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中国精品科技期刊2020
尹航,周文红,白云霞,等. 基于电子鼻、气相-离子迁移谱(GC-IMS)法分析广西螺蛳粉与螺蛳鸭脚煲风味[J]. 食品工业科技,2021,42(9):281−288. doi: 10.13386/j.issn1002-0306.2020070197.
引用本文: 尹航,周文红,白云霞,等. 基于电子鼻、气相-离子迁移谱(GC-IMS)法分析广西螺蛳粉与螺蛳鸭脚煲风味[J]. 食品工业科技,2021,42(9):281−288. doi: 10.13386/j.issn1002-0306.2020070197.
YIN Hang, ZHOU Wenhong, BAI Yunxia, et al. Analysis of the Flavor of Guangxi Luosi-Noodle and Luosi-Hot-Pot by Electronic Nose and Gas Chromatography-Ion Mobility Spectrometry (GC-IMS)[J]. Science and Technology of Food Industry, 2021, 42(9): 281−288. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020070197.
Citation: YIN Hang, ZHOU Wenhong, BAI Yunxia, et al. Analysis of the Flavor of Guangxi Luosi-Noodle and Luosi-Hot-Pot by Electronic Nose and Gas Chromatography-Ion Mobility Spectrometry (GC-IMS)[J]. Science and Technology of Food Industry, 2021, 42(9): 281−288. (in Chinese with English abstract). doi: 10.13386/j.issn1002-0306.2020070197.

基于电子鼻、气相-离子迁移谱(GC-IMS)法分析广西螺蛳粉与螺蛳鸭脚煲风味

Analysis of the Flavor of Guangxi Luosi-Noodle and Luosi-Hot-Pot by Electronic Nose and Gas Chromatography-Ion Mobility Spectrometry (GC-IMS)

  • 摘要: 本文采用气相离子-迁移谱联用技术(gas chromatography-ion mobility spectrometry,GC-IMS),结合电子鼻分析方法,对市场上12个具有代表性的螺蛳粉和螺蛳鸭脚煲进行检测,通过LAV软件对样品挥发性物质的主成分、指纹图谱、相似度加以分析。电子鼻分析显示,螺蛳粉与螺蛳鸭脚煲挥发性物质差异主要源自氮氧化物、甲基类化合物;GC-IMS结果显示,三组样品共发现134个挥发性组分(volatile organic compounds,VOCs),在已定性的38个VOCs中,有33种物质均在螺蛳粉与螺蛳鸭脚煲检测到,造成差异的5个物质来自醛类和酯类;电子鼻和GC-IMS分析结果均表明,螺蛳粉与螺蛳鸭脚煲VOCs相似,相似度得分达到同类食品标准。研究表明,GC-IMS不仅可以通过“指纹”准确直观地分析样品共同及差异特征,而且可通过相似度得分具体量化样品之间的差异大小,此方法在样品风味差异分析中具有优势,但受限于定性普库不全,目前仍需结合其他成熟的风味研究方法。

     

    Abstract: This paper used gas chromatography-ion mobility spectrometry(GC-IMS)and electronic nose analysis to analyze 12 representative Luosi-noodle and Luosi-hot-pot in the market. The main components, fingerprints and similarity of volatile substances in the samples were analyzed by LAV software. Accordinng to the analysis of electronic nose, the difference of volatile matter between Luosi-noodle and Luosi-hot-pot were nitrogen oxides and methyl compounds. The result of GC-IMS showed that volatile organic compounds (VOCs) were found in three groups of samples. In 38 qualitative VOCs, 33 compounds were detected both existed in Luosi-noodle and Luosi-hot-pot. 5 compounds were from aldehydes and esters. The results of electronic nose and GC-IMS analysis showed that Luosi-noodle and Luosi-hot-pot had the same VOCs, and the similarity score reached the same food standard, and the similarity score showed that they belonged to the same food category. Research showed that GC-IMS could not only accurately and intuitively analyze the similarities and differences of the samples through “fingerprints”, but also quantify the differences between samples according to the degree of similarity. This method has advantages in the analysis of the flavor difference of sample, but there is a lack of qualitative sampling, it still needs to be combined with other mature flavor research methods.

     

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