• EI
  • Scopus
  • 食品科学与工程领域高质量科技期刊分级目录第一方阵T1
  • DOAJ
  • EBSCO
  • 北大核心期刊
  • 中国核心学术期刊RCCSE
  • JST China
  • FSTA
  • 中国精品科技期刊
  • 中国农业核心期刊
  • CA
  • WJCI
  • 中国科技核心期刊CSTPCD
  • 中国生物医学SinoMed
中国精品科技期刊2020
李喜悦, 高哲, 崔璨, 安小楠, 王荣芳, 崔同. 枣叶黄酮类成分的分离鉴定及其抗氧化活性研究[J]. 食品工业科技, 2015, (10): 135-138. DOI: 10.13386/j.issn1002-0306.2015.10.019
引用本文: 李喜悦, 高哲, 崔璨, 安小楠, 王荣芳, 崔同. 枣叶黄酮类成分的分离鉴定及其抗氧化活性研究[J]. 食品工业科技, 2015, (10): 135-138. DOI: 10.13386/j.issn1002-0306.2015.10.019
LI Xi-yue, GAO Zhe, CUI Can, AN Xiao-nan, WANG Rong-fang, CUI Tong. Study on structural identification and antioxidant activity of flavonoids from jujube leaves[J]. Science and Technology of Food Industry, 2015, (10): 135-138. DOI: 10.13386/j.issn1002-0306.2015.10.019
Citation: LI Xi-yue, GAO Zhe, CUI Can, AN Xiao-nan, WANG Rong-fang, CUI Tong. Study on structural identification and antioxidant activity of flavonoids from jujube leaves[J]. Science and Technology of Food Industry, 2015, (10): 135-138. DOI: 10.13386/j.issn1002-0306.2015.10.019

枣叶黄酮类成分的分离鉴定及其抗氧化活性研究

Study on structural identification and antioxidant activity of flavonoids from jujube leaves

  • 摘要: 对枣叶的乙醇提取物经乙酸乙酯萃取、高效液相色谱反复制备纯化,得到5种化合物。经LC-MS、1H NMR和13C NMR进行鉴定,分别为:槲皮素-3-O-洋槐糖苷(1)、槲皮素-3-O-芸香糖苷(2)、槲皮素-3-O-β-D-葡萄糖苷(3)、山奈酚-3-O-芸香糖苷(4)、槲皮素-3-O-α-L-阿拉伯糖-(1→2)-α-L-鼠李糖苷(5)。对5种黄酮单体化合物清除ABTS+、DPPH自由基的活性进行了比较,结果表明5种化合物清除ABTS+、DPPH自由基的活性呈现出相同的趋势,其中化合物3表现出最强的活性,化合物1、2、5活性适中,化合物4的活性最低。 

     

    Abstract: Five kind of flavonoids in the jujube leaves were obtained by the isolation with ethanol as the extraction reagent and subsequently purification of ethyl acetate fraction of the ethanol extract by a preparative HPLC, whose structures were verified by1 H NMR and13 C NMR. The five compounds were identified as quercetin-3-O-robinobioside (1) , quercetin-3-O-rutinoside (2) , quercetin-3-O-β-D-glucoside (3) , kaempferol-3-Orutinoside (4) and quercetin-3-O-α-L-arabinosyl- (1→2) -α-L-rhamnoside (5) , respectively. All compounds were evaluated for antioxidant capacity against ABTS+and DPPH radicals. Results revealed similar trends for the capability of the five flavonoids to scavenge the ABTS+and DPPH radicals. Among them, compound 3exhibited the highest activity and compound 1, 2, and 5 showed moderate activity, while compound 4 revealed lower antioxidant capacity.

     

/

返回文章
返回