Study on the synthesis of L-citrulline chelated zinc by microwave in solid state

LIU Ling; FENG Zhen; YAN Nan; MOU Jie; LIU Yi; ZHENG You-guang; AN Lin; ZHANG Rong-li

doi:10.13386/j.issn1002-0306.2014.08.055

LIU Ling, FENG Zhen, YAN Nan, MOU Jie, LIU Yi, ZHENG You-guang, AN Lin, ZHANG Rong-li. Study on the synthesis of L-citrulline chelated zinc by microwave in solid state[J]. Science and Technology of Food Industry, 2014, (08): 283-285. DOI: 10.13386/j.issn1002-0306.2014.08.055

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Study on the synthesis of L-citrulline chelated zinc by microwave in solid state

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The L-citrulline chelated zinc was synthesized with L-citrulline and zinc acetate as reactants in solid state by microwave. To determine the chelation ratio by single factor and orthogonal experiment, we get the best conditions of reaction:sodium carbonate 15%, microwave power 300W, microwave irradiation time 4min, water 5%. Under the optimal conditions, the average yield of L-citrulline chelated zinc was 91.1%. Meanwhile, the structure of the product was preliminarily confirmed by IR spectrometry.

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Study on the synthesis of L-citrulline chelated zinc by microwave in solid state

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