XIAO Man, TANG Bin, JIANG Fatang, WANG Hao, ZHENG Han, ZHANG Ying, XIE Jiao, ZHAN Jianbo. Formulation Optimization of Konjac Glucomannan-Ethyl Cellulose Composite Film and Its Application in Honey Packaging[J]. Science and Technology of Food Industry, 2021, 42(4): 181-186,207. DOI: 10.13386/j.issn1002-0306.2020050020
Citation: XIAO Man, TANG Bin, JIANG Fatang, WANG Hao, ZHENG Han, ZHANG Ying, XIE Jiao, ZHAN Jianbo. Formulation Optimization of Konjac Glucomannan-Ethyl Cellulose Composite Film and Its Application in Honey Packaging[J]. Science and Technology of Food Industry, 2021, 42(4): 181-186,207. DOI: 10.13386/j.issn1002-0306.2020050020

Formulation Optimization of Konjac Glucomannan-Ethyl Cellulose Composite Film and Its Application in Honey Packaging

More Information
  • Received Date: May 05, 2020
  • Available Online: March 01, 2021
  • In order to study formulation optimization of konjac glucomannan(KGM)and ethyl cellulose(EC)composite film and its application to honey packaging,KGM,EC,and dibutyl glycerate(DBS)were used as raw materials,and water and ethyl acetate as the solvent to prepare films,and formulations optimization of the film was tested by the single factor and response surface methodology in conjunction with miscellaneous design. The result showed that the optimal formulation of the composite film was composed of 70% KGM,30% EC,and 8% DBS,and the prepared film had the maximum tensile strength of 64.56 MPa.Based on this,investigating the heat sealing conditions of KGM/EC film and applying the film to honey packaging,the result showed that the film reached a maximum sealing strength of 4.4 N/15 mm using 2% KGM sol as an adhesive to heat seal KGM/EC film for 14 s. The honey packaging bag was stored at 25 ° C and 50%±5% relative humidity for 22 days to achieve water vapor adsorption and desorption balance,and the weight loss rate was 9.3%. No microbial colonies in honey were detected. In summary,the KGM/EC composite film has potential application in honey packaging.
  • [1]
    Mohamed S A A,El-Sakhawy M,El-Sakhawy A M. Polysaccharides,protein and lipid-based natural edible films in food packaging:A review[J]. Carbohydrate Polymers,2020:116178.
    [2]
    Chua M,Chan K,Hocking T J,et al. Methodologies for the extraction and analysis of konjac glucomannan from corms of Amorphophallus konjac K. Koch[J]. Carbohydrate Polymers,2012,87(3):2202-2210.
    [3]
    Li X,Jiang F T,Ni X W,et al. Preparation and characterization of konjac glucomannan and ethyl cellulose blend films[J]. Food Hydrocolloids,2015:229-236.
    [4]
    Du Y,Sun J,Wang L,et al. Development of antimicrobial packaging materials by incorporation of gallic acid into Ca2+ crosslinking konjac glucomannan/gellan gum films. International Journal of Biological Macromolecules,2019,137,1076-1085.
    [5]
    Katsuraya K,Okuyama K,Hatanaka K,et al. Constitution of konjac glucomannan:Chemical analysis and13C NMR spectroscopy[J]. Carbohydrate Polymers,2003,53(2):183-189.
    [6]
    王恒,肖满,吴考,等.甘油对中试魔芋葡甘聚糖流延膜性能的影响[J]. 包装工程,2017,38(7):59-63.
    [7]
    Xiao C,Gao S,Wang H,et al. Blend films from chitosan and konjac glucomannan solutions[J]. Journal of Applied Polymer Science,2000,76(4):509-515.
    [8]
    Wu C,Peng S,Wen C,et al. Structural characterization and properties of konjac glucomannan/curdlan blend films[J]. Carbohydrate Polymers,2012,89(2):497-503.
    [9]
    Rhim J W,Wang L F. Mechanical and water barrier properties of agar/κ-carrageenan/konjac glucomannan ternary blend biohydrogel films[J]. Carbohydrate Polymers,2013,96(1):71-81.
    [10]
    Yang G,Xiong X,Zhang L. Microporous formation of blend membranes from cellulose/konjac glucomannan in NaOH/thiourea aqueous solution[J]. Journal of Membrane Science,2002,201(1):161-173.
    [11]
    Mahnaj T,Ahmed S U,Plakogiannis F M. Characterization of ethyl cellulose polymer[J]. Pharmaceutical Development & Technology,2013,18(5):982-989.
    [12]
    Rekhi G S,Jambhekar S S. Ethylcellulose-a polymer review[J]. Drug Development & Industrial Pharmacy,1995,21(1):61-77.
    [13]
    姚从春. 乙基纤维素气体复合膜的制备与改性研究[D]. 大连:大连理工大学,2013.
    [14]
    Ni X W,Chen W J,Xiao M et al. Physical stability and rheological properties of konjac glucomannan-ethyl cellulose mixed emulsions[J]. International Journal of Biological Macromolecules,2016,92,423-430.
    [15]
    Xiao M,Wan L,Harold C,et al. Characterization of konjac glucomannan-ethyl cellulose film formation via microscopy[J]. International Journal of Biological Macromolecules,2016,85:434-441.
    [16]
    万力,肖满,倪学文,等. 魔芋葡甘聚糖/乙基纤维素共混成膜机理的研究[J]. 湖北工业大学学报,2016,31(1):81-84.
    [17]
    范珺. 蜂蜜的吸湿性分析及包装透湿控制方法[J]. 中国包装,2015,35(9):36-38.
    [18]
    Diblan S,Kaya S. Potassium sorbate diffusion in multilayer polymer films:Effects of water activity and pH[J]. Journal of Food Processing & Preservation,2018,42(1):1-7.
    [19]
    Ma T,Wang Q,Wu H. Optimization of extraction conditions for improving solubility of peanut protein concentrates by response surface methodology[J]. LWT-Food Science and Technology,2010,43(9):1450-1455.
    [20]
    GB/T 1040.3-2006塑料薄膜拉伸强度性能试验方法[S].
    [21]
    QB/T 2358-1998塑料薄膜包装袋热合强度试验方法[S].
    [22]
    GB/T 4789.2-2016食品卫生微生物学检验-菌落总数测定[S].
    [23]
    GB/T 15267-1994食品包装用聚氯乙烯硬片、膜[S].
    [24]
    Riikka Hyppölä,Husson I,Sundholm F. Evaluation of physical properties of plasticized ethyl cellulose films cast from ethanol solution Part I[J]. International Journal of Pharmaceutics,1996,133(1-2):161-170.
    [25]
    Lippold B C,Gunder W,Lippold B H. Drug release from diffusion pellets coated with the aqueous ethyl cellulose dispersion Aquacoat ECD-30 and 20% dibutyl sebacate as plasticizer:Partition mechanism and pore diffusion[J]. European Journal of Pharmaceutics & Biopharmaceutics,1999,47(1):27-32.
    [26]
    庞杰,林琼,张甫生,等. 魔芋葡甘聚糖功能材料研究与应用进展[J]. 结构化学,2003,22(6):633-642.
    [27]
    Suematsu A,Okuma M. Mechanism of low-density particleboard formation. 4. Bending strength of low-density particleboard[J]. Mokuzai Gakkaishi,1992,38(9):847-853.
    [28]
    陈贤情. KGM/CA/PVA三元共混胶粘剂棉秆重组材的制备及其成板机理研究[D]. 陕西:西北农林科技大学,2016:8-11.
    [29]
    潘键,张燕飞,张和平. 复合包装膜的热封性能判定及影响因素分析[J]. 包装与食品机械,2020,38(2):70-72.
    [30]
    杜玉宝,骆光林. 浅谈包装材料热封性能的影响因素[J].塑料包装,2007,17(4):29-32.
    [31]
    Wu K,Zhu Q,Qian H,et al. Controllable hydrophilicity-hydrophobicity and related properties of konjac glucomannan and ethyl cellulose composite films[J]. Food Hydrocolloids,2017,79:301-309.
    [32]
    Frink L A,Armstrong D W. The utilisation of two detectors for the determination of water in honey using headspace gas chromatography[J]. Food Chemistry,2016,205:23-27.
  • Cited by

    Periodical cited type(6)

    1. 张月,杨新玥,黄莉,马帅宇,胥畅,杨腊梅,裴慧洁,何维,杨勇. 乳酸菌复配发酵对川味香肠品质及酪胺含量的影响. 食品与发酵工业. 2025(06): 83-90 .
    2. 李莹,钱敏,曾晓房,白卫东,吴清平,杨小鹃,董浩. 畜禽肉类预制菜肴全链条风险因子研究进展. 食品工业科技. 2025(07): 365-374 . 本站查看
    3. 牟燕,赖茂佳,易宇文,范文教. 微生物发酵剂对川味牦牛肉香肠品质的影响. 中国酿造. 2024(02): 188-193 .
    4. 李晓,王成,郭楠楠,潘道东. 嗜酸乳杆菌发酵鸭肉脯工艺优化及品质分析. 肉类研究. 2024(01): 36-43 .
    5. 赵志磊,李昊轩,牛晓颖,陈萌,庞艳苹. γ射线辐照结合VC、烟酰胺对卤驴肉中亚硝酸盐的降解效果. 食品科学. 2024(16): 197-203 .
    6. 文静,许恒毅,甘蓓,周渊坤,张锦峰. 混合菌株发酵板鸭的研究进展. 江西科学. 2024(04): 710-715 .

    Other cited types(3)

Catalog

    Article Metrics

    Article views (211) PDF downloads (23) Cited by(9)

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return