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中国精品科技期刊2020
刘东傲,解双瑜,李智,等. 不同盐浓度东北农家酱挥发性风味物质的差异分析[J]. 食品工业科技,2022,43(19):356−363. doi: 10.13386/j.issn1002-0306.2022010003.
引用本文: 刘东傲,解双瑜,李智,等. 不同盐浓度东北农家酱挥发性风味物质的差异分析[J]. 食品工业科技,2022,43(19):356−363. doi: 10.13386/j.issn1002-0306.2022010003.
LIU Dongao, XIE Shuangyu, LI Zhi, et al. Analysis on the Difference of the Volatile Flavor Compounds of Northeast Farmhouse Soybean Paste with Different Salt Concentrations[J]. Science and Technology of Food Industry, 2022, 43(19): 356−363. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022010003.
Citation: LIU Dongao, XIE Shuangyu, LI Zhi, et al. Analysis on the Difference of the Volatile Flavor Compounds of Northeast Farmhouse Soybean Paste with Different Salt Concentrations[J]. Science and Technology of Food Industry, 2022, 43(19): 356−363. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2022010003.

不同盐浓度东北农家酱挥发性风味物质的差异分析

Analysis on the Difference of the Volatile Flavor Compounds of Northeast Farmhouse Soybean Paste with Different Salt Concentrations

  • 摘要: 本文研究了东北农家酱发酵过程中盐浓度对其挥发性风味物质的影响。采用顶空固相微萃气相色谱-质谱联用技术(HS-SPME-GC-MS)与电子鼻技术对不同盐浓度(8%、10%、12%)东北农家酱发酵过程中(0、30、60 d)挥发性风味物质的变化与风味特征进行检测,同时通过PCA与聚类分析对样品间的差异性进行统计分析。HS-SPME-GC-MS检测结果表明,发酵0 d时OAV≥0.1的风味物质有2种;发酵30 d时8%、10%与12%盐浓度样品其OAV≥0.1的风味物质分别增加至12、8和8种,发酵60 d时8%、10%、12%盐浓度样品其OAV≥0.1的风味物质分别增加至19、11和10种。且大部分风味物质的OAV值都随着盐浓度的增加而减小。这表明盐浓度对其挥发性风味物质的种类与含量都会产生影响。电子鼻检测结果表明,盐浓度的增加会促进有机硫类化合物的产生,抑制烷烃类、醇类与氢化物类化合物的产生;随发酵时间的增加甲基类、醇类、醛酮类化合物会相应增加而氨类物质、短链烷烃与有机硫化物会相应减少。PCA与聚类分析结果表明,发酵0 d时不同盐浓度样品之间差异很小;而随发酵时间的增加不同盐浓度样品之间的差异会越来越大。综上所述,盐浓度对东北农家酱中的挥发性风味成分会产生显著影响。

     

    Abstract: This paper studied the influence of salt concentration on the volatile flavor compounds during the fermentation of Northeast farmhouse soybean paste. HS-SPME-GC-MS combined with electronic nose technology were used to analyze the changes of volatile flavor substances and flavor characteristics of soybean paste with different salt concentrations (8%, 10%, 12%) during the fermentation process (0, 30, 60 d). The differences between samples were statistically analyzed through PCA and cluster analysis. The results of HS-SPME-GC-MS showed that there were 2 flavors with OAV≥0.1 at 0 days of fermentation. At the time of 30 days, 8%, 10% and 12% salt concentration samples of flavor substances with OAV≥0.1 increased to 12, 8 and 8, respectively. At the time of 60 days, 8%, 10% and 12% salt concentration samples of the flavor substances with OAV≥0.1 increased to 19, 11 and 10, respectively. And the OAV values of most flavor substances decreased with the increase of salt concentration. This indicated that salt concentration affected the type and content of volatile flavor compounds. The results of the electronic nose showed that the increase in salt concentration would promote the production of organic sulfur compounds and inhibit the production of alkanes, alcohols and hydride compounds. With the extension of the fermentation time, the methyl, alcohol, aldehyde and ketone compounds in the soybean paste would gradually increase, while the ammonia, short-chain alkanes and organic sulfides would gradually decrease. The results of PCA and cluster analysis showed that the difference between samples with different salt concentrations fermented for 0 days was very small, and with the extension of the fermentation time, the difference between the soybean paste with different salt concentrations would become more and more significant. To sum up, the salt concentration has a significant effect on the volatile flavor components in the Northeast farmhouse soybean paste.

     

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