Rapid detection methods for six kinds of synthetic pigments in meat products

JIANG Rong-hua; WU Yu-jie; WEN He-xin; LONG Ying-quan; CAI Xiang-yu; YANG Kun; JIANG Si-hua; TAN Chun-fang

doi:10.13386/j.issn1002-0306.2017.24.054

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Science and Technology of Food Industry > 2017 > (24): 278-281. > DOI: 10.13386/j.issn1002-0306.2017.24.054

JIANG Rong-hua, WU Yu-jie, WEN He-xin, LONG Ying-quan, CAI Xiang-yu, YANG Kun, JIANG Si-hua, TAN Chun-fang. Rapid detection methods for six kinds of synthetic pigments in meat products[J]. Science and Technology of Food Industry, 2017, (24): 278-281. DOI: 10.13386/j.issn1002-0306.2017.24.054

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Rapid detection methods for six kinds of synthetic pigments in meat products

Guigang Entry-Exit Inspection and Quarantine Bureau
Inspection and Quarantine Technology Center of Guangxi Entry-Exit Inspection and Quarantine Bureau

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Received Date: May 10, 2017

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Abstract

Abstract

Objective: To establish a method for simultaneous determination of six kind of synthetic pigments including tartrazine, amaranth, carmine, sunset yellow FCF, allura red and carmosine in meat products by HPLC.Methods: Extracted with ethanol-ammonia-water solution in the samples, then defatted by ether.The pigments were separated on Agilent Poroshell 120 SB-C₁₈ column, by gradient elution with a mobile phases made up of 0.02 mol/L NH4 Ac and acetonitrile, determined by diode array detector ( DAD) .Results: Six kinds of synthetic pigments had good linear relations when the concentration was in the range of 0¹0 μg/mL and the average recoveries range of 70.33%⁹3.08%.The correlation coefficient of regression equations could be up to 0.9999 and relative standard deviation was less than 5%.Conclusion: The method was simple, quickly, sensitivity and good reproducibility, which could be applicable to determine six kinds of synthetic pigments in meat products for lots of samles superviser detection.
- six kinds of synthetic pigments,
- simultaneous determination,
- high performance liquid chromatography,
- meat products

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[1]	Kus E, Eroglu H E.Genotoxic and cytotoxic effects of sunset yellow and brilliant blue, colorant food additives, on human blood lymphocytes[J].Pakistan Journal of Pharmaceutical Sciences, 2015, 28 (1) :227-230.
[2]	Goodman d w.Artificial food colour exclusion and free fatty acid supplementation may reduce symptom severity in children with ADHD[J].Evidence Based Mental Health, 2013, 16 (3) :77.
[3]	Sarikaya R, Selvi M, Erkoc F.Evaluation of potential genotoxicity of five food dyes using the somatic mutation and recombination test[J].Chemosphere, 2012, 88 (8) :974-979.
[4]	葛宇.食品中合成色素使用法规及检测标准进展[J].质量与标准化, 2011 (9) :31-35
[5]	国家卫生和计划生育委员会.GB 2760-2014食品安全国家标准食品添加剂使用标准[S].北京:中国标准出版社, 2014.
[6]	中国国家标准化管理委员会.GB 5009.35-2016食品安全国家标准食品中合成着色剂的测定[S].北京:中国标准出版社, 2004.
[7]	国家质量监督检验检疫总局.SN/T 1743-2006食品中的诱惑红、酸性红、亮蓝、日落黄的含量检测高效液相色谱法[S].北京:中国标准出版社, 2006.
[8]	中国国家标准化管理委员会.GB/T 9695.6-2008肉制品胭脂红着色剂测定[S].北京:中国标准出版社, 2008.
[9]	李莹, 付骋宇, 何强, 等.高效液相色谱法同时检测肉制品中4种着色剂[J].食品安全质量检测学报, 2015, 6 (11) :4416-4421.
[10]	胡汉高, 张红菱, 周威, 等.高效液相色谱法检测熟肉制品中5种人工合成色素方法的建立[J].食品科学, 2011, 32 (20) :171-174
[11]	刘忠秋.高效液相色谱法测定肉制品中人工合成着色剂方法探究[J].辽宁医学院学报.2009, 30 (3) :265
[12]	欧阳燕玲, 陈玲, 谢维平.肉制品中人工合成着色剂测定前处理方法的研究[J].中国卫生检验杂志, 2006, 16 (10) :1269.
[13]	王红梅, 郭伟, 王继鹏, 等.高效液相色谱法测定肉制品中使用合成色素的含量[J].食品研究与开发2007, 28 (6) :106-108.
[14]	林春晓, 曾红慧, 付斌, 等.高效液相色谱法检测熟食肉制品中人工合成色素的研究[J].中国热带医学, 2005, 5 (3) :556-557.
[15]	戚荣平, 邱晓枫, 商晓春.熟肉制品中防腐剂、合成着色剂检测方法的探讨[J].中国卫生检验杂志2009, 19 (1) :50-51.
[16]	俞俊, 周丹, 叶燕, 等.高效液相色谱法测定肉制品中四种合成着色剂的研究[J].安徽化工, 2011, 37 (6) :59-60.
[17]	李瑾瑾.食品中合成着色剂分析方法研究[D].南昌:南昌大学, 2011:27.
[18]	林建忠.HPLC法测定食品中色素条件优化的研究[J].中国卫生检验杂志, 1998, 8 (4) :205.
[19]	Dinc E, Aktas A H, Ustundag O.New liquid chromatographic-chemometric a pproach for the determination of Sunset Yellow and Tartrazine in commercial preparation[J].Journal of AOAC International, 2005, 88 (6) :1748-1755.