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中国精品科技期刊2020
李晨辉, 于晓倩, 董汝月, 刘尊英. 明胶/壳聚糖/迷迭香复合膜的制备与表征[J]. 食品工业科技, 2019, 40(10): 57-61,67. DOI: 10.13386/j.issn1002-0306.2019.10.010
引用本文: 李晨辉, 于晓倩, 董汝月, 刘尊英. 明胶/壳聚糖/迷迭香复合膜的制备与表征[J]. 食品工业科技, 2019, 40(10): 57-61,67. DOI: 10.13386/j.issn1002-0306.2019.10.010
LI Chen-hui, YU Xiao-qian, DONG Ru-yue, LIU Zun-ying. Preparation and Characterization of Composite Films Incorporated with Chitosan,Gelatin and Rosemary[J]. Science and Technology of Food Industry, 2019, 40(10): 57-61,67. DOI: 10.13386/j.issn1002-0306.2019.10.010
Citation: LI Chen-hui, YU Xiao-qian, DONG Ru-yue, LIU Zun-ying. Preparation and Characterization of Composite Films Incorporated with Chitosan,Gelatin and Rosemary[J]. Science and Technology of Food Industry, 2019, 40(10): 57-61,67. DOI: 10.13386/j.issn1002-0306.2019.10.010

明胶/壳聚糖/迷迭香复合膜的制备与表征

Preparation and Characterization of Composite Films Incorporated with Chitosan,Gelatin and Rosemary

  • 摘要: 为开发新型具有抗氧化活性的包装材料,以壳聚糖、鱼皮明胶为复合膜基质材料,研究添加迷迭香提取物对复合膜物理性质、微观结构及抗氧化性能的影响。结果表明,添加0.1%迷迭香提取物显著(p<0.05)提高了复合膜的抗氧化性能,将膜的DPPH自由基清除率由15%以下提高到60%以上。迷迭香提取物的添加影响了膜的结构与理化性质。其中,膜的热变性温度由130.97 ℃升至167.52 ℃,同时水溶解性下降了12.62%,但对膜的力学性质没有显著影响。红外光谱显示添加迷迭香提取物影响了O-H键的弯曲和伸缩振动,干扰了复合膜体间的氢键相互作用。研究结果表明,添加0.1%迷迭香提取物既能提高明胶/壳聚糖复合膜的抗氧化能力,又可使复合膜的热稳定性提高,明胶/壳聚糖/迷迭香复合膜活性包装材料具有良好的应用前景。

     

    Abstract: In order to obtain antioxidant activity packaging materials,chitosan-gelatin composite films incorporated with rosemary extract were developed,and the microstructure,physical properties and antioxidant activities of the film were also characterized. The results indicated that the antioxidant activity of the film was significantly(p<0.05)increased after adding 0.1% rosemary extract,and the DPPH free radical scavenging rate of the gelatin-chitosan film was increased from lower than 15% to more than 60%. The microstructure and physicochemical properties of the film were also affected by adding rosemary extract. The thermal denaturation temperature of the film was increased from 130.97 ℃ to 167.52 ℃,and the water solubility of the film was lower 12.62%. However,the mechanical properties of the film were not significantly affected. Fourier transform infrared spectroscopy(FTIR)showed that the incorporation of rosemary extract brought about the changes of hydroxyl groups. The results indicated that incorporating 0.1% rosemary extracts could enhance the antioxidant activity and thermal stability of the film,which would be a feasible way to develop new composite film for active packaging.

     

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