Purification Technology and Stability of Sugar-Smoking Pigment

Jianbo ZHANG; Qihan LIU; Tongtong LIU; Dengyong LIU

doi:10.13386/j.issn1002-0306.2020070137

Volume 42 Issue 10

May 2021

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Science and Technology of Food Industry > 2021 > 42(10): 160-167. > DOI: 10.13386/j.issn1002-0306.2020070137

ZHANG Jianbo, LIU Qihan, LIU Tongtong, et al. Purification Technology and Stability of Sugar-Smoking Pigment[J]. Science and Technology of Food Industry, 2021, 42(10): 160−167. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020070137.

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Purification Technology and Stability of Sugar-Smoking Pigment

Jianbo ZHANG^1,,
Qihan LIU^{1, 2},
Tongtong LIU¹,
Dengyong LIU^{1, 2, ,}

1.
National and Local Joint Engineering Research Center for Fresh Agricultural Products Storage, Processing and Safety Control Technology, School of Food Science and Engineering, Bohai University, Jinzhou 121013, China
2.
Jiangsu Meat Production and Processing Quality and Safety Control Collaborative Innovation Center, Nanjing 210095, China

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Received Date: July 12, 2020
Available Online: March 14, 2021

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Abstract

Abstract

Objective: To purified sugar-smoking pigment and analysis its structure and properties. Methods: In this study, the macroporous resin was used to purified the sugar-smoking pigment, and the stability of the purified sugar-smoking pigment was studied. Results: XAD-7 macroporous resin had good adsorption and desorption capacity for sugar-smoking pigment. The optimal process conditions for the static adsorption and desorption process of sugar-smoking pigment were the concentration of the crude extract of sugar-smoking pigments 60 µg/mL, pH was 8.0, adsorption temperature 35 ℃, concentration of desorption 40% ethanol, pH 10.0 and desorption temperature 40 ℃. desorption solution concentration was 40% ethanol, and pH was 10.0, desorption temperature was 40 ℃. The best process conditions for dynamic adsorption and desorption were diameter/height 1:6, sample flow rate 2.0 mL/min, sample solution concentration 400 µg/mL, desorption solution concentration 40% ethanol, and desorption solution flow rate 1.5 mL/min. Conclusion: After being purified by XAD-7 resin in static and dynamic processes, the purity of sugar-smoking pigment were increased by 45.13% and 36.55%, respectively. The purified sugar smoked pigment was easy to dissolve, and the solution was clear and bright yellow, sensitive to light but has higher thermal stability. The sugar-smoking pigment might be the caramel colour Ⅰ.
- sugar-smoking pigment,
- macroporous resin,
- purification process,
- stability

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References

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