Optimization of Ultrasonic-Assisted Deep Eutectic Solvent Extraction of Total Flavonoids from Corncob

LI Li; YANG Jingqi; YU Dehan; QU Nan; SUN Yue; XU Zhe

doi:10.13386/j.issn1002-0306.2021080197

Volume 43 Issue 10

May 2022

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Science and Technology of Food Industry > 2022 > 43(10): 223-230. > DOI: 10.13386/j.issn1002-0306.2021080197

LI Li, YANG Jingqi, YU Dehan, et al. Optimization of Ultrasonic-Assisted Deep Eutectic Solvent Extraction of Total Flavonoids from Corncob[J]. Science and Technology of Food Industry, 2022, 43(10): 223−230. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021080197.

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Optimization of Ultrasonic-Assisted Deep Eutectic Solvent Extraction of Total Flavonoids from Corncob

Food and Pharmaceutical Engineering Department, Suihua University, Suihua 152061, China

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Received Date: August 18, 2021
Available Online: March 15, 2022

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Abstract

Abstract

Total flavonoids from corncob were extracted using ultrasonic-assisted deep eutectic solvent. Firstly, the extraction solvent composition and component ratio were determined by screening experiment. Then response surface methodology was used to optimize the extraction process. The extraction temperature, liquid-solid ratio, ultrasonic power and extraction time were used as variables, and the extraction amount of total flavonoids was used as response value. The results showed that the optimum extraction process of total flavonoids from corncob with choline chloride/ethylene glycol (molar ratio 1:3) with water content of 30% was as follows: Temperature 61 ℃, 20:1 (mL/g) of liquid-solid ratio, ultrasonic power 137 W, and extraction time 19.5 min, the extraction amount of flavonoids was 4.180 mg/g, with an error of 0.71% compared with the predicted value. The method was proved to be stable and reliable, and could provide scientific data for the development and utilization of flavonoids in corncob.
- corncob,
- total flavonoids,
- deep eutectic solvent,
- ultrasonic

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