Preparation and Stability of Hazelnut Oil Microcapsules

ZHANG Wei; CHEN Lirui; SHI Mengjie; LIU Huan; FAN Liying

doi:10.13386/j.issn1002-0306.2021040331

Volume 43 Issue 2

Jan. 2022

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Science and Technology of Food Industry > 2022 > 43(2): 206-214. > DOI: 10.13386/j.issn1002-0306.2021040331

ZHANG Wei, CHEN Lirui, SHI Mengjie, et al. Preparation and Stability of Hazelnut Oil Microcapsules[J]. Science and Technology of Food Industry, 2022, 43(2): 206−214. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021040331.

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Preparation and Stability of Hazelnut Oil Microcapsules

College of Life Science and Technology, Changchun University of Science and Technology, Changchun 130022, China

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Received Date: May 05, 2021
Available Online: November 13, 2021

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Abstract

Abstract

In order to alleviate the oxidation rate of hazelnut oil, increase the storage period and expand its application range, this study used β-cyclodextrin (β-CD) as the wall material and used the ultrasonic-assisted molecular embedding method to prepare hazelnut oil microcapsules, the process conditions of the microcapsules were optimized by response surface method, and their physical and chemical properties were measured at the same time. The results showed that when the wall material concentration (H₂O/β-CD) was 16:1, the wall-to-core ratio was 5:1, the embedding time was 62 min, and the embedding temperature was 59.3 ℃, the embedding rate of microcapsules was up to 69.18%, and the yield rate reached 59.74%. The average particle size of the microcapsules was 880.4 nm, the moisture content was 2.85%, the solubility was 55.95%, and the angle of repose was 42.49°. The results of scanning electron microscopy, infrared spectroscopy and thermogravimetric analysis showed that the microcapsules had a block, diamond-shaped flake or irregular columnar structure, the embedded material had been formed, and had good thermal stability. Accelerated oxidation experiments showed that microencapsulation could effectively slow down the oxidation rate of hazelnut oil, extend the shelf life, and expand its application range.
- hazelnut oil,
- microencapsulation,
- powdery oil,
- microencapsulation efficiency,
- response surface,
- physical and chemical properties

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[1]	蔡可心, 倪佳洁, 秦文文, 等. 超声波辅助乙醇提取平欧杂交榛榛子油工艺优化[J]. 食品工业科技,2020,41(6):180−184,203. [CAI K X, NI J J, QIN W W, et al. Ultrasonic-assisted ethanol extraction process optimization of flat-European hybrid hazelnut oil[J]. Science and Technology of Food Industry,2020,41(6):180−184,203.
[2]	XU Y X, HANNA M A, JOSIAH S J. Hybrid hazelnut oil characteristics and its potential oleochemical application[J]. Industrial Crops & Products,2007,26(1):69−76.
[3]	车丹, 杨春莉, 王莹, 等. 榛子油的提取及微胶囊化研究进展[J]. 食品科技,2019,44(12):228−232. [CHE D, YANG C L, WANG Y, et al. Research progress on the extraction and microencapsulation of hazelnut oil[J]. Food Science and Technology,2019,44(12):228−232.
[4]	ROYA R A, SAMEEREH H N, FATEMEH B. Immunoisolation of stem cells by simultaneous encapsulation and pegylation[J]. Progress in Biomaterials,2018,7(1):55−60. doi: 10.1007/s40204-018-0084-3
[5]	任小玲, 岳淑丽, 向红, 等. 桉叶精油微胶囊工艺优化及缓释性能研究[J]. 包装工程,2017,38(9):107−112. [REN X L, YUE S L, XIANG H, et al. Process optimization and slow-release performance of eucalyptus essential oil microcapsules[J]. Packaging Engineering,2017,38(9):107−112.
[6]	周宇, 晏敏, 梅明鑫, 等. 微胶囊技术在油脂工业中的研究进展[J]. 食品与发酵工业,2018,44(4):293−300. [ZHOU Y, YAN M, MEI M X, et al. Research progress of microencapsulation technology in oil industry[J]. Food and Fermentation Industries,2018,44(4):293−300.
[7]	李延辉, 郑明珠, 刘景圣. 微胶囊化榛仁油的制备工艺研究[J]. 食品科学,2006,27(6):136−138. [LI Y H, ZHENG M Z, LIU J S. Study on the preparation technology of microencapsulated hazelnut oil[J]. Food Science,2006,27(6):136−138. doi: 10.3321/j.issn:1002-6630.2006.06.027
[8]	FATIH K, VANGA S K, MURUGESAN R, et al. Microencapsulation of hazelnut oil through spray drying[J]. Taylor & Francis,2017,35(5):527−533.
[9]	杨春瑜, 车丹, 卢彦岑, 等. 榛子油的微胶囊化工艺优化[J]. 食品工业科技,2020,41(8):183−188. [YANG C Y, CHE D, LU Y C, et al. Optimization of microencapsulation process of hazelnut oil[J]. Science and Technology of Food Industry,2020,41(8):183−188.
[10]	杨青珍, 王锋, 李康. 超声波辅助提取榛子油的工艺条件优化[J]. 中国粮油学报,2011,26(8):58−61. [YANG Q Z, WANG F, LI K. Optimization of the technological conditions for ultrasonic-assisted extraction of hazelnut oil[J]. Journal of the Chinese Cereals and Oils Association,2011,26(8):58−61.
[11]	刘星, 丁琨, 李冠文, 等. 连翘叶精油微胶囊制备工艺优化及其对油脂抗氧化的影响[J]. 保鲜与加工,2020,20(6):76−83. [LIU X, DING K, LI G W, et al. Preparation process optimization of Forsythia suspensa essential oil microcapsules and its effect on anti-oxidation of fats[J]. Freshness and Processing,2020,20(6):76−83. doi: 10.3969/j.issn.1009-6221.2020.06.013
[12]	王顺民, 薛正莲, 余建斌. 山核桃油微胶囊技术研究[J]. 食品工业科技,2012,33(1):268−271,274. [WANG S M, XUE Z L, YU J B. Research on pecan oil microcapsule technology[J]. Science and Technology of Food Industry,2012,33(1):268−271,274.
[13]	刘光宪, 周巾英, 祝水兰, 等. 沙棘籽油微胶囊的制备及其性质研究[J]. 食品与机械,2017,33(8):194−197. [LIU G X, ZHOU J Y, ZHU S L, et al. Preparation and properties of seabuckthorn seed oil microcapsules[J]. Food and Machinery,2017,33(8):194−197.
[14]	钱奕含. 米威化饼干抗氧化保质包装研究[D]. 无锡: 江南大学, 2020: 37−38. QIAN Y H. Research on antioxidant packaging of rice wafer biscuits[D]. Wuxi: Jiangnan University, 2020: 37−38.
[15]	WANG B, ADHIKARI B, BARROW C J. Optimisation of the microencapsulation of tuna oil in gelatin-sodium hexametaphosphate using complex coacervation[J]. Food Chemistry,2014,158(3):358−365.
[16]	HOGAN S A, MCNAMEE B F, O’RIORDAN E D, et al. Emulsification and microencapsulation properties of sodium caseinate/carbohydrate blends[J]. International Dairy Journal,2001,11(3):137−144. doi: 10.1016/S0958-6946(01)00091-7
[17]	岳昊, 邱斌, 张文龙, 等. 功能油脂微胶囊的工艺优化及稳定性研究[J]. 食品研究与开发,2020,41(15):51−57. [YUE H, QIU B, ZHANG W L, et al. Study on process optimization and stability of functional oil microcapsules[J]. Food Research and Development,2020,41(15):51−57. doi: 10.12161/j.issn.1005-6521.2020.15.010
[18]	朱建宇, 齐宝坤, 张小影, 等. 喷雾干燥制备大豆油脂体微胶囊及其品质分析[J]. 食品工业科技,2020,41(7):146−153,160. [ZHU J Y, QI B K, ZHANG X Y, et al. Preparation and quality analysis of soybean oil microcapsules by spray drying[J]. Science and Technology of Food Industry,2020,41(7):146−153,160.
[19]	范少丽, 敬思群, 纵伟. 双包被番茄红素微胶囊特性分析[J]. 中国调味品,2015,40(6):37−42. [FAN S L, JING S Q, ZONG W. Characteristic analysis of double-coated lycopene microcapsules[J]. China Condiments,2015,40(6):37−42. doi: 10.3969/j.issn.1000-9973.2015.06.009
[20]	AGHBASHLO M, MOBLI H, MADADLOU A. Influence of wall material and inlet drying air temperature on the microencapsulation of fish oil by spray drying[J]. Food Bioprocess Technology,2013,6(6):796−804.
[21]	刘全亮, 马传国, 王化林, 等. 微胶囊化棕榈油的品质分析[J]. 粮油食品科技,2015,23(1):38−42. [LIU Q L, MA C G, WANG H L, et al. Quality analysis of microencapsulated palm oil[J]. Cereals, Oils and Foods Science and Technology,2015,23(1):38−42. doi: 10.3969/j.issn.1007-7561.2015.01.010
[22]	KANO K. Porphyrin-cyclodextrin supramolecular complexes as myoglobin model in water[J]. Colloid and Polymer Science,2008,286(1):79−84. doi: 10.1007/s00396-007-1724-7
[23]	王春玉, 张岩, 韩雨露, 等. 包合法制备橄榄油微胶囊的工艺研究[J]. 粮油食品科技,2015,23(1):30−34,83. [WANG C Y, ZHANG Y, HAN Y L, et al. Study on the technology of preparing olive oil microcapsules by encapsulation[J]. Cereals, Oils and Foods Science and Technology,2015,23(1):30−34,83. doi: 10.3969/j.issn.1007-7561.2015.01.008
[24]	HO B T, JOYCE D C, BHANDARI B R. Release kinetics of ethylene gas from ethylene–α-cyclodextrin inclusion complexes[J]. Food Chemistry,2011,129(2):259−266. doi: 10.1016/j.foodchem.2011.04.035
[25]	王赛丹, 江振西, 曹秀丽, 等. 香根油β-环糊精微胶囊制备工艺优化[J]. 现代化工,2017,37(1):136−139,141. [WANG S D, JIANG Z X, CAO X L, et al. Optimization of preparation process of vetiver oil β-cyclodextrin microcapsules[J]. Modern Chemical Industry,2017,37(1):136−139,141.
[26]	恽菲, 徐晓琰, 狄留庆, 等. 蛇床子素不同环糊精包合物的制备及其生物利用度比较研究[J]. 中草药,2014,45(3):341−348. [YUN F, XU X Y, DI L Q, et al. Preparation of different cyclodextrin inclusion compounds of osthole and comparative study on their bioavailability[J]. Chinese and Herbal Medicine,2014,45(3):341−348.
[27]	CHAN Y T, TAN M C, CHIN N L. Application of Box-Behnken design in optimization of ultrasound effect on apple pectin as sugar replacer[J]. LWT-Food Science and Technology,2019,115(11):1−8.
[28]	JIANG H L, YANG J L, SHI Y P. Optimization of ultrasonic cell grinder extraction of anthocyanins from blueberry using response surface methodology[J]. Ultrasonics-Sono-Chemistry,2017,34(1):325−331.
[29]	NAKANISHI I, ARAI M, FUJIWARA T, et al. X-ray structural studies on two forms of β-CD barbital complexes[J]. Journal of Inclusion Phenomena,1984,2(3−4):689−699. doi: 10.1007/BF00662237
[30]	马云标, 朱科学, 周惠明. 维生素E微胶囊的理化性质表征[J]. 中国油脂,2010,35(1):55−59. [MA Y B, ZHU K X, ZHOU H M. Characterization of physical and chemical properties of vitamin E microcapsules[J]. China Oils and Fats,2010,35(1):55−59.
[31]	朱士龙, 陈迪钊, 李勇, 等. 青藤碱-β-环糊精包合物的制备及表征[J]. 中草药,2012,43(7):1328−1332. [ZHU S L, CHEN D Z, LI Y, et al. Preparation and characterization of sinomenine-β-cyclodextrin inclusion compound[J]. Chinese and Herbal Medicine,2012,43(7):1328−1332.
[32]	REICH G. Near-infrared spectroscopy and imaging: Basic principles and pharmaceutical applications[J]. Advanced Drug Delivery Reviews,2005,57(8):1109−1143. doi: 10.1016/j.addr.2005.01.020
[33]	WAKIL W, GHAZANFAR M U, NASIR F, et al. Insecticidal efficacy of Azadirachta indica, Nucleopolyhedrovirus and chlorantraniliprole singly or combined against field populations fo Helicoverpa armigera Hübner (Lepidoptera: Noctuidae)[J]. Chilean Journal of Agricultural Research,2012,72(1):53−61. doi: 10.4067/S0718-58392012000100009
[34]	HIROO N, TAKASHI S, TADAHIKO K, et al. Evaluation of systemic chemotherapy with magnetic liposomal doxorubicin and a dipole external electromagnet[J]. International Journal of Cancer,2004,109(4):627−635. doi: 10.1002/ijc.20035
[35]	温金梅. GB 2716-2018《食品安全国家标准植物油》标准解读[J]. 中国质量与标准导报,2018,13(11):19−21. [WEN J M. Interpretation of GB 2716-2018 “National food safety standard vegetable oil” standard[J]. China Quality and Standards Guide,2018,13(11):19−21. doi: 10.3969/j.issn.1004-1575.2018.11.013

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