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中国精品科技期刊2020
刘建彬, 刘梦娅, 何聪聪, 宋焕禄, 王冶, 郭佳. 三种市售牛奶巧克力气味活性化合物的对比及其与感官知觉的关系[J]. 食品工业科技, 2014, (01): 299-303. DOI: 10.13386/j.issn1002-0306.2014.01.037
引用本文: 刘建彬, 刘梦娅, 何聪聪, 宋焕禄, 王冶, 郭佳. 三种市售牛奶巧克力气味活性化合物的对比及其与感官知觉的关系[J]. 食品工业科技, 2014, (01): 299-303. DOI: 10.13386/j.issn1002-0306.2014.01.037
LIU Jian-bin, LIU Meng-ya, HE Cong-cong, SONG Huan-lu, WANG Ye, GUO Jia. Comparison of aroma-active compounds among three types of commercial milk chocolate: relationship to sensory perception[J]. Science and Technology of Food Industry, 2014, (01): 299-303. DOI: 10.13386/j.issn1002-0306.2014.01.037
Citation: LIU Jian-bin, LIU Meng-ya, HE Cong-cong, SONG Huan-lu, WANG Ye, GUO Jia. Comparison of aroma-active compounds among three types of commercial milk chocolate: relationship to sensory perception[J]. Science and Technology of Food Industry, 2014, (01): 299-303. DOI: 10.13386/j.issn1002-0306.2014.01.037

三种市售牛奶巧克力气味活性化合物的对比及其与感官知觉的关系

Comparison of aroma-active compounds among three types of commercial milk chocolate: relationship to sensory perception

  • 摘要: 应用DHDA和顶空感官鉴评对三种市售牛奶巧克力的主要气味活性化合物进行了鉴定和对比。共有23种主要气味活性化合物被鉴定。定量数据及感官鉴评数据应用主成分分析法(PCA)进行了分析。结果表明,巧克力A除在己醛(青草香)、戊基呋喃(甜香)、三甲基吡嗪(坚果香)有较高浓度水平,其它化合物浓度水平都较其它两种品牌巧克力都要低;巧克力C在2-壬酮(甜香、蜜香)、乙酸(酸香、尖刺)、四甲基吡嗪(烤香,焦香)、苯甲醛(苦杏仁香)、2-甲基丙酸(腐臭)、呋喃甲醇(药香)、3-甲基丁酸(酸臭)、乙酸苯乙酯(花香、蜜香)、苯甲酸异戊酯(甜香、花香)这些化合物浓度指标上都比其它两种品牌巧克力要高且较突出;而B巧克力的呈强烈黑巧克力香的3-甲基丁醛(麦芽香、可可香)含量尤为突出,且具有较高含量的二甲基吡嗪类(爆米花香)、糠醛(土豆香)、苯甲醇(药香)、苯乙醇(玫瑰香)、苯并噻唑(橡胶味)、乙酰基吡咯(坚果香),其它的一些呈烤香、坚果香的物质含量也较高。结合感官鉴评数据进行相关性分析表明,在牛奶巧克力中,3-甲基丁醛、苯乙醇主要贡献黑巧克力香韵,乙酸、2-甲基丙酸,3-甲基丁酸主要贡献酸香韵,四甲基吡嗪、乙酸苯乙酯主要贡献烤/坚果香韵。另外,清甜香韵和奶香韵与其它香韵有明显负相关作用。 

     

    Abstract: Applied of dynamic headspace dilution analysis ( DHDA) and headspace sensory evaluation, the prominent aroma-active compounds of three types of commercial milk chocolate were identified and compared.A total of 23 odorants were identified. All the data obtained from the quantification and sensory evaluation was analyzed by principal component analysis ( PCA) . The results showed that chocolate A had the relatively higher content of hexanal ( grassy) , furan, 2-pentyl- ( sweety) , Pyrazine and trimethyl- ( nutty) , while chocolate B had the higher content of 2-methyl butanal ( cocoa-like) , pyrazine, -dimethyl ( popcorn-like) , furfural ( potato-like) , benzyl alcohol ( medicine-like) , phenethyl alcohol ( rosy) , benzothiazole ( rubber-like) and acetylpyrrole, ( nutty) . Chocolate C predominated in the content of 2- methyl butyric acid ( fecal) , isoamyl benzoate ( sweety, honey- like) , furfuryl alcohol ( medicine-like) , tetramethylpyrazine ( roast-like) and phenethyl acetate ( honey- like, floral) .The correlation analysis showed that 2- methyl butanal and benzyl alcohol mainly contribute to the chocolate- like aroma of milk chocolate, while acetic acid, 2- methyl propionic acid and 3- methyl butyric acid mainly contribute the acid- like aroma, tetramethylpyrazine and phenethyl acetate mainly contribute to roast- like /nutty flavor. In addition, the intensity of sweety and milky of milk chocolate exhibited a noteworthy negative correlation compared to other note.

     

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