belt drying process on clematis recta formula granule[J]. Pharmacy Today,2020,30(9):612−615. doi: 10.12048/j.issn.1674-229X.2020.09.008

    HE H B, CHANG K Q, WANG H Y, et al. Study of vacuum belt drying process on clematis recta formula granule[J]. Pharmacy Today, 2020, 30(9): 612-615. doi: 10.12048/j.issn.1674-229X.2020.09.008
    [10]
    LUKAS H, LIVIA H, ADRIAAN S, et al. The influence of particle shape, powder flowability, and powder layer density on part density in laser powder bed fusion[J]. Metals,2021,3(11):418−428.
    [11]
    ZACHARY Y, QU M L, MICHAEL C M, et al. Effects of particle size distribution with efficient packing on powder flowability and selective laser melting process[J]. Materials,2022,3(15):705−709.
    [12]
    PABLO J, GUSTAVO V, BARBOSA C A. Food powders flowability characterization: Theory, methods, and applications[J]. Food Science Technology,2010,2(3):211−239.
    [13]
    VIVEK G, DENG T, MICHAEL B S A. A new method for assessing powder flowability based on physical properties and cohesiveness of particles using a small quantity of samples[J]. Powder Technology,2021,11(395):708−719.
    [14]
    李忠毅. 粉体料仓设计CAD系统研究[D]. 青岛: 青岛科技大学, 2022

    LI Z Y. Research on CAD system for poeder silo design[D]. Qingdao: Qingdao University of Science and Technology, 2022.
    [15]
    罗聪, 陆海峰, 郭晓镭, 等. 粉体流动性的静力学及动力学表征研究[J]. 化工新型材料,2020,48(10):186−191. [LUO C, LU H F, GUO X L, et al. Study on statics and kinetics characterization of powder flowability[J]. New Chemical Materials,2020,48(10):186−191. doi: 10.19817/j.cnki.issn1006-3536.20200805.044

    LUO C, LU H F, GUO X L, et al. Study on statics and kinetics characterization of powder flowability[J]. New Chemical Materials, 2020, 48(10): 186-191. doi: 10.19817/j.cnki.issn1006-3536.20200805.044
    [16]
    易建华, 张志婕, 朱振宝, 等. 不同粒径对黑米粉理化性质的影响[J]. 陕西科技大学学报,2021,39(1):39−44. [YI J H, ZHANG Z J, ZHU Z B, et al. Impact of different grain sizes on physicochemical properties of black rice powder[J]. Journal of Shanxi University of Science & Technology,2021,39(1):39−44. doi: 10.19481/j.cnki.issn2096-398x.2021.01.007

    YI J H, ZHANG Z J, ZHU Z B, et al. Impact of different grain sizes on physicochemical properties of black rice powder[J]. Journal Of Shanxi University Of Science & Technology, 2021, 39(1): 39-44. doi: 10.19481/j.cnki.issn2096-398x.2021.01.007
    [17]
    吴跃, 申国鑫, 杨磊, 等. 粒径对褐煤煤粉流动性影响研究[J]. 当代化工,2021,50(7):1572−1695. [WU Y, SHEN G X, YANG L, et al. Effect of particle size on the fluidity of pulverized lignite[J]. Contemporary Chemical Industry,2021,50(7):1572−1695. doi: 10.3969/j.issn.1671-0460.2021.07.014

    WU Y, SHEN G X, YANG L, et al. Effect of particle size on the fluidity of pulverized lignite[J]. Contemporary Chemical Industry, 2021, 50(7): 1572-1695. doi: 10.3969/j.issn.1671-0460.2021.07.014
    [18]
    张光耀, 林世文, 李灵利, 等. 乙醇和芦丁稳定的乳清分离蛋白-大豆油预乳化液在低脂肉丸中的应用[J]. 肉类研究,2022,36(12):28−35. [ZHANG G Y, LIN S W, LI L L, et al. Application of whey protein isolate-soybean oil pre-emulsions stabilized by ethanol and rutin in low-fat meatballs[J]. Meat Research,2022,36(12):28−35.

    ZHANG G Y, LIN S W, LI L L, et al. Application of whey protein isolate-soybean oil pre-emulsions stabilized by ethanol and rutin in low-fat meatballs[J]. Meat Research, 2022, 36(12): 28-35.
    [19]
    张正金. 超细金属铁氰化物/高氯酸铵复合粒子的制备及其性能研究[D]. 南京: 南京理工大学, 2019

    ZHANG Z J. Preparation and properties study of ultrafine metal ferricyanide/ammonium perchlorate composite particles[D]. Nanjing: Nanjing University of Science and Technology, 2019.
    [20]
    FERNANDO A S, REBELLO L F, AUGUSTO C L. Multiple optimization for extraction of ethinylestradiol, levonorgestrel, and their main impurities using mixture design[J]. Journal of Analytical Chemistry,2022,7(77):844−852.
    [21]
    REBECCA B, TALAT S. Analysis of alternative sustainable approach to concrete mixture design[J]. Journal of Sustainable Construction Materials and Technologies,2022,7(2):40−52. doi: 10.47481/jscmt.1114597
    [22]
    ADI H, LARSON I, STEWART P. Use of milling and wet sieving to produce narrow particle size distributions of lactose monohydrate in the sub-sieve range[J]. Powder Technology,2007,179(1):95−99.
    [23]
    聂波, 张国治. 不同粒径胡萝卜粉体理化性质及营养溶出研究[J]. 轻工学报,2016,31(4):69−75. [NIE B, ZHANG G Z. Study on the physicochemical properties and the nutritional content of dissolution of different particle size of carrot powder[J]. Journal of Light Industry,2016,31(4):69−75. doi: 10.3969/j.issn.2096-1553.2016.4.010

    NIE B, ZHANG G Z. Study on the physicochemical properties and the nutritional content of dissolution of different particle size of carrot powder[J]. Journal of Light Industry, 2016, 31(4): 69-75. doi: 10.3969/j.issn.2096-1553.2016.4.010
    [24]
    黄梅华, 吴儒华. 不同粒径金花茶茶花粉体物理特性研究[J]. 食品科学,2018,39(3):76−82. [HUANG M H, WU R H. Study on physical characteristics of different particle size of Camellia chrysantha (Hu) Tuyama powder[J]. Food Science,2018,39(3):76−82. doi: 10.7506/spkx1002-6630-201803012

    HUANG M H, WU R H. Study on physical characteristics of different particle size of Camellia chrysantha (Hu) Tuyama powder[J]. Food Science, 2018, 39(3): 76-82. doi: 10.7506/spkx1002-6630-201803012
    [25]
    FITZPATRICK J. Effect of powder properties and storage conditions on the flowability of milk powders with different fat contents[J]. Journal of Food Engineering,2004(64):435−444.
    [26]
    洪森辉, 陈佳媛, 符宁珍. 粉碎粒度对笋衣营养成分及特性的影响[J]. 农产品加工,2021(8):21−25. [HONG S H, CHEN J Y, FU N Z. Effects of grinding particle size on nutrient composition and characteristics of bamboo shoot coat[J]. Farm Products Processing,2021(8):21−25. doi: 10.16693/j.cnki.1671-9646(X).2021.08.006

    HONG S H, CHEN J Y, FU N Z. Effects of grinding particle size on nutrient composition and characteristics of bamboo shoot coat[J]. Farm Products Processing, 2021(8): 21-25. doi: 10.16693/j.cnki.1671-9646(X).2021.08.006
    [27]
    熊君, 王峰, 孙威, 等. 工艺参数对注射成型塑磁颗粒流动性能的影响[J]. 矿冶,2021,31(5):76−79. [XIONG J, WANG F, SUN W, et al. Influence of process parameters on the flow properties of injection molded plastic magnetic particles[J]. Mining and Metallurgy,2021,31(5):76−79.

    XIONG J, WANG F, SUN W, et al. Influence of process parameters on the flow properties of injection molded plastic magnetic particles[J]. Mining and Metallurgy, 2021, 31(5): 76-79.
    [28]
    陆红佳, 李倩楠, 张文林. 粒度大小对蓝莓皮渣表观结构及其理化特性的影响[J]. 粮食与油脂,2022,35(6):110−115. [LU H J, LI Q N, ZHANG W L. Effect of particle size on apparent structure and physicochemical characteristics of blueberry pomace[J]. Grain and Oil,2022,35(6):110−115. doi: 10.3969/j.issn.1008-9578.2022.06.024

    LU H J, LI Q N, ZHANG W L. Effect of particle size on apparent structure and physicochemical characteristics of blueberry pomace[J]. Grain and Oil, 2022, 35(6): 110-115. doi: 10.3969/j.issn.1008-9578.2022.06.024
    [29]
    MAHDI H K, ZHANG J H, ZOU Y. Effect of particle size distribution on the flowability of plasma atomized Ti-6Al-4V powders[J]. Powder Technology,2021,7(392):536−543.
    [30]
    王静. 药用微晶纤维素粒径调控及其流动性的研究[D]. 西安: 陕西科技大学, 2018

    WANG J. Study on the particle size control and fluidity of medicial microcrystalline cellulose[D]. Xi'an: Shaanxi University of Science and Technology, 2018.
    [31]
    马逢时. 六西格玛管理统计指南[M]. 北京: 中国人民大学出版社, 2007: 518−522

    MA F S. Guide to six sigma management statistics[M]. Beijing: China Renmin University Press, 2007: 518−522.
    [32]
    何桢. 六西格玛管理[M]. 北京: 中国人民大学出版社, 2014: 436−440

    HE Z. Six sigma management[M]. Beijing: China Renmin University Press, 2014: 436−440.
  • Cited by

    Periodical cited type(0)

    Other cited types(1)

Catalog

    Article Metrics

    Article views PDF downloads Cited by(1)

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return