Effect of Three Extraction Methods on the Volatile Components of <i>Zanthoxylum bungeanum</i>

WANG Xuedi; XU Duoxia; WANG Bei; WANG Shaojia; CAO Yanping

doi:10.13386/j.issn1002-0306.2020020274

Volume 42 Issue 2

Jan. 2021

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Science and Technology of Food Industry > 2021 > 42(2): 241-249. > DOI: 10.13386/j.issn1002-0306.2020020274

WANG Xuedi, XU Duoxia, WANG Bei, WANG Shaojia, CAO Yanping. Effect of Three Extraction Methods on the Volatile Components of Zanthoxylum bungeanum[J]. Science and Technology of Food Industry, 2021, 42(2): 241-249. DOI: 10.13386/j.issn1002-0306.2020020274

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Effect of Three Extraction Methods on the Volatile Components of Zanthoxylum bungeanum

1. Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Technology And Business University, Beijing 100048, China;
2. Beijing Engineering and Technology Research Center of Food Additives, Beijing Technology And Business University, Beijing 100048, China

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Received Date: February 26, 2020
Available Online: January 20, 2021

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Abstract

Abstract

The experiment was carried out by using Zanthoxylum bungeanum as raw material and extraction of Zanthoxylum bungeanum by oil extraction,steam distillation and supercritical CO₂ extraction. The purpose of this experiment is to explore the effect of different extraction methods and different extraction parameters on volatile components of Zanthoxylum bungeanum extract.In addition,solid phase micro-extraction(SPME)combined with gas chromatography-mass spectrometry(GC-MS)was employed to determine the volatile substances and content in Zanthoxylum bungeanum extract. The quality evaluation of extract were analyzed by principal component analysis(PCA)method and relative odor activity value(ROAV).Under all conditions,65,100 and 82 kinds of volatile substances were identified by oil extraction,steam distillation and supercritical CO₂ extraction respectively. The highest content of volatile substances was obtained by supercritical CO₂ extraction,followed by steam distillation and oil extraction,13909.90,1152.61 and 249.38 μg/mL,respectively. The results of principal component analysis showed that the change trend of the scores of each group was the same as that of the total content of aroma substances under each single factor condition. Among them,oil extraction,steam distillation and supercritical CO₂ extraction had the highest total content of volatile matter and the highest comprehensive score of aroma matter when the ratio of material to liquid was 1:5、the extraction time was 5 h、and the extraction temperature was 140 ℃,the ratio of material to liquid was 1:10、the extraction time was 2 hours,and 7% ethanol addition、the ratio of ethanol was 85%,respectively. According to the value of relative odor activity,the key aroma components of the three extraction methods were different. Laurene contributes the most to the aroma in the oil extraction method,linalool and eucalyptus alcohol contribute the most to the aroma in the steam distillation method,and linalool contributes the most to the aroma in the supercritical CO₂ extraction method. In conclusion,the differences of extraction methods lead to significant changes in the types and contents of volatile substances and key aroma components in Zanthoxylum bungeanum extracts. The content of volatile substances and aroma components in supercritical CO₂ extracts are both the highest among the three methods.

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[1]	毕君,王春荣,赵京献,等. 北方花椒主产区种质资源考察报告[J]. 河北林果研究,2003,18(2):165-168.
[2]	董小强,王玉明. 花椒习性与栽培技术[J]. 科技视界,2019(1):232-233.
[3]	M S R,Z Y Janet. Safety assessment of food additives:Case example with myrcene,a synthetic flavoring agent[J]. Toxicologic Pathology,2019,47(8):1035-1037.
[4]	L Yu,W LWu,Y Y Pan,et al. Quality evaluation of different varieties of Zanthoxylum bungeanum Maxim. peels based on phenolic profiles,bioactivity,and HPLC fingerprint[J].Journal of Food Science,2020,85(4):1090-1097.
[5]	X X Zhang,X Q Zhou,Z Y Xi,et al. Surfactant-assisted enzymatic extraction of the flavor compounds from Zanthoxylum bungeanum[J]. Separation Science and Technology,2019,55(5):1-10.
[6]	张郁松. 花椒风味物质不同提取方法的比较[J]. 中国调味品,2013,38(6):91-92 ,102.
[7]	孟庆君,李凤飞,杨文江.不同提取方法对花椒提取物提取率和品质的影响[J].中国食品添加剂,2011(6):113-117.
[8]	石雪萍,张卫明. 花椒挥发油的超临界CO₂萃取法与水蒸气蒸馏法提取的比较[J]. 中国野生植物资源,2009,28(6):46-51.
[9]	王芳,石地娟,孙琛,等. 油浸法提取花椒风味物质的研究[J]. 中国调味品,2015,40(6):76-79.
[10]	Z Wenlin,T Si,X Wanpeng,et al. Comparison of volatile components in fresh and dried Zanthoxylum bungeanum Maxim[J]. Food Science and Biotechnology,2019,28(4):1083-1092.
[11]	牛文婧,田洪磊,詹萍. 基于主成分分析的花椒油香气质量评价模型的构建[J]. 食品工业科技,2019,40(17):263-269 ,275.
[12]	何静,陈谷,何倩娴,等. 广陈皮精油的特异性分析[J]. 现代食品科技,2020,36(2):224-231.
[13]	J Ke,Y Qu,S Li,et al. Application of HPLC fingerprint based on acid amide components in Chinese prickly ash(Zanthoxylum)[J]. Industrial Crops and Products,2018,119:267-276.
[14]	田卫环,张蓓. 4种不同产地青、红花椒挥发油成分及香气特征研究[J]. 香料香精化妆品,2017(2):7-11.
[15]	胡丽丽. 花椒调味油制备的研究[D]:成都:西华大学,2013.
[16]	L Hu,C Yin,S Ma,et al. Assessing the authenticity of black pepper using diffuse reflectance mid-infrared Fourier transform spectroscopy coupled with chemometrics[J]. Computers and Electronics in Agriculture,2018,154:491-500.
[17]	T Sriwichai,P Sookwong,M W Siddiqui,et al. Aromatic profiling of Zanthoxylum myriacanthum(makwhaen)essential oils from dried fruits using different initial drying techniques[J]. Industrial Crops and Products,2019,133:284-291.
[18]	Q Guo,W Wu,DL Massart,et al. Feature selection in principal component analysis of analytical data[J]. Chemometrics and Intelligent Laboratory Systems,2002,61(1):123-132.
[19]	蒲凤琳,孙伟峰,车振明,等. 水蒸气蒸馏结合GC-MS法分析比较四川汉源青、红花椒挥发性香气成分[J]. 中国调味品,2017,42(1):23-27.
[20]	W J Zhang,S S Guo,C X You,et al. Chemical composition of essential oils from Zanthoxylum bungeanum Maxim. and their bioactivities against Lasioderma serricorne[J]. Journal of Oleo Science,2016,65(10):871-879.
[21]	孙宝国. 食用调香术[M].北京:化学工业出版社,2010.
[22]	林翔云. 调香术[M]. 3版.北京:化学工业出版社,2013.
[23]	林翔云. 香精香料辞典[M].北京:化学工业出版社,2007.
[24]	王劲. 超临界二氧化碳提取花椒油工艺研究[J]. 中国调味品,2016,41(4):92-95.
[25]	S M Liu,S J Wang,S Y Song,et al. Characteristic differences in essential oil composition of six Zanthoxylum bungeanum Maxim.(Rutaceae)cultivars and their biological significance[J]. Journal of Zhejiang University Science B,2017,18(10):917-920.

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Effect of Three Extraction Methods on the Volatile Components of Zanthoxylum bungeanum