Rapid detection methods for six kinds of synthetic pigments in meat products

JIANG Rong-hua; WU Yu-jie; WEN He-xin; LONG Ying-quan; CAI Xiang-yu; YANG Kun; JIANG Si-hua; TAN Chun-fang

doi:10.13386/j.issn1002-0306.2017.24.054

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Science and Technology of Food Industry > 2017 > (24): 278-281. > DOI: 10.13386/j.issn1002-0306.2017.24.054

JIANG Rong-hua, WU Yu-jie, WEN He-xin, LONG Ying-quan, CAI Xiang-yu, YANG Kun, JIANG Si-hua, TAN Chun-fang. Rapid detection methods for six kinds of synthetic pigments in meat products[J]. Science and Technology of Food Industry, 2017, (24): 278-281. DOI: 10.13386/j.issn1002-0306.2017.24.054

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Rapid detection methods for six kinds of synthetic pigments in meat products

Guigang Entry-Exit Inspection and Quarantine Bureau
Inspection and Quarantine Technology Center of Guangxi Entry-Exit Inspection and Quarantine Bureau

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Received Date: May 10, 2017

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Abstract

Abstract

Objective: To establish a method for simultaneous determination of six kind of synthetic pigments including tartrazine, amaranth, carmine, sunset yellow FCF, allura red and carmosine in meat products by HPLC.Methods: Extracted with ethanol-ammonia-water solution in the samples, then defatted by ether.The pigments were separated on Agilent Poroshell 120 SB-C₁₈ column, by gradient elution with a mobile phases made up of 0.02 mol/L NH4 Ac and acetonitrile, determined by diode array detector ( DAD) .Results: Six kinds of synthetic pigments had good linear relations when the concentration was in the range of 0¹0 μg/mL and the average recoveries range of 70.33%⁹3.08%.The correlation coefficient of regression equations could be up to 0.9999 and relative standard deviation was less than 5%.Conclusion: The method was simple, quickly, sensitivity and good reproducibility, which could be applicable to determine six kinds of synthetic pigments in meat products for lots of samles superviser detection.
- six kinds of synthetic pigments,
- simultaneous determination,
- high performance liquid chromatography,
- meat products

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Rapid detection methods for six kinds of synthetic pigments in meat products