Data Visual Analysis of Physicochemical Parameters of Two Batches of Frying Oil with Different Storage Time

LI Yumei; WAN Xin; CAO Yanping; XIE Jiuying; JI Jingjun; WANG Xin

doi:10.13386/j.issn1002-0306.2021090337

Volume 43 Issue 20

Oct. 2022

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Science and Technology of Food Industry > 2022 > 43(20): 281-290. > DOI: 10.13386/j.issn1002-0306.2021090337

LI Yumei, WAN Xin, CAO Yanping, et al. Data Visual Analysis of Physicochemical Parameters of Two Batches of Frying Oil with Different Storage Time[J]. Science and Technology of Food Industry, 2022, 43(20): 281−290. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021090337.

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Data Visual Analysis of Physicochemical Parameters of Two Batches of Frying Oil with Different Storage Time

LI Yumei^1,,
WAN Xin¹,
CAO Yanping^{2, 3, ,},
XIE Jiuying^{2, 3},
JI Jingjun^{2, 3},
WANG Xin¹

1.
School of Mathematics and Statistics, Beijing Technology and Business University, Beijing 100048, China
2.
Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Technology and Business University, Beijing 100048, China
3.
Beijing Laboratory of Food Quality and Safety, School of Food and Health, Beijing Technology and Business University, Beijing 100048, China

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Received Date: September 29, 2021
Available Online: August 10, 2022

Graphical Abstract

Abstract

Abstract

In this paper, the acid value, carbonyl value and total polar components data measured in the two batches of frying soybean oil which were stored for 18 and 3 months respectively, were used to make some calculations and visual analysis, so as to observe the changes of physicochemical parameters of two batches of oil at the corresponding time points under the same experimental conditions, for providing convenience about the safety monitoring of frying oil. Firstly, statistical description and boxplot analysis were carried out according to the measured data of three physicochemical parameters. Secondly, the curve fitting visualization was carried out. Then, the surface and corresponding contour visualization analyses of “time-temperature-parameter’s value” were carried out. In the boxplot visualization, it was generally observed that the variation ranges of the physicochemical parameters of oil stored for a long time were larger at the same frying temperature. In the curve fitting visualization, it was found that the acid values changed most regularly, which could be used to estimate the corresponding acid values of another batch of oil under the same experimental conditions, and could also be used to estimate the storage time of another batch of oil according to the known storage time of this batch of oil. In the surface and contour visualization, it was found that 190 ℃ was a dividing point of the temperatures. In the frying process above 190 ℃, the physicochemical parameters of oil stored for a longer time increased faster, the oxidation rate increased and the oil was more unstable. At the same time, it was also found that 20 h was a dividing point of the time. After 20 h, the physicochemical parameters of oil stored for a longer time increased faster. In the case of continuous frying, the temperature should not exceed 190 ℃ and the frying time should not exceed 20 h.
- storage time,
- frying oil,
- physicochemical parameters,
- visual analysis,
- fitting curve plot,
- interpolation surface graph,
- contour map

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References (28)

References

[1]	吕芳, 林祥娜, 朱靖雯, 等. 煎炸油脂质变预防及其危害控制研究进展[J]. 工业微生物,2020,50(1):56−62. [LU F, LIN X N, ZHU J W, et al. Research progress in alleviating oxidative harm of fried oil[J]. Industrial Microbiology,2020,50(1):56−62. doi: 10.3969/j.issn.1001-6678.2020.01.010
[2]	李裕梅, 唐润发, 杜芳芳, 等. 食用煎炸油理化指标统计分析方法研究进展[J]. 食品工业科技,2021,42(7):416−426. [LI Y M, TANG R F, DU F F, et a1. Research progress of statistical analysis methods for physicochemical parameters of edible frying oil[J]. Science and Technology of Food Industry,2021,42(7):416−426.
[3]	王进英, 钟海雁, 冯纳, 等. 油茶籽油甘三酯组成的NARP-HPLC-EISD分析及其在高温处理过程中的降解研究[J]. 中国粮油学报,2017,32(3):54−60. [WANG J Y, ZHONG H Y, FENG N, et al. Analysis of NARP-HPLC-EISD composed by Camellia oleosa seed oil triacylglycerol and degradation research during high-temperature processing[J]. Journal of the Chinese Cereals and Oils Association,2017,32(3):54−60. doi: 10.3969/j.issn.1003-0174.2017.03.010
[4]	薛斌, 曹文明, 印瑜洁. 制备型快速柱层析检测煎炸油极性组分含量[J]. 食品与机械,2017,33(9):78−80. [XUE B, CAO W M, YIN Y J. Detect the content of polar components in frying oils by preparative FLASH chromatography[J]. Food & Machinery,2017,33(9):78−80. doi: 10.13652/j.issn.1003-5788.2017.09.016
[5]	王俏君, 赵晨伟, 吴港城, 等. 煎炸油中核心醛的GC-MS分析及变化趋势研究[J]. 中国油脂,2019,44(10):90−94. [WANG Q J, ZHAO C W, WU G C, et al. GC-MS analysis and change trend of core aldehydes in frying oil[J]. China Oils and Fats,2019,44(10):90−94.
[6]	LI X, LI J, WANG Y, et al. Effects of frying oils' fatty acids profile on the formation of polar lipids components and their retention in French fries over deep-frying process[J]. Food Chemistry,2017,237:98−105. doi: 10.1016/j.foodchem.2017.05.100
[7]	LI X, WU G C, YANG F, et al. Influence of fried food and oil type on the distribution of polar compounds in discarded oil during restaurant deep frying[J]. Food Chemistry,2019,272:12−17. doi: 10.1016/j.foodchem.2018.08.023
[8]	SAYYAD R. Effects of deep-fat frying process on the oil quality during French fries preparation[J]. Journal of Food Science and Technology,2017,54(8):2224−2229. doi: 10.1007/s13197-017-2657-x
[9]	YU K S, CHO H, HWANG K T. Physicochemical properties and oxidative stability of frying oils during repeated frying of potato chips[J]. Food Science and Biotechnology,2018,27(3):651−659. doi: 10.1007/s10068-017-0292-y
[10]	SANTOS C S P, GARCÍA L M, CRUZ R, et al. Impact of potatoes deep-frying on common monounsaturated-rich vegetable oils: A comparative study[J]. Journal of Food Science and Technology,2019,56(1):290−301. doi: 10.1007/s13197-018-3489-z
[11]	LIU X F, WANG S, MASUI E, et al. Real-time model for carbonyl value as a function of total polar compounds in oil during frying[J]. Analytical Letters,2021,54(18):1−13.
[12]	ZULU N, KAYITESI E, OGUNDELE O M. Chemical and deep-frying oxidative stability of sunflower–red palm olein blends[J]. British Food Journal,2021,123(12):3938−3953. doi: 10.1108/BFJ-09-2020-0837
[13]	PREMAVALLI K S, MADHURA C V, ARYA S S. Storage and thermal stability of refined cottonseed oil-mustard oil blend[J]. Journal of Food Science and Technology,1998,35(6):530−536.
[14]	AHMED S O, MOHAMMED D O, MOHAMED F A, et al. Effect of frying and storage on oxidative stability of oil blends and quality attributes of biscuits prepared with the blends[J]. Annals Food Science and Technology,2017,18(4):564−572.
[15]	栾霞, 王瑛瑶, 张蕊, 等. 油脂储藏过程中茴香胺值、过氧化值的变化研究[J]. 粮油加工,2009(12):77−79. [LUAN X, WANG Y Y, ZHANG R, et al. Study on the changes of anisidine value and peroxide value during oil storage[J]. Cereals and Oils Processing,2009(12):77−79.
[16]	解久莹, 吉静筠, 李裕梅, 等. 基于多项式拟合对煎炸油质量的预测[J]. 食品工业科技,2019,40(14):11−17. [XIE J Y, JI J Y, LI Y M, et al. Prediction of frying oil quality based on polynomial curve fitting[J]. Science and Technology of Food Industry,2019,40(14):11−17. doi: 10.13386/j.issn1002-0306.2019.14.002
[17]	中华人民共和国卫生部, 中国国家标准化管理委员会. GB/T 5009.37-2003食用植物油卫生标准的分析方法[S]. 北京: 中国标准出版社, 2004. Ministry of Health of the People's Republic of China, Standardization Administration of the People's Republic of China. GB/T 5009.37-2003 Method for analysis of hygienic standard of edible oils[S]. Beijing: China Standards Press, 2004.
[18]	中华人民共和国卫生部, 中国国家标准化管理委员会. GB/T 5009.202-2016食用油中极性组分（ PC ）的测定[S]. 北京: 中国标准出版社, 2016. Ministry of Health of the People’s Republic of China, Standardization Administration of the People’s Republic of China. GB/T 5009.202-2016 Determination of polar compounds in edible vegetable oils used in frying food[S]. Beijing: China Standards Press, 2016.
[19]	孙丽琴, 孙立君, 郑刚. 不同的存放条件对油脂酸价和过氧化值的影响[J]. 粮油仓储科技通讯,2007,2(2):45−46. [SUN L Q, SUN L Q, ZHENG G. Effects of different storage conditions on acid value and peroxide value of oil[J]. Liangyou Cangchu Keji Tongxun,2007,2(2):45−46.
[20]	刘羽鹏, 郑艳春. 食用大豆油储藏期间酸价过氧化值羰基价变化的分析[J]. 黑龙江粮油科技,1996(1):45−46. [LIU Y P, ZHENG Y C. Analysis on the change of acid value, peroxide value and carbonyl value of edible soybean oil during storage[J]. Journal of Heilongjiang Cereals and Oils Science and Technology,1996(1):45−46.
[21]	杨祖伟, 陈晓霞, 孙浩洋, 等. 羰基价测定影响因素考察[J]. 食品安全质量检测学报,2015,6(6):2356−2360. [YANG Z W, CHEN X X, ZUN H Y, et al. Investigation on impact factors of determination of carbonyl group value[J]. Journal of Food Safety and Quality,2015,6(6):2356−2360. doi: 10.19812/j.cnki.jfsq11-5956/ts.2015.06.065
[22]	王进英, 钟海雁, 周波. 油脂在深度煎炸过程中发生的化学反应及其主要产物[J]. 中国油脂,2015,40(11):37−43. [WANG J Y, ZHONG H Y, ZHOU B. Chemical reaction and main products of oils and fats during deep-frying[J]. China Oils and Fats,2015,40(11):37−43. doi: 10.3969/j.issn.1003-7969.2015.11.008
[23]	周雅琳, 周令国, 李智, 等. 影响煎炸油中极性化合物生成因素的研究[J]. 中国粮油学报,2010,25(3):50−53. [ZHOU Y L, ZHOU L G, LI Z, et al. Influencing factors for polar compounds created in oil during deep-frying[J]. Journal of the Chinese Cereals and Oils Association,2010,25(3):50−53.
[24]	王欣, 夏义苗, 史然, 等. 基于LF-NMR及主成分回归分析的油脂煎炸品质预测[J]. 中国食品学报,2015,15(4):160−168. [WANG X, XIA Y M, SHI R, et al. Quality prediction of frying oil based on LF-NMR relaxation characteristics and principal component regression[J]. Journal of Chinese Institute of Food Science and Technology,2015,15(4):160−168.
[25]	陈锋亮, 魏益民, 钟耕. 大豆油高温煎炸质变过程的研究[J]. 中国油脂,2006,31(8):19−22. [CHEN F L, WEI Y M, ZHONG G. Deterioration of soybean oil in deep-frying[J]. China Oils and Fats,2006,31(8):19−22. doi: 10.3321/j.issn:1003-7969.2006.08.006
[26]	慕鸿雁, 郑琦. 3种食用油在薯条煎炸过程中的品质变化[J]. 食品科学,2012,33(19):168−171. [MU H Y, ZHENG Q. Quality change of three kinds of edible oil during frying process[J]. Food Science,2012,33(19):168−171.
[27]	王兴国, 金青哲. 煎炸过程的科学管理及煎炸油品质控制[J]. 中国食品学报,2015,15(1):1−5. [WANG X G, JIN Q Z. Scientific management of frying process in catering industry and quality control of frying oil[J]. Journal of Chinese Institute of Food Science and Technology,2015,15(1):1−5. doi: 10.16429/j.1009-7848.2015.01.001
[28]	安柯静. 油脂煎炸过程极性组分与甘油三酯聚合物及其它组分的关联性研究[D]. 郑州: 河南工业大学, 2018. AN K J. Study on the relationship between total polar components and triglyceride polymers and other components in frying process[D]. Zhengzhou: Henan University of Technology, 2018.

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