Optimization of Supercritical CO<sub>2</sub> Extraction of Essential Oil from Hemp Leaves by Response Surface Methodology

Yuan TIAN; Yufeng SUN; Zhenghai ZHANG; Xu ZHANG; Yu SHI; Yan DONG; Baoyu CUI; Xiaoyan ZHANG; Chengwei HAN; Lianhui WEI; Qingli YANG; Baochang GAO

doi:10.13386/j.issn1002-0306.2020060170

Volume 42 Issue 8

Apr. 2021

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Science and Technology of Food Industry > 2021 > 42(8): 158-163. > DOI: 10.13386/j.issn1002-0306.2020060170

TIAN Yuan, SUN Yufeng, ZHANG Zhenghai, et al. Optimization of Supercritical CO₂ Extraction of Essential Oil from Hemp Leaves by Response Surface Methodology [J]. Science and Technology of Food Industry, 2021, 42(8): 158−163. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020060170.

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Optimization of Supercritical CO₂ Extraction of Essential Oil from Hemp Leaves by Response Surface Methodology

Daqing Branch of Heilongjiang Academy of Sciences, Daqing 163319, China

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Received Date: June 14, 2020
Available Online: January 27, 2021

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Abstract

Abstract

Extracted essential oil from hemp leaves was extracted by supercritical CO₂. Single factor experiments and response surface analysis were applied in the optimization of the extraction process of essential oil from hemp leaves. The influencing factors were extraction pressure (X₁), extraction temperature (X₂), extraction time (X₃) and CO₂ flow rate (X₄), and the extraction rate of essential oil from hemp leaves was used as the evaluation index for response surface analysis. Results showed that, combined with the practical operability and convenience of the extraction process, which extraction pressure 29 MPa, extraction temperature 49 ℃, extraction time 3.4 h, CO₂flow rate 13 mL/min were determined the optimal extraction process. The actual extraction rate was 0.283%, which was close to the theoretical value of 0.281% and the actual deviation between the predicted value and the real value was −0.71%. It was suggested that supercritical CO₂ extraction had practical and development value in the extraction of essential oil from hemp leaves, which could provide a theoretical reference essential oil from hemp leaves in the future.
- hemp leaf,
- essential oils,
- supercritical CO₂ extraction,
- response surface methodology

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