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中国精品科技期刊2020
杨立平, 仪淑敏, 李学鹏, 徐永霞, 李颖畅, 励建荣. 秘鲁鱿鱼丝在加工过程中挥发性风味物质的变化规律[J]. 食品工业科技, 2015, (11): 265-272. DOI: 10.13386/j.issn1002-0306.2015.11.046
引用本文: 杨立平, 仪淑敏, 李学鹏, 徐永霞, 李颖畅, 励建荣. 秘鲁鱿鱼丝在加工过程中挥发性风味物质的变化规律[J]. 食品工业科技, 2015, (11): 265-272. DOI: 10.13386/j.issn1002-0306.2015.11.046
YANG Li-ping, YI Shu-min, LI Xue-peng, XU Yong-xia, LI Ying-chang, LI Jian-rong. Volatile flavor compounds changing in dried- seasoned squid ( Dosidicus gigas) during the processing[J]. Science and Technology of Food Industry, 2015, (11): 265-272. DOI: 10.13386/j.issn1002-0306.2015.11.046
Citation: YANG Li-ping, YI Shu-min, LI Xue-peng, XU Yong-xia, LI Ying-chang, LI Jian-rong. Volatile flavor compounds changing in dried- seasoned squid ( Dosidicus gigas) during the processing[J]. Science and Technology of Food Industry, 2015, (11): 265-272. DOI: 10.13386/j.issn1002-0306.2015.11.046

秘鲁鱿鱼丝在加工过程中挥发性风味物质的变化规律

Volatile flavor compounds changing in dried- seasoned squid ( Dosidicus gigas) during the processing

  • 摘要: 为研究秘鲁鱿鱼丝在加工过程中挥发性风味物质的变化规律,本文采用电子鼻和顶空固相微萃取-气质联用技术(HS-SPME-GC-MS)分析了鱿鱼丝在加工工艺中5个关键控制点(原料、蒸煮4min、40℃烘干、-18℃平衡水分7d、125℃焙烤后压延拉丝)的挥发性风味物质变化。研究表明不同关键控制点样品的电子鼻信号表现出很强的聚类特性,主成分分析(PCA)和载荷分析(LA)测试样品的识别贡献率均达99.8%以上;HS-SPME-GC-MS结果分析出119种物质,各个关键控制点的产品中挥发性风味物质分别是23、31、45、61、35种,并对其中主要的挥发性风味物质的相对含量、相对气味活度值(ROAV)、气味特征及来源进行了计算和分析,表明秘鲁鱿鱼在不同加工过程中挥发性风味物质变化较大,共16种挥发性风味物质对鱼肉气味有显著性贡献,且不同关键控制点的气味物质也不完全相同。 

     

    Abstract: In order to analyze the changes of volatile flavor components of dried- seasoned squid ( Dosidicus gigas) during the processing, the electronic nose ( e Nose) technology and headspace solid phase microextraction combined with gas chromatography- mass spectrometry ( HS- SPME- GC- MS) technology were used to detect the volatile compounds variation of dried- seasoned squid at 5 critical control points, including raw material, cooking4 min, 40℃ drying, -18℃ equilibrium moisture one week and rolling drawing after 125℃ baking.The e Nose signals of different critical control point's samples showed a strong cluster trend.The contribution ratio of the test samples were above 99.8% through principal component analysis ( PCA) and loadings analysis ( LA) , respectively. The total of 119 volatile flavor compounds were identified by HS- SPME- GC- MS, and the kinds during each essential control point of test samples were 23, 31, 45, 61 and 35, respectively. The relative amount, relative odor activity value ( ROAV) , order characteristics and source of volatiles were further calculated and evaluated.Results also indicated that the flavor composition in squid processing changed singnificantly, and the number of contribution volatile flavor compounds to the fish odor was 16 kinds and they were also different in different stages.

     

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