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中国精品科技期刊2020
孙达锋,胡小松,张沙沙. 电子鼻结合气相-离子迁移谱联用技术分析兰茂牛肝菌气调贮藏期间挥发性风味物质的变化[J]. 食品工业科技,2021,42(21):111−117. doi: 10.13386/j.issn1002-0306.2021070297.
引用本文: 孙达锋,胡小松,张沙沙. 电子鼻结合气相-离子迁移谱联用技术分析兰茂牛肝菌气调贮藏期间挥发性风味物质的变化[J]. 食品工业科技,2021,42(21):111−117. doi: 10.13386/j.issn1002-0306.2021070297.
SUN Dafeng, HU Xiaosong, ZHANG Shasha. Changes in Volatile Compounds of Lanmaoa asiatica during Controlled Atmosphere Storage Using Electronic Nose Combined with Gas Chromatography-Ion Mobility Spectroscopy[J]. Science and Technology of Food Industry, 2021, 42(21): 111−117. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021070297.
Citation: SUN Dafeng, HU Xiaosong, ZHANG Shasha. Changes in Volatile Compounds of Lanmaoa asiatica during Controlled Atmosphere Storage Using Electronic Nose Combined with Gas Chromatography-Ion Mobility Spectroscopy[J]. Science and Technology of Food Industry, 2021, 42(21): 111−117. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2021070297.

电子鼻结合气相-离子迁移谱联用技术分析兰茂牛肝菌气调贮藏期间挥发性风味物质的变化

Changes in Volatile Compounds of Lanmaoa asiatica during Controlled Atmosphere Storage Using Electronic Nose Combined with Gas Chromatography-Ion Mobility Spectroscopy

  • 摘要: 采用电子鼻结合气相-离子迁移谱联用(gas chromatography-ion mobility spectroscopy,GC-IMS)技术探究了兰茂牛肝菌在气调贮藏(气体成分:O2 6%+CO2 10%、温度:(5±0.5)℃、湿度:90%)过程中的香气轮廓及变化趋势。结果表明,新鲜兰茂牛肝菌贮藏13 d后,挥发性香气成分出现明显变化,表征新鲜度明显降低。GC-IMS构建的香气轮廓共有50种挥发性香气成分被检出,其中包括16种醛类、10种醇类、6种酮类、1种酸类、1种酯类和16种未被识别,贮藏第1 d和13 d时挥发性物质的种类和含量最高。兰茂牛肝菌气调贮藏期间醛类化合物的种类和含量明显减少,酮类化合物种类和含量增加,苯乙醛和丙酸可作为兰茂牛肝菌气调贮藏期间特征性挥发性物质。综上所述,电子鼻和GC-IMS联用可快速直观地对不同气调贮藏时间的兰茂牛肝菌进行差异分析,并可快速判断兰茂牛肝菌的新鲜度。

     

    Abstract: The changes in volatile compounds of L. asiatica during controlled atmosphere storage (gas composition: O2 6% and CO2 10%, temperature: (5 ± 0.5) ℃, humidity: 90%) were investigated using electronic nose combined with gas chromatography-ion mobility spectrometry (GC-IMS). The results showed that aroma of the L. asiatica samples clearly changed during storage, particularly after 13 days, indicating the freshness reduced. There were 50 volatile compounds (monomer and dimers) detected using GC-IMS, including 16 aldehydes, 10 alcohols, 6 ketones, 1 acid, 1 ester and 16 un-identified compounds, the types and contents of volatile compounds were the highest at the 1st and 13th days of storage. During the controlled atmosphere storage, the types and content of aldehyde compounds decreased while that of keton compounds increased, benzene acetaldehyde and propanoic acid were the key arom compounds detected in L. asiatica. In general, electronic nose combined with GC-IMS could be an effective approach to quickly detect the freshness of the L. asiatica according to the volatiles changes.

     

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